Patent classifications
C07C201/02
CONTINUOUS SYNTHESIS OF ISOOCTYL NITRATE IN A FLOW REACTOR
A process for synthesizing isooctyl nitrate in a continuous flow reactor comprises flowing a H2SO4HNO3 mixture within a flow reactor, flowing isooctyl alcohol into said flow reactor so as to mix the isooctyl alcohol with the H2SO4HNO3 mixture and produce a reaction mixture stream flowing in said reactor, maintaining the reaction mixture stream flowing in said flow reactor at a reaction temperature within in the range 10 to 35 C. inclusive, and wherein the residence time of the reaction mixture stream in the flow reactor is greater than or equal to 5 seconds and less than or equal to 40 seconds, and wherein the H2SO4 of the H2SO4HNO3 mixture is H2SO4 having a concentration of in the range of 85 to 95% inclusive, more desirably 88 to 92% inclusive, most desirably of 90%.
Process for the preparation of a-methyl-[4-(nitro)-2-(trifluoromethyl)-benzyl nitrate
The present invention relates to a process for the preparation of -methyl-[4-(nitro)-2-(trifluoromethyl)]-benzyl nitrate and to the -methyl-[4-(nitro)-2-(trifluoromethyl)]-benzyl nitrate.
Process for the preparation of a-methyl-[4-(nitro)-2-(trifluoromethyl)-benzyl nitrate
The present invention relates to a process for the preparation of -methyl-[4-(nitro)-2-(trifluoromethyl)]-benzyl nitrate and to the -methyl-[4-(nitro)-2-(trifluoromethyl)]-benzyl nitrate.
Process for the acylation of an alpha, omega-alkanediol
The invention relates to a safe and efficient process for the for the acylation of an ,-alkanediol, which can be used in the manufacture of -nitrooxy-C.sub.3-10alkane-1-ols. The process is safer to operators and allows to obtain advantageous yields on industrial scale.
Process for the acylation of an alpha, omega-alkanediol
The invention relates to a safe and efficient process for the for the acylation of an ,-alkanediol, which can be used in the manufacture of -nitrooxy-C.sub.3-10alkane-1-ols. The process is safer to operators and allows to obtain advantageous yields on industrial scale.
Process for nitrate ester formation of an α,ω-alkanediol monoacylate
The invention relates to a safe and efficient process for the nitrate ester formation of an ,-C.sub.3-10alkanediol monoacylate. The process is safer to operators and allows to obtain advantageous yields on industrial scale.
Process for nitrate ester formation of an α,ω-alkanediol monoacylate
The invention relates to a safe and efficient process for the nitrate ester formation of an ,-C.sub.3-10alkanediol monoacylate. The process is safer to operators and allows to obtain advantageous yields on industrial scale.