The present invention relates to a method for producing a metal nanoparticle-polymer composite thin film comprising uniformly shaped metal nanoparticles uniformly dispersed in a polymer matrix, and more particularly to a method for producing a gold nanoparticle-polymer composite thin film, comprising the steps of: (A) preparing a mixture of an ionic liquid and polyethylene oxide; (B) preparing a reaction solution by dissolving a gold nanoparticle precursor in the mixture; (C) producing a gold nanoparticle-polymer composite by applying plasma to the interface of the reaction solution; and (D) separating the gold nanoparticle-polymer composite from the reaction solution.

Disclosed is a method for preparing vanadium or vanadium alloy powder from a vanadium-containing raw material through a shortened process, including: calcinating a mixture of a vanadium-containing raw material and an alkali compound for oxidation to form a water-soluble vanadate; purifying the vanadate followed by vanadium precipitation to produce an intermediate CaV.sub.2O.sub.6 with high purity; dissolving CaV.sub.2O.sub.6 in a molten-salt medium together with other raw materials to form a uniform reaction system; and introducing a reducing agent to the system followed by separation, washing and drying to produce vanadium or vanadium alloy powder having a particle size of 50-800 nm and a purity of 99.0 wt % or more. The method can continuously process vanadium-containing raw materials to prepare vanadium or vanadium alloy powder.

A large-scale multi-step synthesis method for ultralong silver nanowire with controllable diameter, comprises: an ethylene glycol solution containing polyvinylpyrrolidone and sodium chloride is fully heated to obtain a solution with strong reducibility, and then silver nitrate in glycol solution is added for a generation of a large number of crystal seeds; hydrogen peroxide is used to achieve the selection of the crystal seeds for a small amount of crystal seeds with particular sizes; the temperature is immediately raised to increase the reaction rate until the threshold of the etching crystal seeds of nitric acid is broke through; the temperature is lowered for long-timed reaction to slow down the reaction rate, reduce the probability of the isotropic seeds by self-nucleation and promote the absorption of small nucleus in the radial direction of large nucleus or nanowire, thus obtaining the ultralong silver nanowire.

A method for manufacturing a ferromagnetic-particle includes preparing a manufacturing apparatus including a single mode cavity that resonates with a microwave of a predetermined wavelength; a microwave oscillator electrically connected to the single mode cavity and configured to introduce the microwave of a predetermined wavelength into the single mode cavity; a pipe disposed to pass linearly through an inside of the single mode cavity, the pipe being formed of a dielectric material; and a pump configured to introduce, from one end of the pipe, an alkaline reaction liquid in which metal ions of a ferromagnetic metal and hydroxide ions are dissolved; and reacting the reaction liquid in the pipe, introduced by the pump, by introducing the microwave into the single mode cavity so as to generate the ferromagnetic-particle in the pipe.

A method for manufacturing a ferromagnetic-particle includes preparing a manufacturing apparatus including an induction heating coil; a radiofrequency power source electrically connected to the induction heating coil and configured to form an alternating field inside the induction heating coil; a pipe disposed to pass through the induction heating coil, in which at least a partial area of the pipe in an axial direction thereof is formed of a dielectric material and an area, which is nearer to one end of the pipe than the area formed of a dielectric material, is formed of a conductive material; and a pump configured to introduce, from the one end of the pipe, an alkaline reaction liquid in which metal ions of a ferromagnetic metal and hydroxide ions are dissolved; reacting the reaction liquid in the pipe, introduced by the pump, by forming an alternating field inside the induction heating coil; and generating the ferromagnetic-particle in the pipe based on the reaction of the reaction liquid in the pipe.

The present invention achieves a high-energy product using Ferromagnetic 3D elements such as nanowires and methods of making the same. The high energy products or magnets of the invention are able to achieve high magnetization and maintain the magnetic properties at a greater range of temperatures than currently known magnets. For example, a high energy product includes at least one material A selected from the group consisting essentially of Fe, Co, and Ni, wherein material A is in the form of nanowires formed by a solvothermal chemical process. A high energy product may also include at least one material A selected from the group consisting essentially of Fe, Co, and Ni, and at least one material B selected from the group consisting essentially of Fe, Co, and Ni, wherein material A and material B are in the form of an alloy of nanowires formed by a solvothermal chemical process.

Invention provides a one step process for the preparation of metal nanoparticles which are stable at room temperature under normal storage condition for more than 6 months, retain their colloidal and dispersive nature at neutral, acidic (pH <7) and basic (pH >7) pH conditions and can maintain their stability and colloidal nature at low (while frozen), high temperatures and pressure, from water soluble metal chlorides and hydrides.

The present invention provides a preparation method for gold nanoparticles based on functionalized ionic liquid. The method comprises synthesizing a functionalized ionic liquid, 3-(12-bromo-dodecyl)-1-(3-pyrrole propyl)-imidazole bromide, as a stabilizer for synthesizing gold nanoparticles, adjusting the concentration of the ionic liquid and the dosage of the reducing agent, thereby successfully preparing the icosahedral gold nanoparticles, and characterizing the morphology thereof by TEM, XRD and SEM. In the present invention, the method employed for preparing the stabilizer is simple, non-toxic, harmless and pollution-free, moreover the preparation of gold nanoparticles by aqueous phase has the advantages of mild conditions, short reaction time, simple operation, green and pollution-free, and belongs to the environment-friendly preparation.

Processes for preparing stabilized metal-containing nanoparticles comprising silver and/or a silver alloy composite by reacting a silver compound with a reducing agent comprising a hydrazine compound at a temperature between about 20 C. and about 60 C. The reaction being carried out by incrementally adding the silver compound or a mixture of the silver compound and a stabilizer to a solution comprising the reducing agent, a stabilizer, and a solvent. Conductive ink compositions containing stabilized metal-containing nanoparticles prepared by such processes.

A method for producing silver nanowires, containing reduction-precipitating silver in the form of wire in an alcohol solvent having dissolved therein a silver compound, the deposition being performed in the alcohol solvent having dissolved therein a chloride, a bromide, an alkali metal hydroxide, an aluminum salt, and an organic protective agent, the molar ratio Al/OH of the total Al amount of the aluminum salt dissolved in the solvent and the total hydroxide ion amount of the alkali metal hydroxide dissolved therein being from 0.01 to 0.40, the molar ratio OH/Ag of the total hydroxide ion amount of the alkali metal hydroxide dissolved in the solvent and the total Ag amount of the silver compound dissolved therein being from 0.005 to 0.50.