C07C311/48

MULTI-ACID POLYMERS AND METHODS OF MAKING THE SAME
20170274368 · 2017-09-28 ·

A multi-acid polymer disclosed herein has the formula

##STR00001##

wherein R is one or more units of a non-SOF.sub.2 or non-SO.sub.2Cl portion of a polymer precursor in sulfonyl fluoride or sulfonyl chloride form, X is a non-sulfonyl halide group of a multi-sulfonyl halide compound having a minimum of two acid giving groups, and Y is remaining sulfonyl halide groups of the multi-sulfonyl halide compound.

MULTI-ACID POLYMERS AND METHODS OF MAKING THE SAME
20170274368 · 2017-09-28 ·

A multi-acid polymer disclosed herein has the formula

##STR00001##

wherein R is one or more units of a non-SOF.sub.2 or non-SO.sub.2Cl portion of a polymer precursor in sulfonyl fluoride or sulfonyl chloride form, X is a non-sulfonyl halide group of a multi-sulfonyl halide compound having a minimum of two acid giving groups, and Y is remaining sulfonyl halide groups of the multi-sulfonyl halide compound.

Onium salt, negative resist composition, and resist pattern forming process

A negative resist composition comprising an onium salt having formula (A) and a base polymer is provided. The resist composition exhibits a high resolution during pattern formation and forms a pattern with minimal LER. ##STR00001##

Onium salt, negative resist composition, and resist pattern forming process

A negative resist composition comprising an onium salt having formula (A) and a base polymer is provided. The resist composition exhibits a high resolution during pattern formation and forms a pattern with minimal LER. ##STR00001##

Method for handling solids capable of deflagration

Method of processing and handling solids and mixtures capable of deflagration, in particular of processing materials capable of deflagration in the chemical and pharmaceutical industry, wherein the processing and handling is carried out in an environment under a reduced pressure of ≦500 mbara and the processing and/or handling comprises one or more process steps selected from the group consisting of filtration, milling, sieving, mixing, homogenization, granulation, compacting, packaging, drying, storage and transport in a transport container and other steps in apparatuses having mechanical internals.

Method for handling solids capable of deflagration

Method of processing and handling solids and mixtures capable of deflagration, in particular of processing materials capable of deflagration in the chemical and pharmaceutical industry, wherein the processing and handling is carried out in an environment under a reduced pressure of ≦500 mbara and the processing and/or handling comprises one or more process steps selected from the group consisting of filtration, milling, sieving, mixing, homogenization, granulation, compacting, packaging, drying, storage and transport in a transport container and other steps in apparatuses having mechanical internals.

Method for preparing imide salts containing a fluorosulphonyl group
09725318 · 2017-08-08 · ·

A fluorination process for obtaining fluorinated compounds including at least one fluorosulfonyl group. More particularly, a process for preparing a fluorinated compound of formula (II), including at least one step of reacting a compound of formula (I) with anhydrous hydrofluoric acid in at least one organic solvent, in which R1 is equal to R2 except in the specific case where R1═Cl, then R2═F, and when R1 is equal to R2, R1 and R2 represent an electron-withdrawing group which has a Hammett parameter σp of greater than 0, such as F, CF.sub.3, CHF.sub.2, CH.sub.2F, C.sub.2HF.sub.4, C.sub.2H.sub.2F.sub.3, C.sub.2H.sub.3F.sub.2, C.sub.2F.sub.5, C.sub.3F.sub.7, C.sub.3H.sub.2F.sub.5, C.sub.3H.sub.4F.sub.3, C.sub.3HF.sub.6, C.sub.4F.sub.9, C.sub.4H.sub.2F.sub.7, C.sub.4H.sub.4F.sub.5, C.sub.5F.sub.11, C.sub.3F.sub.5OCF.sub.3, C.sub.2F.sub.4OCF.sub.3, C.sub.2H.sub.2F.sub.2OCF.sub.3, CF.sub.2OCF.sub.3, C.sub.6F.sub.13, C.sub.7F.sub.15, C.sub.8F.sub.17 or C.sub.9F.sub.19, and M represents a hydrogen atom, an alkali metal, an alkaline-earth metal or a quaternary ammonium cation.

