A method of fabricating polyacrylonitrile (PACN) nanostructured carbon superstructure shapes is provided that includes forming a PACN polymer superstructure shape by using as a monomer, an initiator, and a solvent or incorporation of a different co-monomer for free radical polymerization, and converting the PACN polymer superstructure shape to a nanostructured carbon superstructure analogue using stabilization and carbonization of the PACN polymer superstructure shape, where the stabilization includes heating the PACN polymer superstructure shape to a temperature that is adequate to form a stabilization reaction, where the carbonization includes using a heat treatment.

The present invention relates to a carbon nanotube-transition metal oxide composite and a method for making the composite. The composite comprises at least one carbon nanotube and a plurality of transition metal oxide nanoparticles. The plurality of transition metal oxide nanoparticles are chemically bonded to the at least one carbon nanotube through carbon-oxygen-metal (C—O-M) linkages, wherein the metal is a transition metal element. The method for making the composite comprising the following steps: step 1, providing at least one carbon nanotube obtained from a super-aligned carbon nanotube array; step 2, pre-oxidizing the at least one carbon nanotube; step 3, dispersing the at least one carbon nanotube in a solvent to form a first suspension; step 4, dispersing a material containing transition metal oxyacid radicals in the first suspension to form a second suspension; and step 5, removing the solvent from the second suspension and drying the second suspension.

An object of the present invention is to provide ferrite particles having a high saturation magnetisation, and being excellent in the dispersibility in a resin, a solvent or a resin composition, a resin composition including the ferrite particles, and a resin film composed of the resin composition. The ferrite particles are a single crystalline body having an average particle size of 1 to 2000 nm, and Mn-based ferrite particles having a spherical shape, and have a saturation magnetisation of 45 to 95 Am.sup.2/kg. The resin composition includes the ferrite particles as a filler. The resin film is composed of the resin composition.

The present disclosure relates to a device comprising todorokite constructed of octahedra of manganese oxide forming a channel, wherein the channel contains a plurality of alkali ions but does not contain crystalline water molecules. In some aspects of the present disclosure, one of the alkali ions is magnesium and the channel may have a diameter of approximately one nanometer.

The present invention relates to silicon-compound-coated fine metal particles, with which surfaces of fine metal particles, composed of at least one type of metal element or metalloid element, are at least partially coated with a silicon compound and a ratio of Si—OH bonds contained in the silicon-compound-coated fine metal particles is controlled to be 0.1% or more and 70% or less. By the present invention, silicon-compound-coated fine metal particles that are controlled in dispersibility and other properties can be provided by controlling the ratio of Si—OH bonds or the ratio of Si—OH bonds/Si—O bonds contained in the silicon-compound-coated fine metal particles. By controlling the ratio of Si—OH bonds or the ratio of Si—OH bonds/Si—O bonds, a composition that is more appropriate for diversifying applications and targeted properties of silicon-compound-coated fine metal particles than was conventionally possible can be designed easily.

There is provided an industrially scalable system and method for preparing graphene oxide and thereafter reduced graphene oxide, with high yields (generally better than 98 percent), in which the yield and quality are maximized. In certain embodiments of the present method and process, the initial particle size of the graphite charge and the temperature profile are of greater importance to a successful outcome than the reactants themselves. It should be noted that unlike the previous Hummers methods and derivatives, secondary oxidizers and exfoliation agents such as nitric acid, sodium nitrate and similar intercalation agents are not necessary to achieve the desired result.

Nanostructured aluminosilicates including aluminosilicate nanorods are formed by heating a geopolymer resin containing up to about 90 mol % water in a closed container at a temperature between about 70° C. and about 200° C. for a length of time up to about one week to yield a first material including the aluminosilicate nanorods. The aluminosilicate nanorods have an average width of the between about 5 nm and about 30 or between about 5 nm and about 60 nm or between about 5 nm and about 100 nm, and a majority of the aluminosilicate nanorods have an aspect ratio between about 2 and about 100.

In a method of preparing a lithium metal oxide, a preliminary lithium metal oxide is prepared. The preliminary lithium metal oxide is washed using a washing solution to remove lithium salt impurities. The washing solution includes water and an organic ligand multimer compound. The lithium metal oxide having improved structural uniformity and stability is obtained using the washing solution.

A unique crystalline mixed transition metal tungstate material has been developed material may be sulfided to generate metal sulfides which are used as a catalyst in a conversion process such as hydroprocessing. The hydroprocessing may include hydrodenitrification, hydrodesulfurization, hydrodemetallation, hydrodesilication, hydrodearomatization, hydroisomerization, hydrotreating, hydrofining, and hydrocracking.

Systems, methods, and compositions are disclosed for a Li-substituted layered-tunneled O3/spinel Na(Ni.sub.xFe.sub.yMn.sub.z)O.sub.2 cathode material, Na.sub.0.87Li.sub.0.25Ni.sub.0.4Fe.sub.0.2Mn.sub.0.4O.sub.2+∂ (LS-NFM) for enhanced sodium ion storage and cycling stability. The LS-NFM electrode is prepared by adjusting the stoichiometric ratio of the Na ion over the sum of Li and transition metal ions below 1. The Rietveld refinement of XRD data indicates that the cathode is composed of 94% layered and 6% spinel components. When cycled at a high current density of 100 mA g.sup.−1, LS-NFM cathode exhibited a first-cycle Coulombic efficiency of 88% and reversible discharge capacity of 107 mAh g.sup.−1 after 50 cycles with the capacity retention of 95%.