Patent classifications
C02F2103/16
RESOURCE UTILIZATION-ORIENTED TREATMENT METHOD FOR SPENT ELECTROLESS NICKEL PLATING BATH
The present disclosure relates to the field of resource utilization-oriented treatment technologies for wastewater, and more particularly, to a resource utilization-oriented treatment method for a spent electroless nickel plating bath. The method includes oxidation de-complexation, synchronous precipitation of nickel and phosphorus, secondary precipitation of nickel, and resource utilization of sodium salt. In the present disclosure, in a reaction process, no sludge is generated to avoid secondary pollution to the environment. Further, the present disclosure has the advantages of short flow and less chemical use, greatly reducing treatment costs. In this way, this method is a low-cost and clean resource utilization-oriented treatment method capable of achieving resource utilization-oriented recovery of nickel, phosphorus, sodium, sulfate radical, or chlorine in the spent electroless nickel plating bath.
DEVICE FOR EFFICIENTLY RECYCLING NICKEL IN WASTEWATER AND METHOD
Disclosed is a device for efficiently recycling nickel from wastewater and a method. The device includes a housing, and an extraction unit and an electro-deposition unit which are respectively arranged inside the housing. The device is reasonable in overall structural design. An oscillating and floating component and a rotating component in an extraction cavity are used to fully and uniformly mix a solution to maximize the extraction strength. A mixing component in an electro-deposition cavity is used to accelerate ion dispersion, to better recycle nickel. The device is easy to operate, low in cost and suitable for mass promotion.
Electrochemical Oxidation of Amine Complexants in Waste Streams from Electroplating Processes
A process of treating a waste stream comprising organic amine compounds complexed with heavy metal ions. The process includes the steps of: (1) adjusting the pH of the waste stream to between about 4 and about 10; (2) b) adding a chloride salt to the waste stream to produce a concentration of chloride ions in the waste stream; and (3) circulating the waste stream through an electrochemical reactor. The electrochemical reactor comprises an array of electrodes comprising alternating anodes and cathodes. The waste stream is circulated through the electrochemical reactor for a period of time sufficient to hydrolyse amine compounds in the waste stream.
METHOD FOR CIRCULARLY PURIFYING METALLURGICAL ARSENIC-CONTAINING ACIDIC WASTE LIQUID AND RECOVERING SULFUR
A method for circularly purifying metallurgical arsenic-containing acidic waste liquid and recovering sulfur, including the following steps: (1) adding a calcium-free arsenic removal agent into the metallurgical arsenic-containing acidic waste liquid for stirring reaction, and filtering the reaction mixture to obtain arsenic-containing slag and a purified liquid; (2) adding calcium hydroxide into the purified liquid for secondary stirring reaction, and performing sedimentation and separation on the mixture to obtain a supernatant and a subjacent concentrated slurry; and refluxing the supernatant to a pretreatment workshop; (3) introducing the subjacent concentrated slurry into the metallurgical arsenic-containing acidic waste liquid, performing stirring reaction, and filtering the reaction mixture to obtain a liquid phase and a slag phase; and (4) washing the slag phase with water to obtain a gypsum product; refluxing the washing liquid to the pretreatment workshop; and taking the liquid phase as a raw material for purifying for removing arsenic.
Method for treating an effluent supersaturated with calcium carbonate in the presence of phosphonate precipitation-inhibiting products
The present invention relates to a method for treating an aqueous liquid effluent containing calcium and carbonate ions and containing precipitation-inhibiting products, said process comprising the following successive steps: a) providing an aqueous liquid effluent supersaturated with CaCO.sub.3 and containing precipitation-inhibiting products; b) having the effluent obtained in step a) pass into a reactor with high solid content with a solid content maintained between 20 and 800 g/l and integrated solid-liquid separation, at a pH comprised between 8 and 9.2 allowing in a single step precipitation in situ of the aragonite polymorph of calcium carbonate and removal of the precipitation-inhibiting products; c) recovering an aqueous liquid supernatant containing a suspended solids content of less than or equal to 0.1% by mass of the solid content in the reactor, advantageously a suspended solids content of less than 50 mg/l, the precipitation-inhibiting products being phosphonates.
