C01P2004/30

Nitride aluminum particle

To provide an aluminum nitride particle having a hexagonal columnar barrel part and bowl-like projection parts at both ends of the columnar part, wherein the long diameter (D) of the barrel part is 10 to 250 μm, the ratio (L.sub.1/D) of the distance (L.sub.1) between the apexes of the two projection pars to the long diameter (D) of the barrel part is 0.7 to 1.3, and the percentage of the length or thickness (L.sub.2) of the barrel part to the distance (L.sub.1) between the apexes of the two projection parts is 10 to 60%. The aluminum nitride particle can provide high heat conductivity and excellent electric insulation to a resin when it is filled into the resin.

Bis(fluorosulfonyl) imide metal salt and method for preparing same

In the present invention, a bis (fluorosulfonyl) imide metal salt is an alkali metal salt of bis (fluorosulfonyl) imide or an alkaline earth metal salt of bis (fluorosulfonyl) imide. The bis (fluorosulfonyl) imide metal salt has an average particle diameter of not less than 0.1 mm, or has an average moisture absorption rate of not more than 2.5 mass ppm/cm.sup.2.Math.min when sealed in a PE bag having a thickness of 80 μm and left for 30 minutes at 23° C. and 65% humidity.

Plate-shaped hydrotalcite with high aspect ratio, method for manufacturing same and resin composition

With respect to a plate-shaped hydrotalcite in which the average width of primary particles is increased, (1) the aspect ratio of secondary particles is increased by suppressing aggregation of primary particles by relatively reducing the average thickness thereof, and 2) the formation of a by-product that impairs the transparency of a resin is suppressed. Provided is a plate-shaped hydrotalcite represented by a formula (1) below:
(M.sup.2+).sub.1−x(M.sup.3+).sub.x(OH).sub.2(A.sup.n−).sub.x/n.Math.mH.sub.2O  (1) where M.sup.2+ indicates at least one divalent metal, M.sup.3+ indicates at least one trivalent metal, A.sup.n− indicates an n-valent anion, n indicates an integer of 1 to 6, and x and m are within respective ranges of 0.1≤x≤0.33 and 0≤m≤10, the formula (1) satisfying (A) to (D) below: (A) the average width of primary particles as measured using an SEM method is 1 μm or greater; (B) the average thickness of primary particles as measured using an SEM method is 80 nm or less; (C) the degree of monodispersity of width is 50% or greater; and (D) the degree of monodispersity of thickness is 50% or greater.

BORON NITRIDE AGGLOMERATE, THERMOSETTING RESIN COMPOSITION CONTAINING SAME, AND USE THEREOF
20210221743 · 2021-07-22 ·

Provided is a boron nitride agglomerate. The boron nitride agglomerate is of a multi-stage structure formed by arranging flaky hexagonal boron nitride primary particles in three-dimensional directions through adhesion of an inorganic binder. Further provided is a method for preparing the boron nitride agglomerate. The method comprises: mixing flaky hexagonal boron nitride primary particles with an inorganic binder, and controlling the mass of the inorganic binder to account for 0.02-20% of the mass of the flaky hexagonal boron nitride primary particles, so as to obtain the boron nitride agglomerate. The boron nitride agglomerate provided can be added to thermosetting resin compositions, and resin sheets, resin composite metal foil, prepregs, laminates, metal foil-covered laminates, and printed wiring boards prepared using the same have higher boron nitride addition, high thermal conductivity, and high peel strength.

Boron structure and boron powder of high purity

A boron structure body includes boron having each concentration of Ti, Al, Fe, Cr, Ni, Co, Cu, W, Ta, Mo and Nb being 0.1 ppmw or less and having a thickness of 0.8 to 5 mm. The boron structure body may have a tubular shape, and when used as a doping agent, a ratio of .sup.11B that is an isotope may be 95 mass % or more. The boron structure body can be easily crushed, and a high-purity boron powder having an average particle diameter of 0.5 to 3 mm and having each metal impurity concentration of 0.3 ppmw or less can be obtained.

Hexagonal boron nitride powder and method for producing the same, and composition and heat dissipation material using the same
11078080 · 2021-08-03 · ·

A hexagonal BN powder including aggregates of primary particles of hexagonal BN containing boron and oxygen as impurity elements at a content of 1.00 to 30.00% and 0 to 1.00% by mass, respectively, which has a peak A in a predetermined particle diameter range and a 50% volume cumulative particle diameter D.sub.50 (d1) of 30.0 to 200.0 μl in a particle size distribution curve, and in which a ratio of a height (a1) of the peak A before treatment to a height (a2) of the peak A after treatment is 0.80 to 1.00 and a ratio of D.sub.50 (d1) before treatment to D.sub.50 (d2) after treatment is 0.80 to 1.00 when the hexagonal BN powder is ultrasonically treated under a predetermined condition for 1 minute. Also disclosed is a method for producing the hexagonal BN powder, a composition and a heat dissipation material.

FABRICATION OF BLUE-FLUORESCENT AND NON-TOXIC NANODIAMONDS 9NDs) FROM ATMOSPHERIC PARTICULATE MATTERS
20210292172 · 2021-09-23 ·

The present invention relates to a method for fabrication of blue-fluorescent and non-toxic nanodiamonds from atmospheric particulate matters including total solid suspended particulate matter (TSPM) and particulate matter with size less than 10μ (PM.sub.10). Mostly, the present invention provides an efficient mitigation process for particulate pollutant by conversion of these pollutants (PM and TSPM) into non-toxic high-value product such as nanodiamond by using the ultrasonic-assisted chemical oxidation method. This method is environmental friendly, simple, and biocompatible for the production of nanodiamonds from such atmospheric particulate matter.

ASPHERICAL HOLLOW SILICA PARTICLES AS SPF BOOSTERS

Described herein are aspherical hollow silica particles, processes for making aspherical hollow silica particles, and uses of aspherical hollow silica particles in sun care compositions. To form the aspherical hollow silica particles, deposition of a silica shell on a calcium carbonate template using a sol-gel chemistry is employed. Subsequent dissolution of the calcium carbonate template forms voids (e.g., a hollow interior) in the aspherical hollow silica particles.

Spinel particles, method for producing same and composition and molded article including spinel particles

Alumina is generally used as an inorganic filler, while spinel, which is known to be lower in thermal conductivity than alumina, is used in applications such as gems, fluorescence emitters, catalyst carriers, adsorbents, photocatalysts and heat-resistant insulating materials, but not expected to be used as a thermally conductive inorganic filler. Thus, an object of the invention is to provide spinel particles having excellent thermal conductive properties. The invention relates to a spinel particle including magnesium, aluminum and oxygen atoms and molybdenum and having a [111] plane crystallite diameter of 220 nm or more.

METHOD FOR PREPARING ZSM-5 ZEOLITE
20210155489 · 2021-05-27 ·

The present invention relates to a method for preparing ZSM-5 zeolite. The present invention can provide a method for preparing ZSM-5 zeolite comprising the steps of: preparing a first solution in a solution state by heating a mixture comprising a silica source, an alumina source, a neutralizing agent and a crystalline ZSM-5 nucleus; preparing a reaction mother liquid by mixing a second solution comprising salts into the first solution; and continuously crystallizing by continuously supplying the reaction mother liquid to a hydrothermal synthesis reactor, wherein formula [1] below is satisfied.


0.20≤W.sub.a/W.sub.b≤0.40  Formula [1]