A preparation method for improving light efficiency and stability of light storing ceramics is provided. Calcium ethanol solution is added into titanium precursor solution firstly and oleic acid dispersant is added, pure water and the light storing powder are subsequently added to obtain a light-storing powder-calcium titanate gel, and dried, crushed and sieved to obtain xerogel powder. Glass matrix material, sieved xerogel powder and another dispersant are placed into a granulator, and directly mechanically stirred and granulated after adding pure water. A plasticizer is added after stirring 4˜8 h, and continuously stirred for 1˜3 h to obtain a mixture, pressing, drying and firing. Calcium titanate is manually introduced to protect the light-storing powder from hydrolysis or high-temperature oxidation. It can also change the propagation path of fluorescence inside ceramics, improve light absorption and fluorescence output efficiency and is conducive to ceramic molding.

A multicolor light-storing ceramic for fire-protection indication and a preparation method thereof are provided. The preparation method includes: adding a glass based raw material, a light-storing powder, a dispersant and an alumina powder into a granulator, adding water mixed with a pore-forming agent and then mechanically stirring for granulation; adding a plasticizer after the stirring of 4˜8 h, and continuing the stirring for 1˜3 h to thereby obtain a mixture; packing the mixture into a mold and performing tableting; demolding and obtaining a light-storing self-luminous quartz ceramic by drying and firing using a kiln; printing a pattern onto a surface of the ceramic and then curing to obtain a light-storing ceramic for indication sign. Using an industrial waste glass has advantages of low sintering temperature and green environmental protection; dispersed pores and alumina introduced as scattering sources improves light absorption efficiency, fluorescence output phase ratio and light transmission of the ceramic.

A preparation method and use of a yellow fluorescent glass ceramic are disclosed. The preparation method includes: mixing a monomer, a cross-linking agent and a filling solvent evenly, then adding fumed silica and stirring evenly, further adding an ultraviolet (UV) photoinitiator and an UV absorber, and stirring thoroughly; adding a yellow phosphor (Y,Gd)AG:Ce, stirring thoroughly and defoaming to obtain a slurry; introducing the slurry into a mold, and curing by UV irradiation or three-dimensional (3D) printing to obtain a body; putting the body into a high-temperature furnace for heating to obtain a phosphor-embedded porous silica glass; putting the porous silica glass into a high-temperature vacuum furnace for densification and sintering to obtain a densified fluorescent glass ceramic; and finally cutting and surface-polishing.

Embodiments of the invention include a transparent material such as glass including a metal such as bismuth, particles of luminescent material such as a nitride phosphor disposed in the transparent material, and a coating disposed over the particles of luminescent material. The coating is formed to prevent reaction between the particles of luminescent material and the metal. The coating may be silica.

Methods for synthesizing fibers having nanoparticles therein are provided, as well as preforms and fibers incorporating nanoparticles. The nanoparticles may include one or more rare earth ions selected based on fluorescence at eye-safer wavelengths, surrounded by a low-phonon energy host. Nanoparticles that are not doped with rare earth ions may also be included as a co-dopant to help increase solubility of nanoparticles doped with rare earth ions in the silica matrix. The nanoparticles may be incorporated into a preform, which is then drawn to form fiber. The fibers may beneficially be incorporated into lasers and amplifiers that operate at eye safer wavelengths. Lasers and amplifiers incorporating the fibers may also beneficially exhibit reduced Stimulated Brillouin Scattering.

The glass ceramic material of the present disclosure contains a glass that contains SiO.sub.2, B.sub.2O.sub.3, Al.sub.2O.sub.3, and M.sub.2O, where M is an alkali metal, and a filler that contains quartz, Al.sub.2O.sub.3, and ZrO.sub.2. The glass ceramic material contains the glass in an amount of 57.4% by weight or more and 67.4% by weight or less, the quartz in the filler in an amount of 29% by weight or more and 39% by weight or less, the Al.sub.2O.sub.3 in the filler in an amount of 1.8% by weight or more and 5% by weight or less, and the ZrO.sub.2 in the filler in an amount of 0.3% by weight or more and 1.8% by weight or less.

Provided is a wavelength conversion member that can be readily adjusted in chromaticity and can be increased in productivity and a production method for the wavelength conversion member. A wavelength conversion member 1 having a first principal surface 1a and a second principal surface 1b opposed to each other includes a glass matrix 2 and phosphor particles 3 disposed in the glass matrix 2, wherein concentrations of the phosphor particles 3 in the first principal surface 1a and in the second principal surface 1b are higher than concentrations of the phosphor particles 3 in surface layer bottom planes 1c and 1d located 20 μm inward from the first principal surface 1a and 20 μm inward from the second principal surface 1b, respectively.

An antimicrobial article that includes: an antimicrobial composite region that includes a matrix comprising a polymeric material, and a first plurality of particles within the matrix. The particles include a phase-separable glass with a copper-containing antimicrobial agent. The antimicrobial composite region can be a film containing the first plurality of particles that is subsequently laminated to a bulk element. The first plurality of particles can also be pressed into the film or a bulk element to define an antimicrobial composite region. An exposed surface portion of the antimicrobial composite region can exhibit at least a log 2 reduction in a concentration of at least one of Staphylococcus aureus, Enterobacter aerogenes, and Pseudomonas aeruginosa bacteria under a Modified EPA Copper Test Protocol.

An optical fibre, for use in the field of distributed measurement of temperature or deformation by optical reflectometry in the frequency domain using the Rayleigh backscattered signal in the fibre, includes a core doped with nanoparticles for example formed from gold particles covered with zirconium oxide, and can be subjected to high temperatures during the measurement. A method for producing the optical fibre includes a step of heat treatment during which the optical fibre is subjected, for a duration of at least one hour, to a heat treatment temperature higher than a maximum temperature to which it will be subjected during a measurement.

A tinted glass composition and glass article including the same, the composition including: about 45 mol % to about 80 mol % SiO.sub.2; about 6 mol % to about 22 mol % Al.sub.2O.sub.3; 0 mol % to about 25 mol % B.sub.2O.sub.3; about 7 mol % to about 25 mol % of at least one alkaline earth oxide selected from MgO, CaO, SrO, BaO, and combinations thereof; about 0.5 mol % to about 20 mol % CuO; 0 mol % to about 6 mol % SnO.sub.2, SnO, or a combination thereof; 0 mol % to about 1.0 mol % C; 0 mol % to about 5 mol % La.sub.2O.sub.3; and 0 mol % to about 10 mol % PbO, and that is substantially free of alkali metal.