Magnetically-controlled graphene-based micro-/nano-motor and fabrication method thereof
A method of fabricating a magnetically-controlled graphene-based micro-/nano-motor includes: (a) mixing FeCl.sub.3 crystal powder with deionized water to obtain a FeCl.sub.3 solution; (b) completely immersing a carbon-based microsphere in the FeCl.sub.3 solution; transferring the carbon-based microsphere from the FeCl.sub.3 solution followed by heating to allow crystallization of FeCl.sub.3 on the surface of the carbon-based microsphere to obtain a FeCl.sub.3-carbon-based microsphere; (c) heating the FeCl.sub.3-carbon-based microsphere in a vacuum chamber until there is no moisture in the vacuum chamber; continuously removing gas in the vacuum chamber and introducing oxygen; and treating the FeCl.sub.3-carbon-based microsphere with a laser in an oxygen-enriched environment to obtain the magnetically controlled graphene-based micro-/nano-motor. A magnetically-controlled graphene-based micro-/nano-motor is further provided.
Method for electrolysis-ozone-corrosion inhibitor/electrolysis-ozone-hydrogen peroxide-corrosion inhibitor coupling treatment on toxic and refractory wastewater
A method for electrolysis-ozone-corrosion inhibitor/electrolysis-ozone-hydrogen peroxide-corrosion inhibitor coupling treatment on toxic and refractory wastewater includes the following steps: adding toxic and refractory wastewater to be treated into a wastewater treatment reaction tank equipped with a plate anode and a plate cathode, and starting a direct current (DC) power supply connected to the plate anode and the plate cathode to treat the toxic and refractory wastewater at an appropriate current density under stirring, during which a corrosion inhibitor and hydrogen peroxide are added to the toxic and refractory wastewater to be treated and ozone is introduced into the toxic and refractory wastewater to be treated through an aeration device. The method can increase the production rate and production quantity of free radicals in a reaction system, effectively improve the treatment efficiency for toxic and refractory wastewater, and reduce the treatment cost.
Methods of treating water with powder activated carbon to reduce organic matter content
Methods are described that reduce the amount of organic matter in water, including reducing an amount of total organic carbon in water. The method includes adding powder activated carbon to the water; mixing the powder activated carbon in the water; and separating the powder activated carbon from the water. Also described are a method for reducing glycol content in water containing glycols, and a method for reducing glycol content in a steel mill wastewater stream containing glycols.
WASTEWATER TREATMENT METHOD AND APPARATUS BASED ON HYDRATE-BASED WATER VAPOR ADSORPTION
The present disclosure relates to the technical field of wastewater treatment, and provides a wastewater treatment method and apparatus based on hydrate-based water vapor adsorption. The apparatus includes a wastewater evaporation zone, a hydrate formation zone, a hydrate decomposition zone, and a data acquisition and control system. Rising water vapor and condensed water formed during evaporation of wastewater at normal temperature react with a hydrate former on a cooling wall surface to form a hydrate, continuous evaporation of the wastewater is promoted, the hydrate is scraped off to a collecting zone below by a scraper after being formed, and the hydrate is decomposed into fresh water, thereby realizing wastewater treatment. The present disclosure provides a method for treating complex wastewater containing a plurality of pollutants, where water vapor is consumed to form the hydrate to promote wastewater evaporation, and water obtained from the decomposition does not contain pollutants theoretically.
Systems and methods for shielded inductive devices
In an embodiment, a circuit includes: a transformer defining an inductive footprint within a first layer; a grounded shield bounded by the inductive footprint within a second layer separate from the first layer; and a circuit component bounded by the inductive footprint within a third layer separate from the second layer, wherein: the circuit component is coupled with the transformer through the second layer, and the third layer is separated from the first layer by the second layer.