B01J2219/00058

On-Demand Rapid Synthesis of Lomustine Under Continuous Flow Conditions

Disclosed herein is a continuous manufacturing process for lomustine that has a short residence time and 63 percent yield. Major advantages of this process are that the total production cost for lomustine is lower, the product is higher quality, and the manufacturing operation is safer for production personnel.

Reactor for Hydrothermal Growth of Structured Materials
20200070114 · 2020-03-05 ·

Design, fabrication, and usage of a reactor are presented for synthesis of structured materials from a liquid-phase precursor by heating. The structured materials are particles, membranes or films of micro-porous molecular sieve crystals such as zeolite and meso-porous materials. The precursor solution and structured materials in the reactor are uniformly heated by a planar heater with characteristic heat transfer dimension in the range of 3 mm to 10 cm. A planar heater having width and length at least three times of the characteristic heat transfer dimension provides at least one surface of uniform temperature distribution for heating purposes. Heating is conducted over a temperature range of 20 to 300 C. The planar heater can be heated by electrical power of by thermal fluid.

SYSTEM TO CONVERT CELLULOSIC MATERIALS INTO SUGAR AND METHOD OF USING THE SAME
20200030764 · 2020-01-30 ·

A system configured to convert cellulosic materials to sugar is provided. The system has a housing a plurality of sensors coupled to the housing configured to receive input from an internal section of the housing, and convert the input to data during operation, and a control system comprising a processor, the control system configured to configured to adjust a parameter of the housing based on the received data, wherein the received data comprises an amount of oxygen within the housing, and if the oxygen in the housing is outside a predetermined range, the control system outputs a signal to an outlet to release a predetermined amount of oxygen.

Thin-film treatment apparatus
10532292 · 2020-01-14 · ·

A thin-film treatment apparatus for treating viscous material, including a housing, having a heatable and/or coolable housing casing, which encloses a rotationally symmetric treatment chamber extending in the axial direction, an inlet port, arranged in an inlet region of the housing, for feeding the material to be treated into the treatment chamber, an outlet port, arranged in an outlet region of the housings, for discharging the material from the treatment chamber, and a coaxially extending, drivable rotor shaft, arranged in the treatment chamber, for producing a material film on the inner face of the housing casing and for conveying the material in the direction from the inlet region toward the outlet region, the rotor shaft including a central rotor shaft body and rotor blades arranged on the circumference thereof, the radially outermost end of which rotor blades is distanced from the inner face of the housing casing.

Double shaft reactor/mixer and system including an end cap for a reactor/mixer and a discharge screw connector block
10525378 · 2020-01-07 · ·

An at least two shaft reactor/mixer, in particular for process engineering treatment of highly viscose, elastic and/or solid containing reaction substance and mixture, in which at the housing inner wall inwardly directed static mixing elements are arranged, which interact with scrapers of the at least two shafts in such a way, that in the area of the spaces between the scrapers the static mixing elements and the housing inner wall sheer forces, in particular a flow disturbance, are generated in an enhanced manner. In addition, there is a system including an end cap for a one or multiple shaft reactor/mixer and a discharge screw connector block being connectable with the end cap in a detachable manner.

Processes and apparatuses for operating a hydrocarbon conversion zone

Processes and apparatus for reforming hydrocarbons to reduce the impact of contaminants created by non-catalyst coking. The reaction zone receives sulfur to inhibit the impact, and a control index is used to control the determine conditions with generally lower pressures. Additionally, a compression zone, pressure control zone and combustion zone operation are provided for the operation of the reaction zone at the generally lower pressures.

PLASMA REACTOR AND METHOD OF OPERATING A PLASMA REACTOR
20190381475 · 2019-12-19 ·

The problem addressed by the invention is that of providing a plasma reactor for decomposition of hydrocarbons which allows stable operation over a prolonged time period. This problem is solved by a plasma reactor for decomposing a hydrocarbon fluid, which comprises a reactor chamber surrounded by a reactor wall and further comprises at least one hydrocarbon inlet and an outlet. A plasma torch having at least two electrodes, which comprise a base part at a first end, is fixed to the reactor wall. At a second end, the electrodes comprise a burner part which projects into the reactor chamber, and a plasma zone is defined between the burner parts of adjacent electrodes. In a region between the plasma zone and the outlet, the hydrocarbon inlet opens into the reactor chamber, and the hydrocarbon inlet is oriented toward the plasma zone such that hydrocarbon fluid flowing therefrom is directed towards the plasma zone. In the plasma reactor disclosed herein, primarily small C particles are formed which prevent fouling or overgrowing of the reactor chamber. Furthermore some large and heavy C particles, which may statistically be formed, penetrate the plasma cloud and can attach specifically to the electrodes.

PHOTOREACTOR FOR PHOTOCATALYSIS, RELATED SYSTEMS, AND RELATED METHODS
20240091732 · 2024-03-21 ·

The disclosure relates to a photoreactor for performing photocatalytic reactions with a particulate photocatalyst loaded in the reactor. The photoreactor includes an internal wall having an outer surface and defining an interior volume, and a transparent external wall having an outer surface and an opposing inner surface. The internal and external walls are spaced apart so that they together define a reaction volume between the walls. The photoreactor further includes an external light transmission apparatus, such as a light source and/or a light guide, positioned around the external wall and being adapted to transmit light through the external and into the reaction volume. When a particulate photocatalyst loaded in the reaction volume is irradiated by external light transmission apparatus while a reactant is flowing through the reaction volume, a photocatalytic reaction can be performed to form a desired reaction product.

Methods and Systems for Cracking Hydrocarbons

The present disclosure relates to processes, methods, systems, and apparatus for steam cracking hydrocarbon in a pyrolysis furnace having a convection zone and a radiant zone. The convection zone includes three heat exchangers in series with a serpentine arrangement. A fluid source is disposed each heat exchanger to provide steam into the heat exchangers. The present disclosure further relates to a process of adjusting the stream flow rate for each fluid source to control operating conditions such as flue gas temperature, stack temperatures, and temperatures of other components of the furnace.

Method for evaluating lifting force in a heat exchanger

A method and a control unit for evaluating lifting force of a gas phase of a substantially vertical upward two-phase flow of a first fluid in a heat exchanger. The first fluid comprises the gas phase and a liquid phase. The method comprises determining that the lifting force of the gas phase is insufficient for lifting the liquid phase based on hot end approach of the heat exchanger and/or on pressure drop of the first fluid over the heat exchanger. The control unit is configured to determine that the lifting force of the gas phase is insufficient for lifting the liquid phase based on hot end approach of the heat exchanger and/or on pressure drop of the first fluid over the heat exchanger. A heat exchanger assembly comprising a heat exchanger and the control unit.