Patent classifications
C07C68/08
PURIFICATION OF AROMA CHEMICALS
The presently claimed invention relates to a process for purification of aroma compounds by distillation. Specifically, it relates to a process for purification of carbonic esters of formula (I) using a combination of distillative processes.
PURIFICATION OF AROMA CHEMICALS
The presently claimed invention relates to a process for purification of aroma compounds by distillation. Specifically, it relates to a process for purification of carbonic esters of formula (I) using a combination of distillative processes.
ORGANIC CARBONATE PRODUCTION PROCESS
The present invention relates to a process for preparing an organic carbonate, comprising contacting carbon dioxide with an alcohol in the presence of water and a catalyst in a reaction zone resulting in the production of the organic carbonate, wherein the organic carbonate is continuously removed from the reaction zone.
ORGANIC CARBONATE PRODUCTION PROCESS
The present invention relates to a process for preparing an organic carbonate, comprising contacting carbon dioxide with an alcohol in the presence of water and a catalyst in a reaction zone resulting in the production of the organic carbonate, wherein the organic carbonate is continuously removed from the reaction zone.
Diaryl carbonate and method for producing the same, and method for producing an aromatic polycarbonate resin
Disclosed are a diaryl carbonate containing a compound of the following formula (I) in an amount of less than 1,000 ppm by mass, and a method for producing the same: ##STR00001## wherein R.sup.l represents a hydrogen atom, a halogen atom, an alkyl group, an alkoxy group, an aryl group, or an aryloxy group. Disclosed methods include reacting urea with an alkyl alcohol to provide a dialkyl carbonate; reacting the dialkyl carbonate with an aryl alcohol to provide an alkylaryl carbonate; subjecting the alkylaryl carbonate to disproportionation to yield a mixture comprising a diaryl carbonate; and purifying the mixture.
Diaryl carbonate and method for producing the same, and method for producing an aromatic polycarbonate resin
Disclosed are a diaryl carbonate containing a compound of the following formula (I) in an amount of less than 1,000 ppm by mass, and a method for producing the same: ##STR00001## wherein R.sup.l represents a hydrogen atom, a halogen atom, an alkyl group, an alkoxy group, an aryl group, or an aryloxy group. Disclosed methods include reacting urea with an alkyl alcohol to provide a dialkyl carbonate; reacting the dialkyl carbonate with an aryl alcohol to provide an alkylaryl carbonate; subjecting the alkylaryl carbonate to disproportionation to yield a mixture comprising a diaryl carbonate; and purifying the mixture.
Diaryl carbonate and method for producing the same, and method for producing an aromatic polycarbonate resin
Disclosed are a diaryl carbonate containing a compound of the following formula (I) in an amount of less than 1,000 ppm by mass, and a method for producing the same: ##STR00001## wherein R.sup.l represents a hydrogen atom, a halogen atom, an alkyl group, an alkoxy group, an aryl group, or an aryloxy group. Disclosed methods include reacting urea with an alkyl alcohol to provide a dialkyl carbonate; reacting the dialkyl carbonate with an aryl alcohol to provide an alkylaryl carbonate; subjecting the alkylaryl carbonate to disproportionation to yield a mixture comprising a diaryl carbonate; and purifying the mixture.
SPIROBIINDANE DERIVATIVES AND A PROCESS FOR PREPARATION THEREOF
The present disclosure relates to spirobiindane derivatives and a process for preparation of the same. Spirobiindane derivatives are used as intermediates for many commercially important compounds such as chiral polymers. The present disclosure provides a simple and economical process for the preparation of spirobiindane derivatives of Formula (I) with high yield and having high purity.
##STR00001##
SPIROBIINDANE DERIVATIVES AND A PROCESS FOR PREPARATION THEREOF
The present disclosure relates to spirobiindane derivatives and a process for preparation of the same. Spirobiindane derivatives are used as intermediates for many commercially important compounds such as chiral polymers. The present disclosure provides a simple and economical process for the preparation of spirobiindane derivatives of Formula (I) with high yield and having high purity.
##STR00001##
PROCESS FOR THE WORK-UP AND REUSE OF SALT-CONTAINING PROCESS WATER
A process for the work-up of salt-containing process water which contains an alkali metal chloride as salt in a concentration of at least 4% by weight and organic or inorganic and organic impurities from chemical production processes and reuse of the salt by a combination of prepurification and concentration, crystallization and purification of the salt and optionally subsequently use of the salt in an electrolysis for producing basic chemicals are described.