B01J2219/0884

Plasma reactor for liquid and gas and method of use

A system and method for performing plasma reactions creating a plasma area in a gas adjacent to a liquid. An embodiment of the plasma reactor includes a housing with an internal reaction chamber, first and second inlet paths to the reaction chamber, and electrodes for producing an electric field. The system may optionally further include a pre-ionization electrode and pre-ionization electric field for pre-ionizing a feed gas prior to entry into a reaction chamber. The reactor uses plasma to ionize gas adjacent with the liquid. The ionized gas reacts with the liquid to form an effluent. Exemplary uses of the plasma reactor include ionic injection, gas dissociation, liquid re-formation, and liquid dissociation.

System and method for rapid, high throughput, high pressure synthesis of materials from a liquid precursor

The present disclosure relates to a system and method for synthesis of condensed, nano-carbon materials to create nanoparticles. In one embodiment the system may have a source of liquid precursor, a flow control element and a shock wave generating subsystem. The flow control element is in communication with the source of the liquid precursor and creates a jet of liquid precursor. The shock wave generating subsystem drives a shock wave through at least a substantial portion of a thickness of the jet of liquid precursor to sufficiently compress the jet of liquid precursor, and to increase a pressure and a temperature of the jet of liquid precursor, to create solid state nanoparticles.

IN-LIQUID PLASMA GENERATION DEVICE AND LIQUID TREATMENT APPARATUS

An in-liquid plasma generation device includes a housing which holds a liquid in an internal space, a gas supply tube which includes an opening in the internal space and discharges a gas into the liquid through the opening, a first electrode which has projecting part projecting into the internal space via the opening from inside of the gas supply tube, the projecting part including a conductor covered by a dielectric, a second electrode which surrounds the projecting part of the first electrode and includes a conductor isolated from the liquid by a dielectric, and a voltage applier which applies a voltage to between the first electrode and the second electrode. A space between the projecting part and the second electrode is a flow passage in which the gas discharged from the opening flows.

Microwave-Based Recovery Of Hydrocarbons And Fossil Fuels
20200399541 · 2020-12-24 ·

The present invention provides methods for decomposing and extracting compositions for the recovery of petroleum-based materials from composites comprising those petroleum-based materials, comprising subjecting the compositions and/or composites to microwave radiation, wherein the microwave radiation is in the range of from about 4 GHz to about 18 GHz. The present invention also provides for products produced by the methods of the present invention and for apparatuses used to perform the methods of the present invention.

Method for preparing 2,6-dichloropyridine through liquid phase photochlorination of pyridine

The present invention relates to a method for preparing 2,6-dichloropyridine with product purity greater than or equal to 99.0% by using trifluoromethyl chlorobenzene as a solvent for reaction between pyridine and chlorine gas. The preparation process comprises the following steps: enabling pyridine and chlorine gas to continuously experience chlorination reaction under irradiation of ultraviolet light by using pyridine and chlorine gas as starting materials and using trifluoromethyl chlorobenzene as a solvent, and cooling a chlorination reaction product and the solvent to obtain pyridine chlorination solution. Advantages: firstly, it pioneers the precedent of direct and high-selectivity preparation of 2,6-dichloropyridine through liquid phase photochlorination, and not only can the 2,6-dichloropyridine product with purity greater than or equal to 99.0% be obtained, but also industrial production is facilitated; and secondly, not only can the reuse of the separated solvent in the preparation process of the 2,6-dichloropyridine product with purity greater than or equal to 99.0% be realized, but also the purposes of low pollution, low energy consumption and low cost in the preparation process can be realized.

Method, apparatus and system for manufacture of a cyanide
10843931 · 2020-11-24 · ·

A method for producing a cyanide including the steps of supplying a hydrocarbon and nitrogen source to an onsite plasma reactor and removing cyanide synthesised inside the onsite plasma reactor to thereby produce the cyanide is disclosed. Also disclosed is a method which includes a monitor for monitoring the cyanide requirement of an onsite cyanide utilising system and supplying the hydrocarbon and nitrogen source in accordance with the cyanide requirement. Additionally, a method for recovering, refining, purifying or treating a metal including the steps of monitoring a cyanide requirement of the method and supplying to the method in a just in time sequence a cyanide synthesised onsite to thereby recover, refine, purify or treat the metal is disclosed.

Alkali source and/or sink using ion-conducting solid electrolyte and mixed ion-electron conductor electrode

Some variations provide an alkali metal or alkaline earth metal atom source (e.g., vapor cell) with a solid ionic conductor and a mixed ion-electron conductor electrode. Mixed ion-electron conductor electrodes are used as efficient sources and/or as sinks for alkali metal or alkaline earth metal atoms, thus enabling electrical control over metal atom content in the vapor cell. Some variations provide a vapor-cell system comprising: a vapor-cell region configured to allow a vapor-cell optical path into a vapor-cell vapor phase; a first electrode containing an mixed ion-electron conductor that is conductive for an ion of at least one element selected from Rb, Cs, Na, K, or Sr; a second electrode electrically isolated from the first electrode; and an ion-conducting layer between the first electrode and the second electrode. The ion-conducting layer is ionically conductive for at least one ionic species selected from Rb.sup.+, Cs.sup.+, Na.sup.+, K.sup.+, or Sr.sup.2+.

APPARATUS, SYSTEM, AND METHOD FOR PROCESSING OF MATERIALS
20200308493 · 2020-10-01 ·

System, apparatuses, and methods for processing feedstock have a decomposing stage for breaking down feedstock into liquid and gaseous products and a condensing stage for condensing gaseous products to a liquid condensate. A mixing stage can also be used to combine gaseous and liquid feedstock portions into a combined liquid feedstock to be fed to the decomposing stage. The decomposing stage can be one or more flux tanks having a field generator for creating an electromagnetic field through the flux tank configured to decompose feedstock inside. The condensing stage can have a catalyst tank, distillation tank, condensing pipes, or a combination thereof. The mixing stage can be a reformer device having pairs of plates, at least some of the plates are capable of rotating to generate a shear force that creates a cavitation effect to combine the gaseous and liquid feedstock portions.

Apparatus and method for treating gas in a liquid medium with ultrasonic energy for chemical reaction

A gas conversion apparatus (100) for converting a process gas to one or more other gases comprises: means (105) for introducing process gas into a liquid medium in a column (125); and an ultrasonic energy generator (140) arranged to generate ultrasonic energy, the apparatus (100) being configured to launch ultrasonic energy generated by the generator (140) into the liquid medium such that process gas is exposed to ultrasonic energy, the apparatus (100) being arranged to allow collection of process gas that has been exposed to ultrasonic energy. The apparatus (100) also preferably comprises a microbubble generator (120) to generate microbubbles of the process gas for exposure to the ultrasonic energy. The ultrasonic energy generator (140) may be configured to generate ultrasonic energy as a consequence of a flow of a drive gas therethrough.

Photocatalytic reduction of carbon dioxide to methanol or carbon monoxide using cuprous oxide

Provided herein are methods of CO.sub.2 reduction to methanol or CO using a Cu.sub.2O catalyst.