Provided is a method with which it is possible to prevent equipment, such as piping and valves, used to discharge and recover a nickel powder-containing slurry from a high pressure reaction tank from being damaged and trapping the nickel powder therein and to enable continuous operation, thereby improving the productivity. This nickel powder production method comprises a step of reacting a nickel sulfate-amine complex solution with hydrogen gas under high pressure in a reaction tank, thereby obtaining a nickel powder slurry containing nickel powder. The method is characterized in that the nickel powder slurry is discharged and transferred through discharge piping from the reaction tank in which the nickel powder-containing slurry has been produced, and then a washing solution is supplied to the discharge piping at a predetermined pressure to wash the discharge piping.

Provided is nickel powder obtained by adding seed crystals to a nickel ammine complex solution and performing hydrogen reduction reaction under high temperatures and high pressures, wherein the nickel powder does not produce dust during handling, and a container can be efficiently filled with the nickel powder. The method for producing nickel powder includes: adding seed crystals and a surfactant having a nonionic or anionic functional group to a solution containing a nickel ammine complex to forma mixed slurry; and subjecting the mixed slurry to hydrogen reduction under high temperature and high pressure conditions in a pressure vessel to obtain nickel powder from the mixed slurry.

Provided is nickel powder obtained by adding seed crystals to a nickel ammine complex solution and performing hydrogen reduction reaction under high temperatures and high pressures, wherein the nickel powder does not produce dust during handling, and a container can be efficiently filled with the nickel powder. The method for producing nickel powder includes: adding seed crystals and a surfactant having a nonionic or anionic functional group to a solution containing a nickel ammine complex to forma mixed slurry; and subjecting the mixed slurry to hydrogen reduction under high temperature and high pressure conditions in a pressure vessel to obtain nickel powder from the mixed slurry.

Provided is nickel powder obtained by adding seed crystals to a nickel ammine complex solution and performing hydrogen reduction reaction under high temperatures and high pressures, wherein the nickel powder does not produce dust during handling, and a container can be efficiently filled with the nickel powder. The method for producing nickel powder includes: adding seed crystals and a surfactant having a nonionic or anionic functional group to a solution containing a nickel ammine complex to forma mixed slurry; and subjecting the mixed slurry to hydrogen reduction under high temperature and high pressure conditions in a pressure vessel to obtain nickel powder from the mixed slurry.

According to one or more embodiments presently described, a mixture of lead oxide and lead metal particles may be formed by a method that includes forming a molten metal lead material from a solid lead metal supply material, introducing the molten metal lead material into a reaction zone of a reactor, and contacting the molten metal lead material with an oxidizing gas in the reaction zone to oxidize a portion of the molten metal lead material and form at least solid lead oxide particles and solid lead metal particles. The molten metal lead material may be introduced to the reaction zone in a laminar flow or as atomized molten particles. The weight ratio of formed solid lead oxide particles to solid lead metal particles may be less than 99:1.

According to one or more embodiments presently described, a mixture of lead oxide and lead metal particles may be formed by a method that includes forming a molten metal lead material from a solid lead metal supply material, introducing the molten metal lead material into a reaction zone of a reactor, and contacting the molten metal lead material with an oxidizing gas in the reaction zone to oxidize a portion of the molten metal lead material and form at least solid lead oxide particles and solid lead metal particles. The molten metal lead material may be introduced to the reaction zone in a laminar flow or as atomized molten particles. The weight ratio of formed solid lead oxide particles to solid lead metal particles may be less than 99:1.

According to one or more embodiments presently described, metal-containing particles may be formed by a method including forming a molten material from a solid supply material, introducing the molten material into a reaction zone of a Barton reactor, and contacting the molten material with a processing gas in the reaction zone to form solid metal-containing particles comprising solid metallic particles and solid metal oxide particles. The Barton reactor may include a reaction vessel which may include a top cover and sidewalls defining the reaction zone, an agitator, a processing gas inlet, and a product outlet. The molten material may be introduced to the reaction zone in a laminar flow or as atomized molten particles. Less than 99% of the particles may include metal oxide.

According to one or more embodiments presently described, metal-containing particles may be formed by a method including forming a molten material from a solid supply material, introducing the molten material into a reaction zone of a Barton reactor, and contacting the molten material with a processing gas in the reaction zone to form solid metal-containing particles comprising solid metallic particles and solid metal oxide particles. The Barton reactor may include a reaction vessel which may include a top cover and sidewalls defining the reaction zone, an agitator, a processing gas inlet, and a product outlet. The molten material may be introduced to the reaction zone in a laminar flow or as atomized molten particles. Less than 99% of the particles may include metal oxide.

According to one or more embodiments presently described, metal-containing particles may be made by a method that includes introducing a molten material into a reaction zone of a reactor system, passing a process gas into the reaction zone in a direction substantially tangential to a sidewall of the reaction zone, and contacting the process gas with the molten material in the reaction zone to form metal-containing particles. The molten material may be introduced into an upper portion of the reaction zone The reaction zone may include a substantially circular cross-section, and the molten metal may be introduced into the reaction zone in a laminar flow or as atomized particles.

According to one or more embodiments presently described, metal-containing particles may be made by a method that includes introducing a molten material into a reaction zone of a reactor system, passing a process gas into the reaction zone in a direction substantially tangential to a sidewall of the reaction zone, and contacting the process gas with the molten material in the reaction zone to form metal-containing particles. The molten material may be introduced into an upper portion of the reaction zone The reaction zone may include a substantially circular cross-section, and the molten metal may be introduced into the reaction zone in a laminar flow or as atomized particles.