Provided is a method for producing a positive electrode active material for nonaqueous electrolyte secondary batteries, the method including: a mixing step of obtaining a W-containing mixture of Li metal composite oxide particles represented by the formula: Li.sub.zNi.sub.1-x-yCO.sub.xM.sub.yO.sub.2 and composed of primary particles and secondary particles formed by aggregation of the primary particles, 2 mass % or more of water with respect to the oxide particles, and a W compound or a W compound and a Li compound, the W-containing mixture having a molar ratio of the total amount of Li contained in water and the solid W compound or the W compound and the Li compound of 3 to 5 with respect to the amount of W contained therein; and a heat treatment step of heating the W-containing mixture to form lithium tungstate on the surface of the primary particles of the Li metal composite oxide particles.

A preparation method of phosphotungstic acid includes mixing a mixed solution containing tungsten, phosphorus and an inorganic acid with an organic-alcohol-containing oil phase for extraction, stripping the obtained supported organic phase and distilled water according to an oil phase:aqueous phase volume ratio of 3:1 to 10:1 to obtain a stripping solution; and carrying out thermal evaporation crystallization or spray drying on the stripping solution to obtain a phosphotungstic acid crystal, wherein the organic alcohol is a C7-C20 alcohol. The inventors have found out that the addition of an inorganic acid to a solution of phosphorus or tungsten and the use of an organic alcohol as an extractant can achieve simultaneous and efficient extraction of phosphotungstic acid. It has also been found that the organic-alcohol-containing oil phase has excellent selectivity for phosphotungstic acid molecules in the mixed solution.

The present invention relates to a process for preparing ammonium metatungstate using a reverse osmosis cell, and to a device for performing the process according to the invention.

A modified garnet-type solid electrolyte, includes: a garnet-type solid electrolyte; a modification layer, such that the modification layer is formed on at least one side of the garnet-type solid electrolyte, and possesses a three-dimensional crosslinking structure comprising at least one strongly acidic lithium salt and at least one weakly acidic lithium salt. A method of forming a modified garnet-type solid electrolyte, includes: exposing a garnet-type solid electrolyte in air to form a pre-passivation layer; mixing solutions of strong acid and weakly acidic salt to form a mixed solution; chemically treating at least one side of the garnet-type solid electrolyte with the mixed solution; and forming a modification layer on the at least one side of the garnet-type solid electrolyte.

An infrared reflective material, a method for producing the same, and an infrared reflective structure are provided. The method includes a preparation step implemented by mixing antimony and zirconium tungstate through a sol-gel manner to form zirconium tungstate composite powders doped with the antimony; a sintering step implemented by sintering the antimony and the zirconium tungstate in the zirconium tungstate composite powders doped with the antimony in a temperature gradient within a range from 500° C. to 1,100° C. for a predetermined time period, so that the antimony and the zirconium tungstate in the zirconium tungstate composite powders doped with the antimony bond together to form into composite tungsten oxide powders; a grinding step implemented by grinding the composite tungsten oxide powders; and a mixing step implemented by mixing the composite tungsten oxide powders that are grinded into an acrylic resin to form the infrared reflective material.

A method of manufacturing a mixed metal oxide powder is provided. The method includes steps of mixing two or more metal precursors in a solvent to form a dispersion of the metal precursors in the solvent; drying the dispersion to obtain a dried mixed metal precursor powder; jet milling the dried mixed metal precursor powder to obtain particles having a size distribution in a range of 0.2-20 micrometers; and exposing the particles to a hydrocarbon flame or oxygen plasma to provide the mixed metal oxide powder. Mixed metal oxide powders produced by the disclosed methods are also provided.

Provided herein are methods for producing crystalline tungsten bronze oxide particles. The method may include atomizing a liquid solution comprising an alkali metal precursor and a tungsten precursor to produce droplets; mixing the droplets with one or more gaseous flows to produce a combined flow; flowing the combined flow through a heated reactor to provide crystalline tungsten bronze oxide particles having the formula M.sub.xWO.sub.3, wherein M is the alkali metal; and collecting the particles.

An electromagnetic wave absorbing particle dispersoid is provided that includes at least electromagnetic wave absorbing particles and a thermoplastic resin, wherein the electromagnetic wave absorbing particles contain hexagonal tungsten bronze having oxygen deficiency, wherein the tungsten bronze is expressed by a general formula: M.sub.xWO.sub.3-y (where one or more elements M include at least one or more species selected from among K, Rb, and Cs, 0.15≤x≤0.33, and 0<y≤0.46), and wherein oxygen vacancy concentration N.sub.V in the electromagnetic wave absorbing particles is greater than or equal to 4.3×10.sup.14 cm.sup.−3 and less than or equal to 8.0×10.sup.21 cm.sup.−3.

Perovskite structures are disclosed comprising: a first element X which may be barium and/or a lanthanide, strontium, iron, cobalt, oxygen, magnesium and tungsten; the structure comprising a region of single perovskite and a region of double perovskite. Also disclosed are methods for forming such structures, electrodes comprising such structures and solid oxide cells using such structures.

According to one embodiment, provided is a tungsten oxide powder including primary particles having an average particle size of 100 nm or less. Each of the primary particles include a crystal phase and an amorphous phase coexisting in each primary particle.