Patent classifications
C08B11/02
METHOD FOR PRODUCING MODIFIED CELLULOSE
The present invention is a method for producing a modified cellulose including the following step A: step A: introducing a cellulose raw material with a substituent having 6 or more carbon atoms to a group in which a hydrogen atom is removed from a hydroxyl group of a cellulose backbone, in the presence of water and a surfactant. The present invention relates to a method for producing a modified cellulose having a high affinity of an organic solvent, a resin or the like, and a hydrophobic medium, using a reaction system with low environmental loads and with prospects of reduction in production costs.
Method for producing water-soluble nonionic cellulose ether powder having high bulk density
Provided is a method of stably producing a water-soluble nonionic cellulose ether powder having a high bulk density at low cost by adding a minimum amount of water. More specifically provided is a method for producing a water-soluble nonionic cellulose ether powder, comprising the steps of: reacting alkali cellulose with an etherifying agent to obtain a reaction product; washing and draining the reaction product to obtain a water-soluble nonionic cellulose ether; mixing the water-soluble nonionic cellulose ether with such an amount of water of 70° C. or higher as to make a water content of the water-soluble nonionic cellulose ether become 55 to 90% by weight to obtain a water-containing water-soluble nonionic cellulose ether having a water content of 55 to 90% by weight; cooling the water-containing water-soluble nonionic cellulose ether; and drying and pulverizing the cooled water-containing water-soluble nonionic cellulose ether.
Method for producing water-soluble nonionic cellulose ether powder having high bulk density
Provided is a method of stably producing a water-soluble nonionic cellulose ether powder having a high bulk density at low cost by adding a minimum amount of water. More specifically provided is a method for producing a water-soluble nonionic cellulose ether powder, comprising the steps of: reacting alkali cellulose with an etherifying agent to obtain a reaction product; washing and draining the reaction product to obtain a water-soluble nonionic cellulose ether; mixing the water-soluble nonionic cellulose ether with such an amount of water of 70° C. or higher as to make a water content of the water-soluble nonionic cellulose ether become 55 to 90% by weight to obtain a water-containing water-soluble nonionic cellulose ether having a water content of 55 to 90% by weight; cooling the water-containing water-soluble nonionic cellulose ether; and drying and pulverizing the cooled water-containing water-soluble nonionic cellulose ether.
PROCESS FOR PRODUCING A CROSSLINKED CELLULOSE ETHER
A process for producing a crosslinked cellulose ether including contacting an activated cellulose material with (i) an aqueous crosslinking agent emulsion, wherein the aqueous crosslinking agent emulsion is a mixture of (ia) at least one crosslinking agent; (ib) water; and (ic) any other optional components desired; and (ii) at least one etherification reagent; wherein the aqueous crosslinking agent emulsion (i) and the at least one etherification reagent (ii) react with the activated cellulose material to form the crosslinked cellulose ether; and a crosslinked cellulose ether produced by the above process.
PROCESS FOR PRODUCING A CROSSLINKED CELLULOSE ETHER
A process for producing a crosslinked cellulose ether including the steps of: (a) contacting at least one cellulose material with at least one alkalization reagent to form an activated cellulose material; (b) contacting the activated cellulose material of step (a) with at least one etherification reagent to form an uncrosslinked cellulose ether; (c) subjecting the cellulose ether of step (b) to a simultaneous or stepwise washing and/or granulating step; (d) adding at least one crosslinking agent to the uncrosslinked cellulose ether during the washing and/or granulating of step (c) to form a crosslinked cellulose ether; and (e) any other optional components desired; and a crosslinked cellulose ether produced by the above process.
Hydrophobically modified chitosan compositions
Disclosed herein is a polymer composition comprising an effective amount of a hydrophobically-modified polymer having functional groups along the backbone occupied by a fatty anhydride moiety. The polymer composition has a potent hemostatic action by gelling blood upon contact, and is suitable for treating internal and external bleeds. As disclosed herein, the modified polymer can be generated without the use of toxic reagents that would require removal from the product. Further, compositions are shelf stable even in a flowable form. That is, the hydrophobic grafts are not lost under product storage conditions (e.g., room temperature storage).
FLAME-RETARDANT RESIN COMPOSITION AND METHOD FOR PRODUCING THE SAME
The present invention provides a resin composition excellent in mechanical properties, stiffness properties, appearance characteristics, flame retardancy and metal corrosion resistance and having a small environmental load, compared to those of conventional polyamide-based flame-retardant resin compositions. The present invention related to a flame-retardant resin composition, comprising: 35 to 85% by mass of a polyamide resin (A); 0.45 to 30% by mass of a cellulose fiber (B) having an average fiber diameter of 10 μm or less; 4.5 to 40% by mass of metal phosphinate (C); and 0 to 35% by mass of a reinforcing material (D) other than the cellulose fiber.
Method for producing hydroxypropyl methyl cellulose
Provided is a method for producing hydroxypropyl methyl cellulose (HPMC) having high hydroxypropoxy content, low ash content, and low insoluble fiber content. More specifically, provided is a method for producing HPMC having a methoxy degree of substitution of from 1.4 to 2.2 and a hydroxypropoxy molar substitution of from 0.5 to 1.0, including steps of: bringing sheet-like or chip-like pulp into contact with an alkali metal hydroxide solution to obtain a reaction product mixture containing alkali cellulose, removing a liquid portion from the reaction product mixture to obtain the alkali cellulose, reacting the alkali cellulose with an etherifying agent to obtain a crude HPMC, disintegrating the crude HPMC into a disintegrated crude HPMC, dispersing the disintegrated crude HPMC in water to obtain a slurry, filtering the slurry to obtain a cake, and washing the cake.
Method for producing hydroxypropyl methyl cellulose
Provided is a method for producing hydroxypropyl methyl cellulose (HPMC) having high hydroxypropoxy content, low ash content, and low insoluble fiber content. More specifically, provided is a method for producing HPMC having a methoxy degree of substitution of from 1.4 to 2.2 and a hydroxypropoxy molar substitution of from 0.5 to 1.0, including steps of: bringing sheet-like or chip-like pulp into contact with an alkali metal hydroxide solution to obtain a reaction product mixture containing alkali cellulose, removing a liquid portion from the reaction product mixture to obtain the alkali cellulose, reacting the alkali cellulose with an etherifying agent to obtain a crude HPMC, disintegrating the crude HPMC into a disintegrated crude HPMC, dispersing the disintegrated crude HPMC in water to obtain a slurry, filtering the slurry to obtain a cake, and washing the cake.
Oil-in-water type composition and food using same
An oil-in-water type composition which can provide a chewy texture both in a non-cooked state and a heated state and does not show water/oil separation, including: an alkyl cellulose, a 1% by mass aqueous solution of which has a viscosity at 20° C. of from 4,000 to 11,000 mPa.Math.s when measured with a Brookfield type viscometer and a 1.5% by mass aqueous solution of which has a storage modulus G′ (65° C.) at 65° C. of from 2,500 to 4,500 Pa; an edible oil or fat; and water. Also provided is a food using the alkyl cellulose.