Aspects of the present disclosure are directed towards a method of making a scandium metal-doped nanoparticle. The method includes mixing a cobalt salt, an iron salt, and an acid in water to form a solution including CoFe.sub.2O.sub.4; mixing a nickel-iron oxide solution and a scandium oxide solution to form a solution including NiSc.sub.0.03Fe.sub.1.97O.sub.4; mixing the cobalt iron oxide solution and the nickel scandium iron oxide solution to form a sol-gel mixture including CoFe.sub.2O.sub.4/(NiSc.sub.0.03Fe.sub.1.97O.sub.4).sub.x (0≤x≤5); adjusting the pH of the sol-gel mixture 6 to 8 with a base to form a first mixture; heating the first mixture to form a powder, and calcining the powder to form the scandium metal-doped nanoparticle of formula CoFe.sub.2O.sub.4/(NiSc.sub.0.03Fe.sub.1.97O.sub.4).sub.x (0≤x≤5). The present disclosure also describes an electrode including the scandium metal-doped nanoparticles. The electrode may be used in magnetic supercapacitors.

A method of producing a positive electrode active material for a nonaqueous electrolyte secondary battery, the method includes preparing nickel-containing composite oxide particles having a ratio .sup.1D.sub.90/.sup.1D.sub.10 of a 90% particle size .sup.1D.sub.90 to a 10% particle size .sup.1D.sub.10 in volume-based cumulative particle size distribution of 3 or less; obtaining a raw material mixture containing the composite oxide particles and a lithium compound and having a ratio of a total number of moles of lithium to a total number of moles of metal elements contained in the composite oxide in a range of 1 to 1.3; subjecting the raw material mixture to a heat treatment to obtain a heat-treated material; subjecting the heat-treated material to a dry-dispersion treatment to obtain a first dispersion; and bringing the first dispersion into contact with a liquid medium to obtain a second dispersion.

A method of producing a positive electrode active material for a nonaqueous electrolyte secondary battery, the method includes preparing nickel-containing composite oxide particles having a ratio .sup.1D.sub.90/.sup.1D.sub.10 of a 90% particle size .sup.1D.sub.90 to a 10% particle size .sup.1D.sub.10 in volume-based cumulative particle size distribution is 3 or less; mixing the composite oxide particles and a lithium compound to obtain a first mixture; subjecting the first mixture to a first heat treatment at a first temperature and a second heat treatment at a second temperature higher than the first temperature to obtain a first heat-treated product; and subjecting the first heat-treated material to a dispersion treatment.

A nickel-containing hydroxide capable of obtaining a positive electrode active material having excellent initial charge-discharge efficiency and a high volume capacity density. The nickel-containing hydroxide for a precursor of a positive electrode active material of a non-aqueous electrolyte secondary battery, wherein when a peak intensity of a diffraction peak appearing in the range of 2θ=19.2±1 in powder X-ray diffraction measurement using CuKα rays is defined as α, and a peak intensity of a diffraction peak appearing in the range of 2θ=38.5±1 in powder X-ray diffraction measurement using CuKα rays is defined as β, the peak intensity ratio of α/β is 0.80 or more and 1.38 or less, and the average long diameter of primary particles is 290 nm or more and 425 nm or less.

Ternary precursor particles used for a lithium-ion battery, the ternary precursor particles having a Ni.sub.xCo.sub.yMn.sub.z(OH).sub.2, wherein, x+y+z=1, 0<x<1, 0<y<1, 0<z<1; each ternary precursor particle is a spheroidal structure, and comprises a shell, a transition layer and a particle core; the shell is a dense structure, the particle core is a porous structure, the transition layer surrounds the particle core and is sandwiched between the shell and the particle core; each ternary precursor particle is a mixture formed by mixing the nickel hydroxide, the cobalt hydroxide and the manganese hydroxide at the atomic level; a crystallinity of the shell is greater than a crystallinity of the transition layer, and the crystallinity of the transition layer is greater than a crystallinity of the particle core.

The present invention generally relates to a method for preparing metal oxide nanosheets. In a preferred embodiment, graphene oxide (GO) or graphite oxide is employed as a template or structure directing agent for the formation of the metal oxide nanosheets, wherein the template is mixed with metal oxide precursor to form a metal oxide precursor-bonded template. Subsequently, the metal oxide precursor-bonded template is calcined to form the metal oxide nanosheets. The present invention also relates to a lithium-ion battery anode comprising the metal oxide nanosheets. In a further preferred embodiment, the battery anode may comprising reduced template, which is reduced graphene oxide (rGO) or reduced graphite oxide.

The present invention is in the field of heterogeneous catalysis.

Particularly, the present invention relates to a process for preparing catalysts advantageously usable in the hydrotreatment processes, for example in hydrodesulphurization, hydrodenitrogenation, hydrodearomatization processes of hydrocarbons.

More in particular, the present invention relates to a process for obtaining said catalysts, which comprise mixed oxides of Nickel, Aluminum, Molybdenum and Tungsten and optionally a transition metal Me selected from the group consisting of Zn, Mn, Cd, and a mixture thereof, an organic component C, and possibly an inorganic binder B.

Said mixed oxides comprise an amorphous phase and a pseudo-crystalline phase isostructural to Wolframite.

The present invention further relates to said hydrotreatment catalysts and a hydrotreatment process wherein said catalysts are used.

Provided are processes for the production of particles for use as a precursor material for synthesis of Li-ion cathode active material of a lithium-ion cell comprising: a non-lithiated nickel oxide particle of the formula MO.sub.x wherein M comprises 80 at % Ni or greater and wherein x is 0.7 to 1.2, M optionally excluding boron in the MO.sub.x crystal structure; and a modifier oxide intermixed with, coated on, present within, or combinations thereof the non-lithiated nickel oxide particle, wherein the modifier oxide is associated with the non-lithiated nickel oxide such that a calcination at 500 degrees Celsius for 2 hours results in crystallite growth measured by XRD of 2 nanometers or less.

A method of producing a positive electrode active material for a nonaqueous electrolyte secondary battery, the method includes preparing nickel-containing composite oxide particles having a ratio .sup.1D.sub.90/.sup.1D.sub.10 of a 90% particle size .sup.1D.sub.90 to a 10% particle size .sup.1D.sub.10 in volume-based cumulative particle size distribution of 3 or less; obtaining a raw material mixture containing the composite oxide particles and a lithium compound and having a ratio of a total number of moles of lithium to a total number of moles of metal elements contained in the composite oxide in a range of 1 to 1.3; subjecting the raw material mixture to a heat treatment to obtain a heat-treated material; subjecting the heat-treated material to a dry-dispersion treatment to obtain a first dispersion; and bringing the first dispersion into contact with a liquid medium to obtain a second dispersion.

A method of producing a positive electrode active material for a nonaqueous electrolyte secondary battery, the method includes preparing nickel-containing composite oxide particles having a ratio .sup.1D.sub.90/.sup.1D.sub.10 of a 90% particle size .sup.1D.sub.90 to a 10% particle size .sup.1D.sub.10 in volume-based cumulative particle size distribution is 3 or less; mixing the composite oxide particles and a lithium compound to obtain a first mixture; subjecting the first mixture to a first heat treatment at a first temperature and a second heat treatment at a second temperature higher than the first temperature to obtain a first heat-treated product; and subjecting the first heat-treated material to a dispersion treatment.