Method for preparing imide salts containing a fluorosulphonyl group
09725318 · 2017-08-08 · ·

A fluorination process for obtaining fluorinated compounds including at least one fluorosulfonyl group. More particularly, a process for preparing a fluorinated compound of formula (II), including at least one step of reacting a compound of formula (I) with anhydrous hydrofluoric acid in at least one organic solvent, in which R1 is equal to R2 except in the specific case where R1═Cl, then R2═F, and when R1 is equal to R2, R1 and R2 represent an electron-withdrawing group which has a Hammett parameter σp of greater than 0, such as F, CF.sub.3, CHF.sub.2, CH.sub.2F, C.sub.2HF.sub.4, C.sub.2H.sub.2F.sub.3, C.sub.2H.sub.3F.sub.2, C.sub.2F.sub.5, C.sub.3F.sub.7, C.sub.3H.sub.2F.sub.5, C.sub.3H.sub.4F.sub.3, C.sub.3HF.sub.6, C.sub.4F.sub.9, C.sub.4H.sub.2F.sub.7, C.sub.4H.sub.4F.sub.5, C.sub.5F.sub.11, C.sub.3F.sub.5OCF.sub.3, C.sub.2F.sub.4OCF.sub.3, C.sub.2H.sub.2F.sub.2OCF.sub.3, CF.sub.2OCF.sub.3, C.sub.6F.sub.13, C.sub.7F.sub.15, C.sub.8F.sub.17 or C.sub.9F.sub.19, and M represents a hydrogen atom, an alkali metal, an alkaline-earth metal or a quaternary ammonium cation.

Functionalized choline chloride ionic liquid, preparation method thereof and use in electrochemical energy storage device

The present invention discloses a process for preparing a functionalized choline chloride ionic liquid as defined in formula (I), and thereof use in an electrochemical energy storage device, as an electrolyte solution or an additive for a lithium ion battery and a supercapacitor. The ionic liquid electrolyte material has better biocompatibility, flame retardance, high ionic conductivity, low viscosity, and wide electrochemical window. ##STR00001## wherein R.sup.1 is selected from the group consisting of: (CH.sub.2═CH—(CH.sub.2).sub.n)—, CN(CH.sub.2).sub.n—, or R.sup.2.sub.3Si—; R.sup.2 is selected from CH.sub.3—(CH.sub.2).sub.m—, n is an integer selected from 1 to 3, m is an integer selected from 0 to 2; or one of R.sup.2 is (CH.sub.3).sub.3Si—O—. Anion A in Formula I is selected from the group consisting of: Cl.sup.−, Br.sup.−, I.sup.−, BF.sub.4.sup.−, NO.sub.3.sup.−, SO.sub.4.sup.2−, CF.sub.3COO.sup.−, CF.sub.3SO.sub.3.sup.−, (CF.sub.3SO.sub.2).sub.2N.sup.−, PF.sub.6.sup.−, BF.sub.2C.sub.2O.sub.4.sup.−, or B(C.sub.2O.sub.4).sub.2.sup.−.

Functionalized choline chloride ionic liquid, preparation method thereof and use in electrochemical energy storage device

The present invention discloses a process for preparing a functionalized choline chloride ionic liquid as defined in formula (I), and thereof use in an electrochemical energy storage device, as an electrolyte solution or an additive for a lithium ion battery and a supercapacitor. The ionic liquid electrolyte material has better biocompatibility, flame retardance, high ionic conductivity, low viscosity, and wide electrochemical window. ##STR00001## wherein R.sup.1 is selected from the group consisting of: (CH.sub.2═CH—(CH.sub.2).sub.n)—, CN(CH.sub.2).sub.n—, or R.sup.2.sub.3Si—; R.sup.2 is selected from CH.sub.3—(CH.sub.2).sub.m—, n is an integer selected from 1 to 3, m is an integer selected from 0 to 2; or one of R.sup.2 is (CH.sub.3).sub.3Si—O—. Anion A in Formula I is selected from the group consisting of: Cl.sup.−, Br.sup.−, I.sup.−, BF.sub.4.sup.−, NO.sub.3.sup.−, SO.sub.4.sup.2−, CF.sub.3COO.sup.−, CF.sub.3SO.sub.3.sup.−, (CF.sub.3SO.sub.2).sub.2N.sup.−, PF.sub.6.sup.−, BF.sub.2C.sub.2O.sub.4.sup.−, or B(C.sub.2O.sub.4).sub.2.sup.−.