The present disclosure relates to a process for preparing polymers using a plug flow reactor. The process includes providing an aqueous monomer solution comprising amide monomers; evaporating the aqueous monomer solution to form a concentrated monomer solution; and polymerizing the concentrated monomer solution in a plug flow reactor comprising a shell side and a tube side to form a first process fluid comprising polymers. The concentrated monomer solution flows on the shell side from the inlet to the outlet.

A device for carrying out a chemical reaction by a continuous method has a reactor with at least two reactor sections which define a direction of flow. The reactor has plug flow properties along the direction of flow. A recirculation line is present to withdraw a partial flow from the reactor at a first point and return it to the reactor at a second point located above the first point in the direction of flow. Means are provided which prevent a temperature increase in the reactor over a predetermined temperature range, for example change of more than approximately 50 K.

A reactor includes: a heat exchange section including: a first flow channel configured to flow a reaction fluid and a second flow channel configured to flow a heat medium; an introduction path for a temperature sensor, extending from an insertion opening provided on a side surface of the heat exchange section to the first flow channel or the second flow channel; a pipe for a temperature sensor, connected to a side surface of the heat exchange section and communicating with the introduction path through the insertion opening; and a jig provided in the pipe. The jig is provided with a guide hole extending from the base end toward the tip end and opened toward the insertion opening of the introduction path. The guide hole is provided with a tapered hole directed from the base end toward the tip end.

The present disclosure relates to a process for preparing polymers using a plug flow reactor. The process includes providing an aqueous monomer solution comprising amide monomers; evaporating the aqueous monomer solution to form a concentrated monomer solution; and polymerizing the concentrated monomer solution in a plug flow reactor comprising a shell side and a tube side to form a first process fluid comprising polymers. The concentrated monomer solution flows on the shell side from the inlet to the outlet.

A system and method for producing dimethyl ether (DME) via dry reforming and DME synthesis in the same vessel, including converting methane and carbon dioxide in the vessel into syngas (including hydrogen and carbon monoxide) via dry reforming in the vessel, cooling the syngas via a heat exchanger in the vessel, and synthesizing DME from the syngas in the vessel.

The present invention relates to a cascade process useful for (fast) ionic polymerisation of liquid monomer(s) containing reaction mixture for the production of the corresponding polymer(s).

The present invention relates to processes and apparatus useful for (fast) ionic polymerisation of liquid monomer(s) containing reaction mixture for the production of the corresponding polymer(s).

Reduced tube pitch within a shell-and-tube heat exchange reactor such as, for example, an EO reactor, is provided by utilizing a welding material that has a high tensile (i.e., a tensile strength of greater than 600 MPa). Reduced tube pitch allows for more elongated tubes (the tubes are filled with a catalyst) to be present in a reactor, and thus a smaller reactor can be manufactured. Notably, the use of a high tensile strength welding material allows the implementation of a small welding groove located between a beveled sidewall of a beveled upper portion of an opening provided in a tube sheet overlay material (that is located atop a tube sheet) and an outermost sidewall of the elongated tube passing through the opening in the tube sheet overlay material.

Processes for controlling the rate and temperature of cooling fluid through a heat exchange zone in, for example, an alkylation reactor using an ionic liquid catalyst. A cooling fluid system may be used to provide the cooling fluid which includes a chiller and a reservoir. The cooling fluid may pass from the reservoir through the heat exchange zone. A bypass line may be used to pass a portion of the cooling fluid around the heat exchange zone. The amount of cooling fluid may be adjusted, with a valve, based upon the temperature of the cooled process fluid flowing out of the heat exchange zone. Some of the cooling fluid from the chiller may be circulated back to the chiller in a chiller loop.

Design, fabrication, and usage of a reactor are presented for synthesis of structured materials from a liquid-phase precursor by heating. The structured materials are particles, membranes or films of micro-porous molecular sieve crystals such as zeolite and meso-porous materials. The precursor solution and structured materials in the reactor are uniformly heated by a planar heater with characteristic heat transfer dimension in the range of 3 mm to 10 cm. A planar heater having width and length at least three times of the characteristic heat transfer dimension provides at least one surface of uniform temperature distribution for heating purposes. Heating is conducted over a temperature range of 20 to 300 C. The planar heater can be heated by electrical power of by thermal fluid.