B01J13/185

Methods of Making Capsules

A method of making a population of capsules, the capsules can include a core including a benefit agent and a shell surrounding the core, wherein the shell can include a first shell component.

Methods of Making Polymeric Capsules
20200330952 · 2020-10-22 ·

A method for making capsules having a core surrounded by a polymeric shell can include dispersing droplets of a disperse-phase in a continuous phase by passing the disperse phase through a plurality of holes in a membrane, from a first side of the membrane to a second side of the membrane and into the continuous phase, while the continuous phase is flowed across the second side of the membrane and the membrane is mechanically moved. The disperse phase can include a polymer precursor, an anti-solvent, and a benefit agent, and the continuous phase includes water. The method can further include admixing the dispersion of droplets of disperse phase in the continuous phase under conditions sufficient to initiate polymerization of the polymer precursor within the droplets of disperse phase and polymerizing the polymer precursor to form the shell.

Microcapsule Clusters
20200316551 · 2020-10-08 · ·

The present invention teaches a composition and process for irreversibly agglomerated charge stable core shell microcapsules, each microcapsule containing a benefit agent core material, which may be the same or different, the polymeric all or walls comprising one or more (meth)acrylate polymers, or optionally combinations with other polymers, along with a polyvalent cation. The capsules of the invention adhere better to surfaces, are more stable and are useful for delivery of benefit agents.

Method for continuously manufacturing an aerogel powder having a hydrophobic-hydrophilic bipolar core-shell structure

A method for producing an aerogel granule having a hydrophobic-hydrophilic bipolar core-shell structure combines an aerogel precursor having a hydrophilic structure with another aerogel precursor having a hydrophobic structure. The method comprises the steps of: mixing a hydrophilic alkoxysilane compound, a hydrophobic alkyl-substituted alkoxysilane compound, and an organic solvent to form a mixture; adding an acidic catalyst to the mixture to perform hydrolysis; adding a basic catalyst to the hydrolyzed mixture to perform condensation, and during the condensation adding a dispersion solvent to the hydrolyzed mixture and stirring the hydrolyzed mixture to gelate so as to form the aerogel granule having a hydrophobic-hydrophilic bipolar core-shell structure.

Hollow resin particles and application thereof

Hollow resin particles, a production process for producing the same and application thereof. The hollow resin particles include a thermoplastic resin shell and a hollow part surrounded by the shell. The thermoplastic resin is a polymer produced from a polymerizable component containing 0.6 to 3.0 wt % of a crosslinkable monomer having at least two polymerizable carbon-carbon double bonds per molecule and 97 to 99.4 wt % of an uncrosslinkable monomer having one polymerizable carbon-carbon double bond per molecule. A blowing agent is encapsulated in the hollow resin particles. The blowing agent contains 50 to 100 wt % of an organic compound having a vapor pressure higher than 100 kPa at 25 C. Further, the encapsulation ratio of the blowing agent ranges from 3 to 13 wt % of the hollow resin particles.

Method for producing colloidosome microcapsules

This invention relates to a process for colloidosome-type microcapsules elaboration from solid particles microcapsules obtained by ionic gelation. In the process, an (O/W) type emulsion is initially generated stabilized with the solid particles microcapsules, and then the particles are fixed to the interface by adsorption of polyelectrolytes, cross-linking, heat treatment or fatty coating, generating the colloidosome with the water-insoluble phase encapsulated in the core and covered by the shell particles.

FOAM MOLDING MASTERBATCH, AND MOLDED FOAM ARTICLE
20200262996 · 2020-08-20 · ·

The present invention aims to provide a masterbatch for foam molding which can be suitably used in molding involving high shear force or molding requiring low molding temperature and which can provide a foam molded article having a high expansion ratio and good appearance quality. The present invention also aims to provide a foam molded article formed from the masterbatch for foam molding. Provided is a masterbatch for foam molding, containing: a base resin; and a thermally expandable microcapsule, the masterbatch having a true specific gravity of 0.80 g/cm.sup.3 or more and a Mooney viscosity ML 1+4 (100 C.) of 20 to 90, the base resin containing an EPDM resin, the masterbatch containing the thermally expandable microcapsule in an amount of 40 to 300 parts by weight relative to 100 parts by weight of the base resin.

METHOD FOR PRODUCING CAPSULES COMPRISING AT LEAST ONE WATER-SOLUBLE OR HYDROPHILIC SUBSTANCE, AND RESULTING CAPSULES
20200246226 · 2020-08-06 ·

The present invention relates to a method for preparing solid microcapsules that comprises of the following steps: a) the preparation of a composition C1, comprising at least one water-soluble or hydrophilic substance dispersed in a hydrophobic phase; b) the addition, under stirring, of the said composition C1 in a polymeric composition C2, the compositions C1 and C2 being immiscible with each other, whereby an emulsion (E1) is obtained; c) the addition, under stirring, of the emulsion (E1) in a composition C3, the compositions C2 and C3 being immiscible with each other, whereby a double emulsion (E2) is obtained; d) the application of a shear to the emulsion (E2), whereby a double emulsion (E3) is obtained; and e) the polymerisation of the composition C2, whereby solid microcapsules dispersed in the composition C3 are obtained.

High-ultraviolet absorption lignin/chemical sun-screening agent microcapsule and preparation method therefor

The present invention, belonging to the technical field of chemical sun-screening agent preparation, discloses a high-ultraviolet absorption lignin/chemical sun-screening agent microcapsule using lignin as a wall material and a preparation method therefor. The method of the present invention comprises the following steps: (1) dissolving 1-20 parts by weight of lignin in 100-200 parts by weight of an aqueous solution with a pH of 12, adjusting the pH of the solution to 7-10, and then removing insoluble substances by filtration to obtain a lignin solution; and (2) mixing 10-50 parts by weight of the lignin solution in step (1) with 1-10 parts by weight of a chemical sun-screening agent, and performing ultrasonic radiation under a power of 200-1500 W for 10 s to 25 min to obtain a lignin/chemical sun-screening agent microcapsule emulsion. The lignin/chemical sun-screening agent microcapsule of the present invention has excellent ultraviolet absorption performance, can avoid photodegradation of the chemical sun-screening agent, and has good stability; and it effectively prevents the chemical sun-screening agent from directly contacting and hurting the skin, having great application prospects in the field of sun-screening skincare products.

MASTER BATCH FOR EXPANSION MOLDING AND FOAM MOLDED BODY
20200231763 · 2020-07-23 · ·

The present invention aims to provide a masterbatch for foam molding which can be suitably used in molding involving high shear force or molding requiring low molding temperature and which can provide a foam molded article having a high expansion ratio and good appearance quality. The present invention also aims to provide a foam molded article formed from the masterbatch for foam molding. Provided is a masterbatch for foam molding, containing: a base resin; and a thermally expandable microcapsule, the masterbatch having a true specific gravity of 0.80 g/cm.sup.3 or more, the base resin containing an olefin elastomer, the masterbatch containing the thermally expandable microcapsule in an amount of 40 to 300 parts by weight relative to 100 parts by weight of the base resin.