Patent classifications
C01G51/40
Iron-based oxide magnetic particle powder and method for producing iron-based oxide magnetic particle powder
An e-type iron-based oxide magnetic particle powder has narrow particle size distribution and has a low content of fine particles which do not contribute to magnetic recording characteristics. As a result, a narrow coercive force distribution is achieved and the powder is suitable for increasing recording density of a magnetic recording medium. The powder containing substituting metal elements can be obtained by: adding an alkali to an aqueous solution containing trivalent iron ions and ions of the metals for partially substituting Fe sites to neutralize the aqueous solution to a pH of 1.5 to 2.5; then adding a hydroxycarboxylic acid; further adding the alkali to neutralize the aqueous solution to a pH of 8.0 to 9.0; washing with water a precipitation of an iron oxyhydroxide containing the substituting metal elements produced; and coating the iron oxyhydroxide containing the substituting metal elements with a silicon oxide and heating the resultant.
METHOD FOR PRODUCING OXIDE PARTICLES WITH CONTROLLED COLOR CHARACTERISTICS, OXIDE PARTICLES, AND COATING OR FILM-LIKE COMPOSITION COMPRISING THE SAME
A method for producing oxide particles with controlled color characteristics and to provide oxide particles with controlled color characteristics includes controlling color characteristics of the oxide particles by controlling the ratio of M-OH bonds, the binding of one or more different elements (M) other than oxygen or hydrogen with hydroxyl group (OH), in oxide particles selected from metal oxide particles and metalloid oxide particles. Oxide particles having controlled color characteristics of any one of reflectance, transmittance, molar absorption coefficient, hue, or color saturation can be provided by controlling the percentage of the M-OH bonds contained in metal oxide particles or metalloid oxide particles.
Method for the synthesis of nanoparticles of heterometallic nanocomposite materials
A simple one pot sol-gel method for the synthesis of bi-metal nanostructures is based on non-noble metals (Fe, Co and Sn) and titanium. The method involves the synthesis of mixed metal nanoscale composites using low cost precursors which allow for the synthesis of desired nanocomposite materials with self-scarifying titanium or silica supports. The procedure does not require any surfactant or any need for pH controlled step. Applicants' method involves the in-situ generation of precursors and their simultaneous entrapment in a gel. This simple one pot synthesis allows for the synthesis of homogenous size, shape and distribution of targeted nanostructures. Further, this method can be applied for the preparation of various nanocomposite materials using different choices of metals and self-scarifying supports. Applicants also show that Pd, the noble metal based nanocomposite is feasible.
ANODE ACTIVE MATERIAL FOR SECONDARY BATTERY, PREPARATION METHOD THEREOF AND SECONDARY BATTERY COMPRISING THE SAME
The present disclosure relates to an anode active material for a sodium ion secondary battery, a method for preparing the same, and a sodium ion secondary battery including the same. More particularly, the anode active material for a sodium ion secondary battery includes a cobalt tin spinel oxide obtained by a simple precipitation process, and can be applied to a sodium ion secondary battery having high capacity characteristics.
A METHOD FOR PREPARING METAL OXIDE NANOSHEETS
The present invention generally relates to a method for preparing metal oxide nanosheets. In a preferred embodiment, graphene oxide (GO) or graphite oxide is employed as a template or structure directing agent for the formation of the metal oxide nanosheets, wherein the template is mixed with metal oxide precursor to form a metal oxide precursor-bonded template. Subsequently, the metal oxide precursor-bonded template is calcined to form the metal oxide nanosheets. The present invention also relates to a lithium-ion battery anode comprising the metal oxide nanosheets. In a further preferred embodiment, the battery anode may comprising reduced template, which is reduced graphene oxide (rGO) or reduced graphite oxide.
Method for producing oxide particles with controlled color characteristics, oxide particles, and coating or film-like composition comprising the same
An object of the present invention is to provide a method for producing oxide particles with controlled color characteristics and to provide oxide particles with controlled color characteristics. The present invention provides a method for producing oxide particles, comprising controlling color characteristics of the oxide particles by controlling the ratio of M-OH bonds, the binding of one or more different elements (M) other than oxygen or hydrogen with hydroxyl group (OH), in oxide particles selected from metal oxide particles and metalloid oxide particles. According to the present invention, oxide particles having controlled color characteristics of any one of reflectance, transmittance, molar absorption coefficient, hue, or color saturation can be provided by controlling the percentage of the M-OH bonds contained in metal oxide particles or metalloid oxide particles.
PREPARATION METHOD OF TIN-BASED LITHIUM COBALTATE PRECURSOR AND USE THEREOF
The present disclosure discloses a preparation method of a tin-based lithium cobaltate precursor and use thereof. The method involves adding a cobalt salt solution, a precipitant and a complexing agent for reaction to obtain a precipitate, wherein the precipitant is a mixed solution of carbonate and stannate; calcining the precipitate; and mixing the calcined material with dioxane, ball-milling the mixture, and subjecting the ball-milled product to a heating and pressurization treatment to obtain the tin-based lithium cobaltate precursor. In the present disclosure, after carbonate and stannate are blended, the blend react with cobalt salt to form the co-precipitate of cobalt carbonate and cobalt stannate, and after calcination, a mixture of cobalt(II,III) oxide and tin dioxide is formed. By utilizing dioxane for solvent hot pressing, particles are bonded to each other, forming grain boundary channels. In addition, by doping with tin, the conductivity of the material is improved.
POSITIVE ACTIVE MATERIAL AND LITHIUM-ION BATTERY
The present application provides a positive active material, a positive electrode and a lithium-ion battery. The positive active material comprising a first particle and a second particle, wherein the first particle has a chemical formula of Li.sub.eCo.sub.gM.sub.1-gO.sub.2-i, and the second particle has a chemical formula of Li.sub.fCo.sub.hN.sub.1-hO.sub.2-j, the element M is at least two selected from a group consisting of Ni, Mn, Al, Mg, Ti, La, Y and Zr, the element N is at least one selected from a group consisting of Ni, Mn, Al, Mg, Ti, La, Y and Zr, and 0.8e1.2, 0<g<1, 0.1i0.2, 0.8f1.2, 0<h<1, 0.1j0.2, the number of types of the element M in the first particle is greater than the number of types of the element N in the second particles. The positive active material of the present application has a good stability and can improve the capacity retention rate of the lithium-ion battery.
Positive electrode active material for non-Aqueous electrolyte secondary battery, non-Aqueous electrolyte secondary battery, and method for producing positive electrode active material for non-aqueous electrolyte secondary battery
According to one embodiment, a positive electrode active material for a non-aqueous electrolyte secondary battery contains a lithium/transition metal composite oxide that contains 80 mol % or more, relative to the total mol number of metal elements other than Li, of Ni and at least one kind of metal element selected from among Co, Mn, Al, W, Mg, Mo, Nb, Ti, Si and Zr. When a filtrate of a suspension, said suspension being prepared by adding 250 mg of the positive electrode active material to 10 mL of a 17.5 mass % aqueous solution of hydrochloric acid, dissolving by heating at 90? C. for 2 hours and then diluting to 50 mL, is analyzed by inductively coupled plasma mass spectrometry, the elution amount of S in the filtrate is 0.002 mmol or greater.
OPEN VESSELS AND THEIR USE
Vessels such as crucibles, pans, open cups and saggars, containing a monolithic ceramic material, and a ceramic matrix composite, wherein the monolithic ceramic material is an inner tart. A method for making oxide materials that can be utilized in the contact with corrosive materials and that allows for higher conversions in a given heating process.