The invention relates to a method for the preparation of a homogenized tobacco material, said method comprising: —pulping and refining cellulose fibres to obtain fibres having a mean size per weight comprised between about 0.2 millimetres and about 4 millimetres; —grinding a blend of tobacco of one or more tobacco types to tobacco particles having a mean size per weight comprised between about 0.03 millimetres and about 0.12 millimetres; —Combining the cellulose fibres with the tobacco particles and with a binder to form a slurry; —homogenizing the slurry; —adding asparaginase to the slurry; and—forming the homogenized tobacco material from the slurry, wherein the homogenized tobacco material comprises from about 1 percent and about 5 percent in dry weight basis of the binder.

Embodiments described herein include a method of making a tobacco extract comprising; (a) contacting tobacco with an extraction solvent such that tobacco components are extracted from the tobacco into the solvent, wherein the extraction solvent comprises a supercritical fluid; (b) separating the residual tobacco solids from the supercritical extraction solvent containing tobacco components; (c) exposing the extraction solvent containing tobacco components to conditions in a vessel at which the extraction solvent is subcritical, thereby releasing the tobacco components from the extraction solvent; and then (d) washing the vessel with an entrapment solvent which dissolves the tobacco components, wherein the entrapment solvent comprises an aerosol generating agent.

Embodiments described herein include a method of making a tobacco extract comprising; (a) contacting tobacco with an extraction solvent such that tobacco components are extracted from the tobacco into the solvent, wherein the extraction solvent comprises a supercritical fluid; (b) separating the residual tobacco solids from the supercritical extraction solvent containing tobacco components; (c) exposing the extraction solvent containing tobacco components to conditions in a vessel at which the extraction solvent is subcritical, thereby releasing the tobacco components from the extraction solvent; and then (d) washing the vessel with an entrapment solvent which dissolves the tobacco components, wherein the entrapment solvent comprises an aerosol generating agent.

The present invention relates to a process to obtain tobacco flavor extracts, the process comprising: —conditioning a mixture of tobaccos in a primary tobacco manufacture heating the mixture of tobacco to a temperature comprised between about 30 degrees Celsius and about 90 degrees Celsius for a time interval comprised between about 30 seconds and about 1 hour; —recovering emissions produced by the mixture conditioning; and —obtaining at least one flavor extract from the recovered emissions. The present invention also relates to an apparatus to obtain tobacco flavor extracts.

The present invention relates to a process to obtain tobacco flavor extracts, the process comprising: —conditioning a mixture of tobaccos in a primary tobacco manufacture heating the mixture of tobacco to a temperature comprised between about 30 degrees Celsius and about 90 degrees Celsius for a time interval comprised between about 30 seconds and about 1 hour; —recovering emissions produced by the mixture conditioning; and —obtaining at least one flavor extract from the recovered emissions. The present invention also relates to an apparatus to obtain tobacco flavor extracts.

A method for increasing bulkiness of reconstituted tobacco by adding tobacco stem particles includes (1) pulverizing a first portion of tobacco stems to obtain tobacco stem particles; (2) classifying the tobacco stem particles with mesh sieves and selecting the tobacco stem particles with a predetermined mesh size; (3) extracting a second portion of the tobacco stems with water and grinding to form a tobacco stem slurry that has a beating degree of 12-14° SR, and mixing the tobacco stem slurry with tobacco leaves in a weight ratio of 6:4 and grinding to obtaining a tobacco slurry that has a beating degree of 18-20° SR; (4) cutting plant fiber pulp boards and dispersing in water to form a plant fiber pulp; (5) preparing a filler solution that contains 10 wt % of a mineral filler; (6) mixing, rolling and drying to obtain the reconstituted tobacco.

A method for increasing bulkiness of reconstituted tobacco by adding tobacco stem particles includes (1) pulverizing a first portion of tobacco stems to obtain tobacco stem particles; (2) classifying the tobacco stem particles with mesh sieves and selecting the tobacco stem particles with a predetermined mesh size; (3) extracting a second portion of the tobacco stems with water and grinding to form a tobacco stem slurry that has a beating degree of 12-14° SR, and mixing the tobacco stem slurry with tobacco leaves in a weight ratio of 6:4 and grinding to obtaining a tobacco slurry that has a beating degree of 18-20° SR; (4) cutting plant fiber pulp boards and dispersing in water to form a plant fiber pulp; (5) preparing a filler solution that contains 10 wt % of a mineral filler; (6) mixing, rolling and drying to obtain the reconstituted tobacco.

The disclosure provides liquid compositions configured for oral use, the liquid composition comprising water in an amount of about 40% by weight or higher, based on total weight of the composition, a flavoring agent or an active ingredient or both a flavoring agent and an active ingredient, and one or more additional components selected from the group consisting of sweeteners, humectants, and alkali metal salts, wherein the composition has a water activity (Aw) of about 0.85 or lower. The liquid compositions are generally suitable for spraying into the oral cavity.

The disclosure provides a composition including a filler, a lipid having a melting point of about 29° C. or above, water, and a flavoring agent or an active ingredient or both a flavoring agent and an active ingredient, which is optionally substantially free of isomalt and substantially free of tobacco material, excluding any nicotine component present, based on the total weight of the composition. The disclosure also provides compositions including a filler, a lipid having a melting point of about 29° C. or above, water in an amount of at least about 15% by weight, based on total weight of the composition, and a flavoring agent or an active ingredient or both a flavoring agent and an active ingredient.

The disclosure provides for an oral composition comprising a gel. The gel may be formed of a long chain carbohydrate, such as an alginate, that is crosslinked with a suitable crosslinking agent. Other material, such as fillers, active ingredients, flavor components, and the like may be included in the gel or otherwise combined with the gel to form an oral product. The disclosure further provides methods of preparing oral compositions.