Patent classifications
C07C53/124
Preparation of (R)-3-hydroxybutyric acid or its salts by one-step fermentation
The subject invention relates to a process of preparing (R)-3-hydroxybutyric acid or a salt thereof by one-step fermentation with a nonpathogenic microorganism. The fermentation of (R)-3-hydroxybutyric acid was performed by supplying with certain carbon and nitrogen sources. These microorganisms include a Glutamic acid Bacterium HR057 strain or one type of genetically engineered Corynebacterium Glutamicum.
Process for the production of diacyl peroxides
Process for the production of a diacyl peroxide involving the reaction of an anhydride with hydrogen peroxide, removal of the formed carboxylic acid, production of an anhydride from said carboxylic acid, and recycling of the anhydride within the process.
Process for the production of diacyl peroxides
Process for the production of a diacyl peroxide involving the reaction of an anhydride with hydrogen peroxide, removal of the formed carboxylic acid, production of an anhydride from said carboxylic acid, and recycling of the anhydride within the process.
Method of preparing N-butyric acid by using poly-3-hydroxybutyrate
The present invention relates to a method of preparing n-butyric acid by using poly-3-hydroxybutyrate. The method comprises following steps: placing poly-3-hydroxybutyrate in a closure means, passing hydrogen into the closure means to eliminate air after making an initial hydrogen pressure be 2 to 6 MPa, carrying out an agitation at 190 to 240 C. for reaction for 6 to 36 hours to obtain n-butyric acid. The preparation method provided by the present invention does not require a catalyst or a reaction solvent, and converts poly-3-hydroxybutyrate into n-butyric acid by a one-step reaction under a hydrogen atmosphere. The conversion rate of poly-3-hydroxybutyrate is 100%, the yield of n-butyric acid reaches up to 97%, the purity of n-butyric acid in all obtained liquid products reaches up to 98%, and no additional subsequent separation process is needed to the target product n-butyric acid.
Method of preparing N-butyric acid by using poly-3-hydroxybutyrate
The present invention relates to a method of preparing n-butyric acid by using poly-3-hydroxybutyrate. The method comprises following steps: placing poly-3-hydroxybutyrate in a closure means, passing hydrogen into the closure means to eliminate air after making an initial hydrogen pressure be 2 to 6 MPa, carrying out an agitation at 190 to 240 C. for reaction for 6 to 36 hours to obtain n-butyric acid. The preparation method provided by the present invention does not require a catalyst or a reaction solvent, and converts poly-3-hydroxybutyrate into n-butyric acid by a one-step reaction under a hydrogen atmosphere. The conversion rate of poly-3-hydroxybutyrate is 100%, the yield of n-butyric acid reaches up to 97%, the purity of n-butyric acid in all obtained liquid products reaches up to 98%, and no additional subsequent separation process is needed to the target product n-butyric acid.
MULTIPLE-COMPONENT SOLID PHASES CONTAINING AT LEAST ONE ACTIVE PHARMACEUTICAL INGREDIENT
The subject invention concerns a method for identifying complementary chemical functionalities to form a desired supramolecular synthon. The subject invention also pertains to multiple-component phase compositions comprising one or more pharmaceutical entities and methods for producing such compositions.
MULTIPLE-COMPONENT SOLID PHASES CONTAINING AT LEAST ONE ACTIVE PHARMACEUTICAL INGREDIENT
The subject invention concerns a method for identifying complementary chemical functionalities to form a desired supramolecular synthon. The subject invention also pertains to multiple-component phase compositions comprising one or more pharmaceutical entities and methods for producing such compositions.
Transition metal-catalyzed production of alcohol and carbonyl compounds from hydrocarbons
Processes for converting a hydrocarbon reactant into an alcohol compound and/or a carbonyl compound are disclosed in which the hydrocarbon reactant and a supported transition metal catalystcontaining molybdenum, tungsten, or vanadiumare irradiated with a light beam at a wavelength in the UV-visible spectrum, optionally in an oxidizing atmosphere, to form a reduced transition metal catalyst, followed by hydrolyzing the reduced transition metal catalyst to form a reaction product containing the alcohol compound and/or the carbonyl compound.
Transition metal-catalyzed production of alcohol and carbonyl compounds from hydrocarbons
Processes for converting a hydrocarbon reactant into an alcohol compound and/or a carbonyl compound are disclosed in which the hydrocarbon reactant and a supported transition metal catalystcontaining molybdenum, tungsten, or vanadiumare irradiated with a light beam at a wavelength in the UV-visible spectrum, optionally in an oxidizing atmosphere, to form a reduced transition metal catalyst, followed by hydrolyzing the reduced transition metal catalyst to form a reaction product containing the alcohol compound and/or the carbonyl compound.
A PROCESS FOR MANUFACTURING OF FIRE SUPPRESSING CRYSTALS
A process for the manufacturing of fire suppressing crystals having a high Q-factor particle size distribution, said fire suppression crystals being intended for use as a fire suppressing additive in polymer compositions, the process comprising the steps; a) Preparing a mother liquor comprising water and a salt composition obtained in step c) or d), the temperature of said mother liquor being adjusted to 10-50 C. and comprising said salt composition to a level of at least 90% of saturation. Calcium hydroxide is added to the mother liquor to a level of at least 90% of saturation. b) Preparing an acid solution comprising water and two or more acids selected from the group consisting of; C.sub.2-C.sub.6 mono-, di- and/or tri-carboxylic acids, and optionally a phosphorous compound. The temperature of said acid solution is adjusted to 20-90 C. 31 and comprising acids to a level of at least 50% of saturation. c) The mother liquor, comprising calcium hydroxide, obtained from step a) is subjected to intense agitation under which the acid solution obtained from step b) is slowly added to said mother liquor allowing reaction to form salt until supersaturation is achieved while maintaining PH at a level securing that no unreacted acids remains after reaction, d) Crystals formed in the reaction of step c) is continuously or discontinuously removed from the reaction product of step c).