There is described a method for heating a sample material in a sample holder, the method comprising receiving the sample holder in a heating chamber of a heating system, the sample holder having at least one sample recipient with the sample material therein; dynamically forming an individual mini microwave cavity around the sample recipient; and applying microwaves generated by at least one microwave generator directly to the sample.

An instrument and method for accelerating the solid phase synthesis of peptides are disclosed. The method includes the steps of deprotecting a protected first amino acid linked to a solid phase resin by admixing the protected linked acid with a deprotecting solution in a microwave transparent vessel while irradiating the admixed acid and solution with microwaves, activating a second amino acid, coupling the second amino acid to the first acid while irradiating the composition in the same vessel with microwaves, and cleaving the linked peptide from the solid phase resin by admixing the linked peptide with a cleaving composition in the same vessel while irradiating the composition with microwaves.

A stirrer includes a magnetic bar and a microwave absorbing layer around the magnetic bar. The stirrer absorbs a microwave and converts the microwave to thermal energy to heat the mixed solution reactant.

An industrial microwave ultrasonic reactor has an inner wall liner. A microwave generation device is formed by microwave units distributed on an outer sidewall, or by a microwave pipe disposed outside the reactor and microwave units distributed on the microwave pipe. One end of the microwave pipe communicates with the bottom of the reactor via a connection pipe I, and the other end communicates with the top via a return pipe. A shield is disposed outside the microwave generation device to separate the microwave units from the outside, and a heat removal device is disposed outside the shield. An ultrasonic wave generation device is formed by 10 to 30 sets of ultrasonic pulse units disposed at intervals along the outer sidewall. Each set has 10 to 50 members distributed along the circumferential direction of the reactor. A stirring shaft is fixed below a stirring motor and extends into the reactor.

Disclosed is a microwave irradiating and heating device including a reaction furnace (1) for containing a sample material to be irradiated with microwave and to be heated, a lid (2) provided for the reaction furnace (1) and having a single hole (21), a microwave irradiating source (3) for emitting a microwave, the microwave irradiating source (3) being disposed outside the reaction furnace, and a rotated quadric surface mirror (4) for reflecting the microwave emitted from the microwave irradiating source (3) into the reaction furnace (1) through the hole (21) of the lid (2), the rotated quadric surface mirror (4) being disposed above the reaction furnace (1).

A method for conversion of greenhouse gases comprises: introducing a flow of a dehumidified gaseous source of carbon dioxide into a reaction vessel; introducing a flow of a dehumidified gaseous source of methane into the reaction vessel; and irradiating catalytic material in the reaction vessel with microwave energy. The irradiated catalytic material is heated and catalyzes an endothermic reaction of carbon dioxide and methane that produces hydrogen and carbon monoxide. At least a portion of heat required to maintain a temperature within the reaction vessel is supplied by the microwave energy. If desired, a mixture that includes carbon monoxide and hydrogen can flow out of the reaction vessel and be introduced into a second reaction vessel to undergo catalyzed reactions producing multiple-carbon reaction products.

A reaction chamber contains catalytic material(s). Tunable microwave source(s) each emit microwave radiation at corresponding time-varying microwave frequency(ies) or at simultaneous multiple different microwave frequencies. Microwave transmission element(s) irradiate the interior volume of the reaction chamber with the microwave radiation, emitted by the microwave source(s), that propagates along the transmission element(s) into the reaction chamber. The reaction chamber is characterized by a maximum temperature variation of a fixed-frequency, steady-state temperature spatial profile that results from irradiation of the reaction chamber by microwave radiation at a substantially fixed microwave frequency and at a reference microwave power level. Irradiation of the reaction chamber at the reference microwave power level by the microwave radiation with the time-varying microwave frequency(ies), or the simultaneous multiple different microwave frequencies, results in a multi-frequency temperature spatial profile having a maximum temperature variation less than the maximum temperature variation of the fixed-frequency, steady-state temperature spatial profile.

A chemical reaction method having steps of preparing a chemical reaction apparatus by partitioning an inside of a horizontal flow reactor into multiple chambers by multiple partition plates, and flowing a liquid horizontally with an unfilled space being provided thereabove, generating microwaves with a microwave generator, and transmiting the microwaves, with at least one waveguide, to the unfilled space in the reactor. Also forming a top portion of the partition plates act as a weir, inclining the reactor such that, in each of the chambers, a weir height on the inlet side is higher than a weir height on the outlet side by at least an overflow depth at the partition plate on the outlet side, flowing content over each of the partition plates inside the reactor, and configuring the weir heights of the partition plates in the reactor are the same in a state where the reactor is not inclined.

An instrument and method for high pressure microwave assisted chemistry are disclosed. The method includes the steps of applying microwave radiation to a sample in a sealed vessel while measuring the temperature of the sample and measuring the pressure generated inside the vessel and until the measured pressure reaches a designated set point, opening the vessel to release gases until the pressure inside the vessel reaches a lower designated set point, closing the vessel, and repeating the steps of opening the vessel at designated pressure set points and closing the vessel at designated pressure set points to the sample until the sample reaction reaches a designated high temperature. The designated set points can controllably differ from one another as the reaction proceeds. Microwave energy can be applied continuously or intermittently during the opening and closing steps. The apparatus includes a microwave cavity, a microwave transparent pressure resistant reaction vessel in the cavity, a cap on the reaction vessel, a pressure sensor for measuring pressure in the vessel, a temperature sensor, and means for opening and closing the cap at predetermined pressure set points measured by the pressure sensor to release pressure from the vessel.

A system for processing hydrocarbon materials, comprising a hydrocarbon feedstock source; a process gas source; a waveguide; and a reaction tube structure. The process gas source comprises one or more sources of gases selected from the group consisting of helium, argon, krypton, neon, xenon, methane, propane, butane, ethane, acetylene, propylene, butylene, ethylene, carbon monoxide, carbon dioxide, water vapor, hydrogen, and nitrogen. The waveguide comprises a lateral portion comprising housing having a first end portion configured to be connected to a microwave generator, a closed opposite end portion, a primary axis extending from the first end portion to the second end portion, and a central portion having an opening, wherein the central portion has a depth that is smaller than a corresponding depth of the first end portion and the second end portion, and a coaxial portion having a first end portion connected to the opening and a lateral dimension that is perpendicular to the primary axis. The reaction tube structure comprises an outer wall made of a dielectric material, and is configured such that when hydrocarbon feedstock from the feedstock source and process gas from the process gas source are fed into the reaction tube structure and microwaves are received in the waveguide, one or more surface waves are propagated in the reaction tube structure to form a plasma within the reaction tube structure and cause the feedstock and process gas to react and form into a product stream, and wherein the reaction tube structure has a lateral dimension that is perpendicular to the lateral portion and parallel to the coaxial portion, and the reaction tube structure is connected to a second end of the coaxial portion.