Patent classifications
C07C319/26
PNEUMTIC CONVEYANCE METHOD FOR METHIONINE
The present invention provides a method of airflow transportation of methionine that can minimize the crushing of methionine, which is characterized in that when methionine is transported as airflow using carrier gas, the flow state of methionine is a low concentration floating flow type, and the mixing ratio of methionine and carrier gas is in the range of 4 to 10 kg-methionine/kg-carrier gas. In the method of airflow transportation of methionine of the present invention, if the D50 of methionine is in the range of 150 to 425 m, the increase rate of the fine powder can be suppressed to 1.5% or less by maintaining the mixing ratio at 4 to 10 kg-methionine/kg-carrier gas, and can be suppressed to 1% or less by maintaining the mixing ratio at 5 to 10 kg-methionine/kg-carrier gas.
PNEUMTIC CONVEYANCE METHOD FOR METHIONINE
The present invention provides a method of airflow transportation of methionine that can minimize the crushing of methionine, which is characterized in that when methionine is transported as airflow using carrier gas, the flow state of methionine is a low concentration floating flow type, and the mixing ratio of methionine and carrier gas is in the range of 4 to 10 kg-methionine/kg-carrier gas. In the method of airflow transportation of methionine of the present invention, if the D50 of methionine is in the range of 150 to 425 m, the increase rate of the fine powder can be suppressed to 1.5% or less by maintaining the mixing ratio at 4 to 10 kg-methionine/kg-carrier gas, and can be suppressed to 1% or less by maintaining the mixing ratio at 5 to 10 kg-methionine/kg-carrier gas.
ORGANIC REACTIONS CARRIED OUT IN AQUEOUS SOLUTION IN THE PRESENCE OF A HYDROXYALKYL(ALKYL)CELLULOSE OR AN ALKYLCELLULOSE
The present invention relates to a method of carrying out an organic reaction in aqueous solution in the presence of a hydroxyalkyl(alkyl)cellulose or an alkylcellulose.
ORGANIC REACTIONS CARRIED OUT IN AQUEOUS SOLUTION IN THE PRESENCE OF A HYDROXYALKYL(ALKYL)CELLULOSE OR AN ALKYLCELLULOSE
The present invention relates to a method of carrying out an organic reaction in aqueous solution in the presence of a hydroxyalkyl(alkyl)cellulose or an alkylcellulose.
Organic reactions carried out in aqueous solution in the presence of a hydroxyalkyl(alkyl)cellulose or an alkylcellulose
The present invention relates to a method of carrying out an organic reaction in aqueous solution in the presence of a hydroxyalkyl(alkyl)cellulose or an alkylcellulose.
Organic reactions carried out in aqueous solution in the presence of a hydroxyalkyl(alkyl)cellulose or an alkylcellulose
The present invention relates to a method of carrying out an organic reaction in aqueous solution in the presence of a hydroxyalkyl(alkyl)cellulose or an alkylcellulose.
Method for Preparation of N-Acetyl Cysteine Amide and Derivatives Thereof
The present invention includes methods for making and isolating N-acetylcysteine amide, (2R,2R)-3,3-disulfanediyl bis(2-acetamidopropanamide, diNACA), intermediates and derivatives thereof comprising: contacting cystine with an alcohol and a chlorinating reagent to form an organic solution containing L-cystine dimethylester dihydrochloride; combining dried or undried L-cystine dimethylester dihydrochloride with a triethylamine, an acetic anhydride, and an acetonitrile to form a di-N-acetylcystine dimethylester; mixing dried di-N-acetylcystine dimethylester with ammonium hydroxide to form a di-N-acetylcystine amide (diNACA); and separating dried di-N-acetylcystine dimethylester into N-acetylcysteine amide with dithiothreitol, triethylamine and an alcohol.
Preparation method of polythiol for optical lenses by using metal sulfide
Provided is a preparation of a thioether-based polythiol in a high purity using a metal monosulfide for the incorporation of a thioether group, wherein the content of such components as a metal polysulfide present in the metal monosulfide is controlled to a predetermined level or lower. As a result, an optical lens of high quality with a high refractive index can be produced using the polythiol.
Preparation method of polythiol for optical lenses by using metal sulfide
Provided is a preparation of a thioether-based polythiol in a high purity using a metal monosulfide for the incorporation of a thioether group, wherein the content of such components as a metal polysulfide present in the metal monosulfide is controlled to a predetermined level or lower. As a result, an optical lens of high quality with a high refractive index can be produced using the polythiol.
Preparation method of polythiol for optical lenses by using metal sulfide
Provided is a preparation of a thioether-based polythiol in a high purity using a metal monosulfide for the incorporation of a thioether group, wherein the content of such components as a metal polysulfide present in the metal monosulfide is controlled to a predetermined level or lower. As a result, an optical lens of high quality with a high refractive index can be produced using the polythiol.