Patent classifications
B01D15/185
METHOD FOR PURIFYING ALLULOSE CONVERSION REACTION PRODUCT
The present invention relates to a method of purifying allulose and a method of preparing allulose using the method of purifying, and more specifically the purification method includes mixing allulose conversion product with powdered activated carbon and applying the solid-liquid separation to efficiently remove impurities.
Process for purification of neutral human milk oligosaccharide using simulated moving bed chromatography
The present application discloses a process for the purification of a neutral human milk oligosaccharide (neutral HMO). The process uses simulated moving bed (SMB) chromatography which allows the continuous purification of large quantities of HMOs with high purity. Contrary to chemical synthesis routes of neutral HMOs, and their subsequent purification, the presented process allows the provision of HMOs free of noxious chemicals, such as e.g. trace amounts of heavy metals or organic solvents. The individual neutral HMO product may be obtained in solid form by spray drying or as a concentrated syrup. The provided neutral HMO is very well-suited for use in food applications.
PROCESS FOR PURIFICATION OF NEUTRAL HUMAN MILK OLIGOSACCHARIDE USING SIMULATED MOVING BED CHROMATOGRAPHY
The present application discloses a process for the purification of a neutral human milk oligosaccharide (neutral HMO). The process uses simulated moving bed (SMB) chromatography which allows the continuous purification of large quantities of HMOs with high purity. Contrary to chemical synthesis routes of neutral HMOs, and their subsequent purification, the presented process allows the provision of HMOs free of noxious chemicals, such as e.g. trace amounts of heavy metals or organic solvents. The individual neutral HMO product may be obtained in solid form by spray drying or as a concentrated syrup. The provided neutral HMO is very well-suited for use in food applications.
Method for chromatographic purification of viscous loads
The invention relates to a method for purifying a mixture to be separated, in a multicolumn chromatography system, the method comprising successively and cyclically: a step of collecting a raffinate, a step of injecting the mixture to be separated, a step of collecting an extract and an eluent injection step, at an operating temperature; wherein the mixture to be separated has a viscosity at 20? C. greater than or equal to 3 mPa.Math.s; and wherein the dry matter mass concentration of the mixture to be separated is equal, within 5%, to a threshold concentration, said threshold concentration is such that: the viscosity of the mixture to be treated at a dry matter mass concentration equal to the threshold concentration and at the operating temperature, is equal to twice the viscosity of the mixture to be treated, at a dry matter mass concentration equal to 85% of the threshold concentration and at the operating temperature.
Process for recovering para-xylene using a metal organic framework adsorbent in a simulated moving-bed process
Para-xylene is separated from a mixture of C8 aromatics using a simulated moving bed (SMB) adsorption process, wherein a MOF is used as an adsorbent and an alkane or alkene having 7 or less carbon atoms, such as hexane or heptane is used as desorbent. Because of the difference in boiling points of a hexane or heptane desorbent as compared to conventional desorbents such as toluene or para-diethylbenzene, less energy is required to separate hexane or heptane from C8 aromatics by distillation than the energy required to separate toluene or diethylbenzene from C8 aromatics by distillation.
Processes for recovering paraxylene
Disclosed is a process for recovering paraxylene in which a first simulated moving bed adsorption unit is used to produce two extract streamsone rich in paraxylene and a paraxylene-rich extract stream that is lean in ethylbenzene and an ethylbenzene-rich extract stream that is lean in paraxylene- and a paraxylene-depleted raffinate stream. A significant amount of the ethylbenzene is removed in the ethylbenzene-rich extract stream (at least enough to limit buildup in the isomerization loop), so the paraxylene-depleted raffinate stream may be isomerized in the liquid phase. Avoiding vapor phase isomerization saves energy and capital, as liquid phase isomerization requires less energy and capital than the vapor phase isomerization process due to the requirement of vaporizing the paraxylene-depleted stream and the use of hydrogen, which requires an energy and capital intensive hydrogen recycle loop.
Process for separation of diamines and/or omega-aminoacids from a feed mixture
The present disclosure relates to methods for separating at least one amine chosen from diamines and omega-aminoacids from a feed mixture using a simulated moving bed (SMB) adsorptive technology.
SIMULATED MOVING BED SEPARATION PROCESS
The process involves the use of two rotary valves to implement Varicol operation of a simulated moving bed apparatus to separate a product from at least one multicomponent feed. In a particular embodiment, paraxylene is separated from a mixture of C8 aromatic hydrocarbons. The use of the Varicol process further enhances the separation of the desired product and provides flexibility with a simulated moving bed apparatus using dual rotary valves.
CONTINUOUS PROCESS FOR PURIFICATION OF STEVIOL GLYCOSIDES FROM STEVIA LEAVES USING SIMULATED MOVING BED CHROMATOGRAPHY
Disclosed is a continuous process for the purification of steviol glycosides extracted from the dried stevia leaves using continuous simulated moving bed processes and nanofiltration without the addition of organic solvents to obtain a purified steviol product comprising sweet steviol glycosides. The sweet steviol glycosides can be used as substitutes for caloric sweeteners in beverages and in other food items.
METHOD FOR PREPARING D-PSICOSE CRYSTAL
A method for producing high purity D-psicose crystals having a purity of 98% (w/w) or more and a grain size of MA200 or more. The method includes: removing impurities from a D-psicose solution to obtain a purified D-psicose solution; concentrating the purified D-psicose solution; cooling the concentrated D-psicose solution to 30 C. to 40 C. through a heat exchanger; seed crystallizing the D-psicose solution at 30 C. to 40 C. to obtain a seed crystallized massecuite; and full-scale crystallizing the seed crystallized massecuite. The method can produce pure D-psicose crystals in a suitable form for industrial application through an economical crystallization process from the D-psicose solution without using organic solvents.