Disclosed is a nano dispersion copper alloy with high air-tightness and low free oxygen content and a brief manufacturing process thereof, wherein alloy comprises the following components: Al.sub.2O.sub.3, Ca and La. The manufacturing process comprises the following steps of: preparing Cu—Al.sub.2O.sub.3 alloy powder by an internal oxidation method; mixing the Cu—Al.sub.2O.sub.3 alloy powder with Cu—Ca—La alloy powder; sheathing the mixed powder under protection of argon; performing hot extrusion and then rotary forging; vacuumizing the sheath after the rotary forging; and sealing and placing the sheath in a nitrogen atmosphere with a temperature of 450° C. to 550° C. and a pressure intensity of 40 Mpa to 60 Mpa for 3 hours to 5 hours. The dispersion copper prepared by the present disclosure has the advantages of low free oxygen content (≤15 ppm), high dimensional stability, good air-tightness and an air leakage rate≤1.0×10.sup.−10 Pa m.sup.3/s after hydrogen annealing.

A carbon-coated transition metal nanocomposite material includes carbon-coated transition metal particles having a core-shell structure. The shell layer of the core-shell structure is a graphitized carbon layer doped with oxygen and/or nitrogen, and the core of the core-shell structure is a transition metal nanoparticle. The nanocomposite material has a structure rich in mesopores, is an adsorption/catalyst material with excellent performance, can be used for catalyzing various hydrogenation reduction reactions, or used as a catalytic-oxidation catalyst useful for the treatment of volatile organic compounds in industrial exhaust gases.

The present invention relates to a method for manufacturing a needle-shaped or rod-shaped porous iron powder. Specifically, the present invention provides a method for manufacturing a needle-shaped or rod-shaped porous iron and a needle-shaped or rod-shaped porous iron powder manufactured thereby, the method comprising the steps of: preparing a ferrous chloride dehydrate by concentrating a ferrous chloride aqueous solution; solid-liquid separating the ferrous dichloride to prepare ferrous chloride dehydrate powder; oxidizing the ferrous chloride dehydrate powder; and reducing the oxidized ferrous chloride powder.

The present invention relates to a method for manufacturing a needle-shaped or rod-shaped porous iron powder. Specifically, the present invention provides a method for manufacturing a needle-shaped or rod-shaped porous iron and a needle-shaped or rod-shaped porous iron powder manufactured thereby, the method comprising the steps of: preparing a ferrous chloride dehydrate by concentrating a ferrous chloride aqueous solution; solid-liquid separating the ferrous dichloride to prepare ferrous chloride dehydrate powder; oxidizing the ferrous chloride dehydrate powder; and reducing the oxidized ferrous chloride powder.

Disclosed herein is a method for reducing a metal oxide in a metal containing precursor. The method comprises providing a reaction mixture comprising the metal oxide containing precursorand an aluminium reductant; heating the reaction mixture in the presence of solid or gaseous aluminium chloride to temperature at which reactionsthatresultin the metal oxide being reduced are initiated; controlling reaction conditions whereby the reaction mixture is prevented from reaching a temperature at which thermal runaway can occur; and isolating reaction products that include reduced metal oxide.

A method for manufacturing a catalyst for a fuel cell can include provision of a platinum precursor and a carbon material. The platinum precursor and the carbon material can be mixed to form a platinum carbon mixture. The platinum carbon mixture can be heated to form a porous solid. The porous solid can be milled to form a powder. The powder can be reacted with a reducing agent to form the catalyst.

A method for manufacturing a catalyst for a fuel cell can include provision of a platinum precursor and a carbon material. The platinum precursor and the carbon material can be mixed to form a platinum carbon mixture. The platinum carbon mixture can be heated to form a porous solid. The porous solid can be milled to form a powder. The powder can be reacted with a reducing agent to form the catalyst.

A method for manufacturing a catalyst for a fuel cell can include provision of a platinum precursor and a carbon material. The platinum precursor and the carbon material can be mixed to form a platinum carbon mixture. The platinum carbon mixture can be heated to form a porous solid. The porous solid can be milled to form a powder. The powder can be reacted with a reducing agent to form the catalyst.

A method of forming a nanoparticle can include admixing an aqueous solution into an oil-phase to thereby form an emulsion of droplets of the aqueous solution in the oil phase, the aqueous solution comprising a nanostructure precursor and a polymer, adding a silane precursor and catalyst to form a silica shell around each of the droplets to nanoreactors; annealing at a first temperature below the decomposition temperature of the polymer to aggregate the nanostructure precursor within the nanoreactor; and annealing at a second temperature above the decomposition temperature of the polymer to convert the aggregated nanostructure precursor to the nanostructure and decompose the polymer.

A method of forming a nanoparticle can include admixing an aqueous solution into an oil-phase to thereby form an emulsion of droplets of the aqueous solution in the oil phase, the aqueous solution comprising a nanostructure precursor and a polymer, adding a silane precursor and catalyst to form a silica shell around each of the droplets to nanoreactors; annealing at a first temperature below the decomposition temperature of the polymer to aggregate the nanostructure precursor within the nanoreactor; and annealing at a second temperature above the decomposition temperature of the polymer to convert the aggregated nanostructure precursor to the nanostructure and decompose the polymer.