A process for the oxidation of powder materials containing starch, which comprises the steps of mixing a powder material comprising starch with an aqueous solution of hydrogen peroxide (H.sub.2O.sub.2), adding to the mixture thus obtained an aqueous solution of ammonia which reacts with said mixture and drying the mixture to obtain a powder material containing oxidized starch.

A multi-stage modified thermoplastic starch (TPS) masterbatch is obtained by four-stage modification treatment as follows: (i) 100 parts of starch with a moisture content of 15% to 30% are added to a high-speed mixer and stirred under room temperature; (ii) Heated to 50° C. to 70° C., polybutadiene (PB), plasticizer and a chemical modifier are added. The mixture is then stirred a second time; (iii) Heated to 75° C. to 95° C., tackifier, lubricant, filler and chain extender are added. The mixture is again stirred a third time. (iv) A biodegradable resin is added at this temperature, and the resulting mixture is stirred a fourth time. After the stirring is completed, the resulting mixture is incubated at this temperature for a predetermined time, and then added to a twin-screw extruder for melt extrusion. The present invention also discloses a preparation method and use.

A multi-stage modified thermoplastic starch (TPS) masterbatch is obtained by four-stage modification treatment as follows: (i) 100 parts of starch with a moisture content of 15% to 30% are added to a high-speed mixer and stirred under room temperature; (ii) Heated to 50° C. to 70° C., polybutadiene (PB), plasticizer and a chemical modifier are added. The mixture is then stirred a second time; (iii) Heated to 75° C. to 95° C., tackifier, lubricant, filler and chain extender are added. The mixture is again stirred a third time. (iv) A biodegradable resin is added at this temperature, and the resulting mixture is stirred a fourth time. After the stirring is completed, the resulting mixture is incubated at this temperature for a predetermined time, and then added to a twin-screw extruder for melt extrusion. The present invention also discloses a preparation method and use.

Disclosed herein is a starch based corrugating adhesive comprising modified starch, and methods for making such corrugating adhesive. In some embodiments, the corrugating adhesive may contain a carrier component comprising a gelatinized modified starch, and a suspended component comprising a granular modified starch. In some embodiments, the granular and gelatinized modified starch may be from the same base starch. In some embodiments, the modified starch is obtained from a starch having an amylose content between about 30% and less than 40%. Also disclosed herein are corrugated materials made using the corrugating adhesives described herein.

Disclosed herein is a starch based corrugating adhesive comprising modified starch, and methods for making such corrugating adhesive. In some embodiments, the corrugating adhesive may contain a carrier component comprising a gelatinized modified starch, and a suspended component comprising a granular modified starch. In some embodiments, the granular and gelatinized modified starch may be from the same base starch. In some embodiments, the modified starch is obtained from a starch having an amylose content between about 30% and less than 40%. Also disclosed herein are corrugated materials made using the corrugating adhesives described herein.

The present invention relates to a stabilized starch obtained by reacting under alkaline conditions a base starch having a protein content of less than 0.4% w/w with a reactant capable of forming active chlorine, wherein the reactant is used in an amount sufficient to provide between 4000 and 8200 ppm of active chlorine during the stabilization reaction.

The present invention relates to a stabilized starch obtained by reacting under alkaline conditions a base starch having a protein content of less than 0.4% w/w with a reactant capable of forming active chlorine, wherein the reactant is used in an amount sufficient to provide between 4000 and 8200 ppm of active chlorine during the stabilization reaction.

A multi-stage modified thermoplastic starch (TPS) masterbatch is obtained by four-stage modification treatment as follows: (i) 100 parts of starch with a moisture content of 15% to 30% are added to a high-speed mixer and stirred under room temperature; (ii) Heated to 50° C. to 70° C., polybutadiene (PB), plasticizer and a chemical modifier are added. The mixture is then stirred a second time; (iii) Heated to 75° C. to 95° C., tackifier, lubricant, filler and chain extender are added. The mixture is again stirred a third time. (iv) A biodegradable resin is added at this temperature, and the resulting mixture is stirred a fourth time. After the stirring is completed, the resulting mixture is incubated at this temperature for a predetermined time, and then added to a twin-screw extruder for melt extrusion. The present invention also discloses a preparation method and use.

A multi-stage modified thermoplastic starch (TPS) masterbatch is obtained by four-stage modification treatment as follows: (i) 100 parts of starch with a moisture content of 15% to 30% are added to a high-speed mixer and stirred under room temperature; (ii) Heated to 50° C. to 70° C., polybutadiene (PB), plasticizer and a chemical modifier are added. The mixture is then stirred a second time; (iii) Heated to 75° C. to 95° C., tackifier, lubricant, filler and chain extender are added. The mixture is again stirred a third time. (iv) A biodegradable resin is added at this temperature, and the resulting mixture is stirred a fourth time. After the stirring is completed, the resulting mixture is incubated at this temperature for a predetermined time, and then added to a twin-screw extruder for melt extrusion. The present invention also discloses a preparation method and use.

A delivery device for an active agent comprises nanoparticles based on a biopolymer such as starch. The delivery device may also be in the form of an aptamer-biopolymer-active agent conjugate wherein the aptamer targets the device for the treatment of specific disorders. The nanoparticles may be made by applying a high shear force in the presence of a crosslinker. The particles may be predominantly in the range of 50-150 nm and form a colloidal dispersion of crosslinked hydrogel particles in water. The biopolymer may be functionalized. The aptamer may be conjugated directly to the cross-linked biopolymers. The active agent may be a drug useful for the treatment of cancer. The delivery device survives for a period of time in the body sufficient to allow for the sustained release of a drug and for the transportation and uptake of the conjugate into targeted cells. However, the biopolymer is biocompatible and resorbable.