B22F2009/245

METHOD FOR CONTINUOUS AND CONTROLLABLE PRODUCTION OF SINGLE WALLED CARBON NANOTUBES
20190232375 · 2019-08-01 ·

The present disclosure is directed to methods for producing a single-walled carbon nanotube in a chemical vapor deposition (CVD) reactor. The methods comprise contacting liquid catalyst droplets and a carbon source in the reactor, and forming a single walled carbon nanotube at the surface of the liquid catalyst droplets.

Fine silver particle dispersing solution

In a fine silver particle dispersing solution wherein 30 to 75% by weight of fine silver particles, which are coated with an organic acid having a carbon number of 5 to 8 or a derivative thereof and which have an average particle diameter of 1 to 100 nm, are dispersed in a water-based dispersion medium which is a solvent containing water as a main component, the fine silver particle dispersing solution containing ammonia and nitric acid, there is added 0.15 to 0.6% by weight of a surface regulating agent, which preferably contains a polyether-modified polydimethylsiloxane and a polyoxyethylene alkyl ether or a polyether, or 0.005 to 0.6% by weight of an antifoaming agent which is preferably a silicone antifoaming agent.

Method for preparing nano-silver powder and application in preparation of electrically conductive ink of the nano-silver powder and electrically conductive ink

A method for preparing nano-silver powder dispersible in environment friendly weak solvents, and an electrically conductive ink comprising the nano-silver powder are disclosed. The disclosure describes a disperser dissoluble in water and weak solvents and an alcohol amine as reducing agent to prepare mono-dispersed nano-silver, and employs ultrafiltration for purification and spray drying process to obtain a nano-silver powder dispersible in weak solvents, and thereby obtain an eco-solvent nano-silver electrically conductive ink. The electrically conductive ink in accordance with the disclosure has advantages of high safety, low volatility, low toxicity, high flash point, resistant to ultraviolet radiation and moisture etc., and can be used with uncoated bearing substrates, and is suitable for use in outdoor environments.

FERROMAGNETIC-PARTICLE MANUFACTURING APPARATUS

A method for manufacturing a ferromagnetic-particle includes preparing a manufacturing apparatus including a single mode cavity that resonates with a microwave of a predetermined wavelength; a microwave oscillator electrically connected to the single mode cavity and configured to introduce the microwave of a predetermined wavelength into the single mode cavity; a pipe disposed to pass linearly through an inside of the single mode cavity, the pipe being formed of a dielectric material; and a pump configured to introduce, from one end of the pipe, an alkaline reaction liquid in which metal ions of a ferromagnetic metal and hydroxide ions are dissolved; and reacting the reaction liquid in the pipe, introduced by the pump, by introducing the microwave into the single mode cavity so as to generate the ferromagnetic-particle in the pipe.

LARGE-SCALE MUTL-STEP SYNTHESIS METHOD FOR ULTRALONG SILVER NANOWIRE WITH CONTRALLABLE DIAMETER
20190168309 · 2019-06-06 ·

A large-scale multi-step synthesis method for ultralong silver nanowire with controllable diameter, comprises: an ethylene glycol solution containing polyvinylpyrrolidone and sodium chloride is fully heated to obtain a solution with strong reducibility, and then silver nitrate in glycol solution is added for a generation of a large number of crystal seeds; hydrogen peroxide is used to achieve the selection of the crystal seeds for a small amount of crystal seeds with particular sizes; the temperature is immediately raised to increase the reaction rate until the threshold of the etching crystal seeds of nitric acid is broke through; the temperature is lowered for long-timed reaction to slow down the reaction rate, reduce the probability of the isotropic seeds by self-nucleation and promote the absorption of small nucleus in the radial direction of large nucleus or nanowire, thus obtaining the ultralong silver nanowire.

METHOD FOR PRODUCING TANTALUM POWDER FOR CAPACITORS BY REDUCING TANTALUM OXIDE WITH ALKALINE EARTH METAL

A method produces tantalum powder by reducing tantalum oxide with an alkaline earth metal. The method includes (1) mixing tantalum oxide with an excessive alkaline earth metal reducing agent, simultaneously mixing at least one alkali metal and/or alkaline earth metal halide accounting for 10-200% of the weight of the tantalum oxide, heating the mixture to a temperature of 700-1200? C. in a furnace filled with inert gas, and soaking so that the tantalum oxide and reducing agent are subjected to a reduction reaction; (2) at the end of soaking, lowering the temperature to 600-800? C., vacuumizing the interior of the furnace to 10 Pa or less, and soaking under the negative pressure so that the excessive magnesium and tantalum powder mixture are separated; (3) thereafter, raising the temperature of the furnace to 750-1200? C. in the presence of inert gas, and soaking so that the tantalum powder is further sintered in the molten salt; (4) then cooling to room temperature and passivating to obtain a mixed material containing halide and tantalum powder; and (5) separating the tantalum powder from the mixture.

NANOHYBRID STRUCTURES CONTAINING ANTIMICROBIAL NANOPARTICLES
20240180161 · 2024-06-06 · ·

This invention relates to forming unique nanohybrid structures through selective integration of inorganic antimicrobial nanoparticles with other inorganic and organic materials and then, chemically bonding the nanohybrid structures to organic polymers for application as surface coatings, antimicrobial surfacing, food packaging, biomedical, agricultural, air-filtration/cleaning and water filtration/cleaning applications to kill, inhibit, and/or reduce the growth of pathogenic/infectious/contaminating microorganisms and their biofilms.

METHOD FOR PRODUCING SILVER NANOWIRES, SILVER NANOWIRES, AND INK USING SAME

A method for producing silver nanowires, containing reduction-precipitating silver in the form of wire in an alcohol solvent having dissolved therein a silver compound, the deposition being performed in the alcohol solvent having dissolved therein a chloride, a bromide, an alkali metal hydroxide, an aluminum salt, and an organic protective agent, the molar ratio Al/OH of the total Al amount of the aluminum salt dissolved in the solvent and the total hydroxide ion amount of the alkali metal hydroxide dissolved therein being from 0.01 to 0.40, the molar ratio OH/Ag of the total hydroxide ion amount of the alkali metal hydroxide dissolved in the solvent and the total Ag amount of the silver compound dissolved therein being from 0.005 to 0.50.

Method For Producing Metal Nanoparticle-Polymer Composite Thin Film

The present invention relates to a method for producing a metal nanoparticle-polymer composite thin film comprising uniformly shaped metal nanoparticles uniformly dispersed in a polymer matrix, and more particularly to a method for producing a gold nanoparticle-polymer composite thin film, comprising the steps of: (A) preparing a mixture of an ionic liquid and polyethylene oxide; (B) preparing a reaction solution by dissolving a gold nanoparticle precursor in the mixture; (C) producing a gold nanoparticle-polymer composite by applying plasma to the interface of the reaction solution; and (D) separating the gold nanoparticle-polymer composite from the reaction solution.

Silver powder, method for producing same, and hydrophilic conductive paste

A silver powder, wherein the silver powder satisfies D.sub.50-IPA>D.sub.50-W, where in measurement of a volume-based particle size distribution of the silver powder by a laser diffraction particle size distribution analysis, D.sub.50-IPA (m) is a cumulative 50% point of particle diameter of the silver powder when isopropyl alcohol (IPA) is used as a measurement solvent for dispersing the silver powder, and D.sub.50-W (m) is a cumulative 50% point of particle diameter of the silver powder when water is used as a measurement solvent for dispersing the silver powder, and wherein a phosphorus content in the silver powder is 0.01% by mass or more but 0.3% by mass or less.