B01J2219/089

CONTINUOUS PRODUCTION EQUIPMENT AND PREPARATION METHOD FOR GRAPHENE COMPOSITE MATERIAL

Continuous production equipment for graphene composite material includes a raw material preparation device; a reaction device, a material discharge end of the raw material preparation device being connected to the reaction device; and an extraction device configured to extract and purify crude composite material obtained from the reaction device, a material feed end of the extraction device being connected to the material discharge end of the reaction device, and a material discharge end of the extraction device being configured to convey polyamide monomer extract obtained by extraction to a liquid conveying pipe of the raw material preparation device. The raw material preparation device includes a raw material melting kettle configured to melt polyamide monomer and mix the molten polyamide monomer with graphene, and the raw material melting kettle is provided with a high-shear emulsifying machine and an ultrasonic disperser.

Method of making graphene nanocomposites by multiphase fluid dynamic dispersion
10106419 · 2018-10-23 · ·

A method of dispersing graphene and graphitic nanomaterials uses a multiphase fluid dynamic technique. The method includes a device, incorporating a high intensity fluid dynamics technique, controlling the expansion and compression ratio of the working stream that leads to an effective dispersion of the nanomaterial in the matrix. The condensation of the injected steam creates high intensity and controllable cavitation, leading to effective dispersion of the graphitic nanomaterial. The dispersion is most preferably done in a medium that creates a repulsive potential to balance the attractive inter-graphitic layer potential.

Plasma-arc-through apparatus and process for submerged electric arcs with venting
10100416 · 2018-10-16 · ·

An application for a recycler includes a pressure and temperature resistant metal vessel that is filled with a liquid. Within the vessel is at least one submerged electric arc between a pair of electrodes (e.g. carbon based electrodes) powered by either a DC or AC current. The electric arc produces a combustible gas as the liquid is pumped through a bore in one or both of the electrodes, delivering the liquid directly to the location of the arc, thereby reducing or eliminating any ignition of the gas by the arc. Should ignition occur, at least one vent in the electrode(s) or electrode holder(s) vents pressure from within the bore to the vessel area outside of the electrode(s).

Direct Microwave Production of Graphene
20180286599 · 2018-10-04 · ·

Provided is a method of producing graphene directly from a non-intercalated and non-oxidized graphitic material, comprising: (a) dispersing the graphitic material in a liquid solution to form a suspension, wherein the graphitic material has never been previously exposed to chemical intercalation or oxidation; and (b) subjecting the suspension to microwave or radio frequency irradiation with a frequency and an intensity for a length of time sufficient for producing graphene; wherein the liquid solution contains a metal salt dissolved in water, organic solvent, ionic liquid solvent, or a combination thereof. The method is fast (minutes as opposed to hours or days of conventional processes), environmentally benign, and highly scalable.

PHOTOCATALYST PRODUCTION METHOD, AND HYDROGEN AND OXYGEN PRODUCTION METHOD USING SAID PHOTOCATALYST

Provided is a photocatalyst with significantly enhanced water splitting performance in YTOS or in a composition in which the yttrium element of YTOS has been replaced with another element. Also provided is a method for producing a photocatalyst that has a composition represented by the following general formula (I), the method including mixing, with a raw material of the photocatalyst, a flux component at a mass ratio of 0.01 times to 50 times, the flux component being composed of one or more chlorides and/or iodides of at least one selected from Li, Na, K, Rb, Mg, Ca, Sr, and Ba, and calcining a resultant product at 450? C. to 1050? C.:


M.sub.aTi.sub.bO.sub.cS.sub.d(I)

(where M is a combination of one or more selected from Pr, Nd, Pm, Sm, Eu, Gd, Tb, Dy, Ho, Er, Tm, and Y, a is a number of 1.7 to 2.3, b is a number of 2, c is a number of 4.7 to 5.3, and d is a number of 1.7 to 2.3).

METHOD FOR MANUFACTURING ZINC PHOSPHATE (ZN3(PO4)2)

The present disclosure relates to a method for producing zinc phosphate with the application of ultrasound having a frequency greater than 100 KHZ.

Low cost and fast method to massively produce graphene and graphene oxide with carbon-rich natural materials and the use of the same
12091322 · 2024-09-17 ·

This invention provides an innovative method to manufacture graphene layers or quantities and graphene oxide layers or quantities from graphite, coal slags, asphalt, and other carbon-rich sold materials in nature. The present invention uses controllable microwave irradiation to heat the mixtures of basic material, graphite, or coal slags, or asphalt, or their combinations with ionic liquids and surfactant plus environmentally friendly oxidation agents. This invention can generate the said-products of graphene layers and graphene oxides in a short time period of one second to 300 seconds. The present invention does not involve any concentrated sulfuric acid, nitric acid, nor huge water quantities needed for the purification, unlike the prior art. The as-produced graphene-based materials can be used for preparing conductive films for touch screens, producing graphene carbon fibers and three-dimensional porous graphene nanomaterials, and preparing graphene-based other intelligent nanocomposites for super-light-weight machines and vehicles.

Method and apparatus for producing core-shell type metal nanoparticles

A method and apparatus for producing core-shell type metal nanoparticles which are excellent in productivity are provided, in particular, the present invention provides a method of production of core-shell type metal nanoparticles including (a) a step of introducing a solution of a salt of a first metal to a first flow path of a flow type reaction apparatus and applying plasma to the solution of the salt of the first metal in the first flow path to obtain a solution which contains metal nanoparticles of the first metal and (b) a step of introducing a solution of a salt of a second metal to a second flow path of the flow type reaction apparatus, making it merge with the solution which contains metal nanoparticles of the first metal to obtain a mixed solution, and applying plasma to the mixed solution to cover the metal nanoparticles of the first metal by the second metal.

SYSTEM AND APPARATUS FOR PROCESSING MATERIAL TO GENERATE SYNGAS WITH A MULTI-PHASE POWER SOURCE

System for processing material to generate syngas in a modular architecture may include a plurality of primary reactor chambers and a shared secondary reactor chamber. Each primary reactor chamber includes electrodes protruding into the chamber, the electrodes operable to generate an arc capable to generate first-stage gas from breakdown of the material when electricity is applied to the electrodes. The secondary reactor chamber is operable to receive the first-stage gas generated by the plurality of primary reactor chambers and to receive water vapour. The gas generated within the plurality of primary reactor chambers combine and interact with the water vapour to form second-stage gas. Turbulence can be generated within the secondary reactor chamber to improve mixing of the first-stage gas with the water vapour. Powering of each of the primary reactor chambers can be done with a different phase of power from a multi-phase input to ensure balanced power utilization.

Pressure stepped microwave assisted digestion

An instrument and method for high pressure microwave assisted chemistry are disclosed. The method includes the steps of applying microwave radiation to a sample in a sealed vessel while measuring the temperature of the sample and measuring the pressure generated inside the vessel and until the measured pressure reaches a designated set point, opening the vessel to release gases until the pressure inside the vessel reaches a lower designated set point, closing the vessel, and repeating the steps of opening the vessel at designated pressure set points and closing the vessel at designated pressure set points to the sample until the sample reaction reaches a designated high temperature. The designated set points can controllably differ from one another as the reaction proceeds. Microwave energy can be applied continuously or intermittently during the opening and closing steps. The apparatus includes a microwave cavity, a microwave transparent pressure resistant reaction vessel in the cavity, a cap on the reaction vessel, a pressure sensor for measuring pressure in the vessel, a temperature sensor, and means for opening and closing the cap at predetermined pressure set points measured by the pressure sensor to release pressure from the vessel.