Systems are provided that permit temperature control of a catalyst bed for conversion of alcohols to fuel hydrocarbons by modulating the water content of the alcohol feed stream provided to the catalyst bed. In some embodiments a secondary catalyst bed is provided for the conversion of light hydrocarbons found in the initial hydrocarbon product to fuel hydrocarbons that are liquid at ambient temperature and pressure.

A method of producing carbon nanotubes in a fluidized bed reactor includes preparing a carbon nanotube by supplying a catalyst and a carbon source to an interior of the fluidized bed reactor having an internal pressure of 0.5 barg to 1.2 barg (gauge pressure), thereby improving the yield and purity of carbon nanotubes.

A method of installing a thermocouple in a reactor tube of a tubular reactor, comprising lowering a weighted tow line through a stack of catalyst carriers and using a tow line to pull the thermocouple down the reactor tube through inner channels of the stack of catalyst carriers into a desired installation position.

A continuous slurry-bed tank reactor, comprising a tank reactor body, an agitator, and tubular separation membranes. A method of using the continuous slurry-bed tank reactor comprising adding a catalyst, feeding reactants, stopping feeding the reactants, starting a heating system, changing directions of the reactants flowing through the tubular separation membranes.

An improved reactor comprising a shell and at least one reactor internal component. The reactor internal component includes a tube bundle comprising a plurality of tubes attached by at least one tube support plate comprising at least one radial strut and at least one bracket configured to secure to at least one tube of the tube bundle. The tubes are arranged in concentric bands about a longitudinal axis of the reactor. The reactor comprises a gas inlet plate, a catalyst support plate, and a top plate.

A method for manufacturing solketal ((2,2-Dimethyl-1,3-dioxolan-4-yl)methanol) includes: (1) milling starting reagents, including at least: glycerol, a catalyst selected from a hard Lewis acid including at least one transition metal, and acetone, the molar ratio (glycerol):(acetone) being less than or equal to 0.8; preferably less than or equal to 0.7, at an ambient temperature greater than or equal to 50° C., preferably greater than or equal to 56° C., in a three-dimensional microbead mill in a liquid phase for a residence time less than or equal to 15 minutes, preferably less than or equal to 10 minutes, and in particular less than or equal to 5 minutes; (2) recovering, as output from the mill, a final composition including solketal and, where appropriate, one or more sub-products corresponding to the starting reagents that have not reacted and/or to 1,3-O-isopropylidene-glycerol, and (3) optionally, separating the solketal from the one or more sub-products.

The present disclosure provides methods and apparatuses of producing hydrogen. The methods comprise: (a) contacting a plastic with a catalyst and a gas feed; and (b) applying a microwave at a first temperature. The apparatuses comprise: a reactor for mixing plastic with a catalyst to form a mixture; an inlet for introducing a gas feed; a microwave generator; an optional temperature sensor; and an outlet configured to exhaust the product hydrogen formed in the reactor.

A reactor temperature measurement system includes a Fiber Bragg Grating sensor array arranged in a body of the reactor for monitoring temperatures at multiple positions in an axial direction of the body to obtain temperature sensing optical signals; and a fiber grating demodulator, connected to the Fiber Bragg Grating sensor array, and used to demodulate the temperature sensing optical signals. A method for preparing a Fiber Bragg Grating includes preparing a Fiber Bragg Grating by using a single-mode fiber and annealing the Fiber Bragg Grating, which includes heating the Fiber Bragg Grating to a temperature above 400° C. and maintaining for 100 to 200 hours.

A method of manufacturing lithium-metal nitride including suspending a lithium—metal-oxide-powder (LMOP) within a gaseous mixture, incrementally heating the suspended LMOP to a holding temperature of between 400 and 800 degrees Celsius such that the LMOP reaches the holding temperature, and maintaining the LMOP at the holding temperature for a time period in order for the gaseous mixture and the LMOP to react to form a lithium-metal nitride powder (LMNP).

A methane production system includes: a raw material gas supply part configured to store and supply a raw material gas; a catalyst supply part configured to store and supply a catalyst; a methanation reaction part connected to the raw material gas supply part and the catalyst supply part and configured to generate a reaction gas by performing a methanation reaction using the raw material gas and the catalyst supplied from the raw material gas supply part and the catalyst supply part; a temperature measurement part connected to the methanation reaction part and configured to measure a temperature of the methanation reaction part; a temperature maintaining part connected to the raw material gas supply part; and a raw material gas injection part connected to the raw material gas supply part to receive the raw material gas from the raw material gas supply part.