The present invention is a method for producing a quartz glass crucible for pulling a single crystal silicon from a silicon melt held therein, including the steps of: producing a quartz glass crucible having an outer layer including an opaque quartz glass containing bubbles therein and an inner layer including a transparent quartz glass containing substantially no bubbles; roughening a region of an inner surface of the produced quartz glass crucible, the region being in contact with the silicon melt when holding the silicon melt; and heating the quartz glass crucible having the roughened inner surface to crystallize a surface of the roughened region. This can produce a quartz glass crucible for pulling a single crystal silicon which can suppress generation of a brown ring on the inner surface of the crucible during pulling the single crystal silicon and can suppress crystallinity disorder of the single crystal silicon.

A method of forming a part includes forming a glass-ceramic matrix composite material to form a pre-consolidated feedstock sheet with a pre-determined shape. The pre-consolidated feedstock sheet is sectioned into a first piece of pre-consolidated feedstock sheet and a second piece of pre-consolidated feedstock sheet. The first piece of pre-consolidated feedstock sheet and a second piece of pre-consolidated feedstock sheet are assembled with a second piece of pre-consolidated feedstock sheet to form a composite layup. The first piece of pre-consolidated feedstock sheet and the second piece of pre-consolidated feedstock sheet are joined by compressing the composite layup to form a glass-ceramic matrix composite part.

A method of forming a part includes forming a glass-ceramic matrix composite material to form a pre-consolidated feedstock sheet with a pre-determined shape. The pre-consolidated feedstock sheet is sectioned into a first piece of pre-consolidated feedstock sheet and a second piece of pre-consolidated feedstock sheet. The first piece of pre-consolidated feedstock sheet and a second piece of pre-consolidated feedstock sheet are assembled with a second piece of pre-consolidated feedstock sheet to form a composite layup. The first piece of pre-consolidated feedstock sheet and the second piece of pre-consolidated feedstock sheet are joined by compressing the composite layup to form a glass-ceramic matrix composite part.

A mixture including glass fragments is located in a containment vessel and is processed in a kiln to form a commercially useful building product. The mixture is initially heated over a first time period to a first temperature intermediate the glass transition point temperature and about 950? C. or 1,100? C. (Section A). At the first temperature the glass fragments slump and bond to each other and the mixture is soaked at this temperature for a second time period (Section B). After reducing the temperature (Section C), the mixture is annealed for another time period (Section D). Finally, the kiln is cooled to allow the mixture to be removed (Section E).

A mixture including glass fragments is located in a containment vessel and is processed in a kiln to form a commercially useful building product. The mixture is initially heated over a first time period to a first temperature intermediate the glass transition point temperature and about 950? C. or 1,100? C. (Section A). At the first temperature the glass fragments slump and bond to each other and the mixture is soaked at this temperature for a second time period (Section B). After reducing the temperature (Section C), the mixture is annealed for another time period (Section D). Finally, the kiln is cooled to allow the mixture to be removed (Section E).

A high strength glass fiber is prepared by following steps: weighing raw materials according to a mass percentage of 50-60% silica sol, 24-31% aluminum sol, 8-11% magnesia, 4-5% calcium oxide, 0.1-2% titanium dioxide, 0-0.5% ferric oxide, 0.5-2% niobium pentoxide, 0.5-1.5% antimony trioxide, 0.3-1.5% bismuth nitrate, and 0.1-0.5% boric acid. Deionized water is added. The raw material undergoes mixing by ball milling, spray-drying, calcining, isostatic pressing, melting, and wire-drawing. The invention adopts silicon sol, aluminum sol and bismuth nitrate. Through ball milling and spray-drying, silicon aluminum barium plasmas is evenly coated on surface of other oxide powders. Then nano particles, of silica, alumina and bismuth oxide are obtained by calcining. Under the effect of the high specific surface energy of nano particles, and the close contact of each component, high strength glass fiber is obtained in relatively low fiber drawing temperature while the glass melting temperature and time are significantly reduced.

A high strength glass fiber is prepared by following steps: weighing raw materials according to a mass percentage of 50-60% silica sol, 24-31% aluminum sol, 8-11% magnesia, 4-5% calcium oxide, 0.1-2% titanium dioxide, 0-0.5% ferric oxide, 0.5-2% niobium pentoxide, 0.5-1.5% antimony trioxide, 0.3-1.5% bismuth nitrate, and 0.1-0.5% boric acid. Deionized water is added. The raw material undergoes mixing by ball milling, spray-drying, calcining, isostatic pressing, melting, and wire-drawing. The invention adopts silicon sol, aluminum sol and bismuth nitrate. Through ball milling and spray-drying, silicon aluminum barium plasmas is evenly coated on surface of other oxide powders. Then nano particles, of silica, alumina and bismuth oxide are obtained by calcining. Under the effect of the high specific surface energy of nano particles, and the close contact of each component, high strength glass fiber is obtained in relatively low fiber drawing temperature while the glass melting temperature and time are significantly reduced.

To provide granules for the production of silicate glass, said granules being less likely to adhere even if heated at a high temperature exceeding 800 C. A method for producing granules, which has a step of mixing a glass raw material composition composed essentially of an alkali metal source, an alkaline earth metal source and a powdery silicon source, with water, followed by compression molding, and which is characterized in that the glass raw material composition contains at least 50 mass % of the silicon source, and at least 10 mass % in total of the alkali metal source and the alkaline earth metal source, as calculated as oxides, based on 100 mass % of the silicate glass obtainable from the granules, the alkali metal source contains an alkali metal carbonate, and D90 representing the particle size at a cumulative volume of 90% in the particle size accumulation curve of the alkaline earth metal source is at most 100 m.

To provide granules for the production of silicate glass, said granules being less likely to adhere even if heated at a high temperature exceeding 800 C. A method for producing granules, which has a step of mixing a glass raw material composition composed essentially of an alkali metal source, an alkaline earth metal source and a powdery silicon source, with water, followed by compression molding, and which is characterized in that the glass raw material composition contains at least 50 mass % of the silicon source, and at least 10 mass % in total of the alkali metal source and the alkaline earth metal source, as calculated as oxides, based on 100 mass % of the silicate glass obtainable from the granules, the alkali metal source contains an alkali metal carbonate, and D90 representing the particle size at a cumulative volume of 90% in the particle size accumulation curve of the alkaline earth metal source is at most 100 m.

One aspect relates to a process for the preparation of a quartz glass grain, including providing a silicon dioxide granulate from a pyrogenically produced silicon dioxide powder, making a glass melt out of silicon dioxide granulate, making a quartz glass body out of at least part of the glass melt and reducing the size of the quartz glass body to obtain the quartz glass grain. One aspect further relates to a quartz glass grain which is obtainable by this process. One aspect further relates to opaque quartz glass bodies, which are obtainable by further processing of the quartz glass grain.