C01F5/40

Device and method for making a hollow tube of micron-sized crystalline magnesium sulfate

A device for creating hollow tubes of crystalline magnesium sulphate sized a micron pertains to the production technology for inorganic micron-scale materials. The device consist of two halogenation tanks, a solar collector, a temperature-controlled crystallization chamber, a centrifuge, a conveyor belt, and a dryer. The solar collector is connected to a heat pipe at the bottom of a brine pool to form a circulation path. Said method is to convert high magnesium brine into saturated brine with a Mg.sup.2+:Na.sup.+ mass ratio between (8?15):1 by a brine blending operation at a temperature of 60? C.?90? C. it is controlled to be cooled and crystallized at a cooling rate of 0.6?2.0? C./min, solid-liquid centrifugal separation is carried out when it is cooled down to 40?48.5? C., and the solid phase is dried at a temperature of 48.5?70? C., and finally micron-sized crystalline magnesium sulfate hollow tubes are obtained.

MAGNESIUM REMOVAL PROCESS

A method for removing alkali earth metals from a filtrate including a first crystallization step and a second crystallization step, wherein the first crystallization step is a forced circulation crystallizer, and wherein the second crystallization step is a draft tube crystallizer. Also included is a method for reducing magnesium in a chemical liquor including crystallizing magnesium into a magnesium sulfate hydrate in a first crystallization step and precipitating magnesium via addition of a caustic material in a chemical precipitation step.

MAGNESIUM REMOVAL PROCESS

A method for removing alkali earth metals from a filtrate including a first crystallization step and a second crystallization step, wherein the first crystallization step is a forced circulation crystallizer, and wherein the second crystallization step is a draft tube crystallizer. Also included is a method for reducing magnesium in a chemical liquor including crystallizing magnesium into a magnesium sulfate hydrate in a first crystallization step and precipitating magnesium via addition of a caustic material in a chemical precipitation step.

IMPROVED METHODS OF EXTRACTION OF PRODUCTS FROM TITANIUM-BEARING MINERALS

The invention relates to processes for the extraction of products from titanium-bearing minerals. In particular embodiments the invention relates to methods of recycling sulphuric acid used in a titanium dioxide extraction process. The invention also relates to methods for minimising chromophore contamination in calcined titanium dioxide. The process may also comprise steps for removing contaminants from recycled acid or desirable products.

IMPROVED METHODS OF EXTRACTION OF PRODUCTS FROM TITANIUM-BEARING MINERALS

The invention relates to processes for the extraction of products from titanium-bearing minerals. In particular embodiments the invention relates to methods of recycling sulphuric acid used in a titanium dioxide extraction process. The invention also relates to methods for minimising chromophore contamination in calcined titanium dioxide. The process may also comprise steps for removing contaminants from recycled acid or desirable products.

PRE-TREATMENT AGENT AND PRE-TREATMENT METHOD FOR ANTITHROMBIN III TO BE SUBJECTED TO LIMULUS TEST
20190025309 · 2019-01-24 · ·

To provide means for reducing reaction interference observed when AT III is subjected to limulus test, whereby the limulus test of antithrombin III can be carried out at high accuracy. Reaction interference observed when AT III is subjected to limulus test can be reduced by subjecting AT III to a protein inactivation treatment in the co-presence of a divalent metal salt.

PRE-TREATMENT AGENT AND PRE-TREATMENT METHOD FOR ANTITHROMBIN III TO BE SUBJECTED TO LIMULUS TEST
20190025309 · 2019-01-24 · ·

To provide means for reducing reaction interference observed when AT III is subjected to limulus test, whereby the limulus test of antithrombin III can be carried out at high accuracy. Reaction interference observed when AT III is subjected to limulus test can be reduced by subjecting AT III to a protein inactivation treatment in the co-presence of a divalent metal salt.

POTASSIUM MAGNESIUM FERTILIZER
20180339949 · 2018-11-29 ·

A method for producing a double sulfate of potassium and magnesium by dry mechanical attrition of potassium sulfate and magnesium sulfate hexahydrate, comprising obtaining potassium sulfate by sulfatation of potash to bisulfate of potassium and disproportionation of the bisulfate of potassium to potassium sulfate in a water-methanol solution, and obtaining magnesium sulfate hexahydrate by sonic-assisted partial sulfatation of calcined serpentinic silicate.

Apparatus and method for producing magnesium sulfate from coal-fired boiler flue gas
10131546 · 2018-11-20 ·

The present invention provides an apparatus and a method for producing magnesium sulfate through flue gas desulfurization, and specifically provides an apparatus and a method suitable for producing magnesium sulfate through direct crystallization in a magnesium oxide based desulfurization waste liquid tower of flue gas with a small content of oxygen like a coal fired boiler flue gas. The apparatus includes an oxygenation equipment, a flue gas desulfurization equipment, a seriflux cycling equipment, an evaporation and concentration equipment, a cycling and precipitating equipment, an oxidation equipment, a crystallization equipment, a centrifugation equipment and a drying equipment, etc. The apparatus and method of the present invention can greatly reduce electric power consumption of oxidation fans and steam consumption, as well as guarantee desulfurization efficiency and quality of a magnesium sulfate by-product, reduce lots of operation costs of the magnesium sulfate production system, and reduce desulfurization operation costs.

Apparatus and method for producing magnesium sulfate from coal-fired boiler flue gas
10131546 · 2018-11-20 ·

The present invention provides an apparatus and a method for producing magnesium sulfate through flue gas desulfurization, and specifically provides an apparatus and a method suitable for producing magnesium sulfate through direct crystallization in a magnesium oxide based desulfurization waste liquid tower of flue gas with a small content of oxygen like a coal fired boiler flue gas. The apparatus includes an oxygenation equipment, a flue gas desulfurization equipment, a seriflux cycling equipment, an evaporation and concentration equipment, a cycling and precipitating equipment, an oxidation equipment, a crystallization equipment, a centrifugation equipment and a drying equipment, etc. The apparatus and method of the present invention can greatly reduce electric power consumption of oxidation fans and steam consumption, as well as guarantee desulfurization efficiency and quality of a magnesium sulfate by-product, reduce lots of operation costs of the magnesium sulfate production system, and reduce desulfurization operation costs.