C08F6/001

Method of preparing aromatic vinyl compound-vinyl cyanide compound polymer and apparatus for preparing the same

The present invention relates to a method of preparing an aromatic vinyl compound-vinyl cyanide compound polymer including a step of separating volatile components from a polymerization product containing an aromatic vinyl compound-vinyl cyanide compound polymer, a residual aromatic vinyl monomer, a residual vinyl cyanide monomer, and an organic solvent using a volatilization tank, and a step of condensing the separated volatile components using a condenser, wherein an organic solvent or an aromatic vinyl monomer is sprayed onto the volatile components being transferred to the condenser. Volatile components may be fully condensed in a condenser, thereby significantly reducing the amount of volatile components discharged to the outside without being condensed. Therefore, wastewater treatment costs consumed in treating the volatile components may be reduced, and the amount of vinyl cyanide monomers harmful to the human body discharged into the atmosphere may be significantly reduced.

PROCESS FOR SEPARATING COMPONENTS OF A POLYMER-MONOMER MIXTURE OBTAINED BY HIGH-PRESSURE POLYMERIZATION OF ETHYLENICALLY UNSATURATED MONOMERS

A process for separating polymeric and gaseous components of a polymer-monomer mixture at a pressure of from 0.12 MPa to 0.6 MPa and a temperature of from 120° C. to 300° C. in a separation vessel is provided. The separation vessel has a vertically arranged cylindrical shape with a ratio of length to diameter L/D of from 0.6 to 10 and an inlet pipe capable of introducing the polymer-monomer mixture into the separation vessel which the inlet pipe extends vertically from the top of the separation vessel into the separation vessel. Further a process for preparing ethylene homopolymers or copolymers from ethylenically unsaturated monomers in the presence of free-radical polymerization initiators at temperatures from 100° C. to 350° C. and pressures in the range of from 110 MPa to 500 MPa comprising such a process for separating a polymer-monomer mixture is provided.

Hydrocarbon Resin and Method for Production Thereof
20230183389 · 2023-06-15 ·

The invention relates to a method for producing a hydrocarbon resin, in which method a monomer mixture which contains an aromatic component containing indene and/or C.sub.1-4 alkylindene and a cyclic diolefin component containing a cyclic diolefin compound is polymerized by heating to a polymerization temperature of at least 180° C. to obtain a product stream containing hydrocarbon resin, wherein oligomers which contain units originating from the cyclic diolefin compound and/or units originating from the aromatic component are separated from the product stream and returned to the monomer mixture, and wherein the hydrocarbon resin is heated in an annealing step to a temperature of 150° C. to 300° C. for a period of 15 minutes to 240 hours. The invention also relates to a hydrocarbon resin that is obtainable by the method, to a hydrogenated hydrocarbon resin, and to the use of the hydrocarbon resin and the hydrogenated hydrocarbon resin.

Hydrocarbon Resin and Method for Production Thereof
20230183389 · 2023-06-15 ·

The invention relates to a method for producing a hydrocarbon resin, in which method a monomer mixture which contains an aromatic component containing indene and/or C.sub.1-4 alkylindene and a cyclic diolefin component containing a cyclic diolefin compound is polymerized by heating to a polymerization temperature of at least 180° C. to obtain a product stream containing hydrocarbon resin, wherein oligomers which contain units originating from the cyclic diolefin compound and/or units originating from the aromatic component are separated from the product stream and returned to the monomer mixture, and wherein the hydrocarbon resin is heated in an annealing step to a temperature of 150° C. to 300° C. for a period of 15 minutes to 240 hours. The invention also relates to a hydrocarbon resin that is obtainable by the method, to a hydrogenated hydrocarbon resin, and to the use of the hydrocarbon resin and the hydrogenated hydrocarbon resin.

PROCESS FOR THE SEPARATION OF A STREAM COMPRISING VAPOUR AND SOLIDS IN A SEPARATION VESSEL
20170335023 · 2017-11-23 ·

The present invention relates to vapour-solids separations, and in particular provides a process for the separation of a stream comprising vapour and a stream comprising solids from a stream comprising vapour and solids using a separation vessel, said separation vessel having: a. a first inlet for the stream to be separated, b. a liquid outlet, c. a vapour outlet, d. a demister located on the vapour outlet, and e. a second inlet by which liquid can be passed to the demister said process comprising (i) passing the stream comprising vapour and solids through the first inlet and in to the separation vessel, (ii) recovering from the vapour outlet a vapour stream which comprises vapour from the stream comprising vapour and solids and which vapour stream has passed through the demister in the separation vessel, (iii) passing to the separation vessel, via the second inlet, a first liquid stream which contacts the vapour stream in the demister, and (iv) recovering from the liquid outlet a second liquid stream which comprising the solids from the stream comprising vapour and solids, and liquid from the first liquid stream.

PROCESS FOR THE SEPARATION OF A STREAM COMPRISING VAPOUR AND SOLIDS IN A SEPARATION VESSEL
20170335023 · 2017-11-23 ·

The present invention relates to vapour-solids separations, and in particular provides a process for the separation of a stream comprising vapour and a stream comprising solids from a stream comprising vapour and solids using a separation vessel, said separation vessel having: a. a first inlet for the stream to be separated, b. a liquid outlet, c. a vapour outlet, d. a demister located on the vapour outlet, and e. a second inlet by which liquid can be passed to the demister said process comprising (i) passing the stream comprising vapour and solids through the first inlet and in to the separation vessel, (ii) recovering from the vapour outlet a vapour stream which comprises vapour from the stream comprising vapour and solids and which vapour stream has passed through the demister in the separation vessel, (iii) passing to the separation vessel, via the second inlet, a first liquid stream which contacts the vapour stream in the demister, and (iv) recovering from the liquid outlet a second liquid stream which comprising the solids from the stream comprising vapour and solids, and liquid from the first liquid stream.

Reactor for Multi-Phase Composition

A reactor comprising a first portion having a generally cylindrical housing, an inlet at one end of said first portion housing, the opposed end of said first portion housing being the outlet of said first portion, where said first portion includes a rotatable shaft positioned axially within said housing and including at least two shearing paddles extending radially from said rotatable shaft and a second portion having a generally frustoconical housing having a first end larger than a second end, said first end constituting an inlet to said second portion and coextensive with said opposed end of said first portion housing, and an outlet at said second end, where said second portion includes a rotatable shaft positioned axially within said housing and including at least one generally helical flight extending radially from said rotatable shaft.

Paraffin mixture and method for producing same
09745231 · 2017-08-29 · ·

The present invention provides a paraffin mixture that is suitable for use as cosmetics and cleansing oil for skin and hair and has excellent volatility. The paraffin mixture according to the present invention is a mixture that contains isoparaffin having a carbon number of 12 to 16, and the mixture has a boiling point range of 185° C. to 215° C. and has the content of 2,2,4,6,6-pentamethylheptane at less than 10 mass %.

Vinyl aromatic/diene-block copolymers having good organoleptic properties

The invention relates to a vinyl aromatic/diene-block copolymer A, obtained by an anionic polymerization of a monomer composition, comprising: Al: 60-95 wt.-% of at least one vinyl aromatic monomer, and A2:5-40 wt.-% of at least one diene monomer, wherein the vinyl aromatic/diene-block copolymer A in total comprises less than 10 parts per million (ppm) of acetaldehyde, methacrolein and styrene based on the total amount of vinyl aromatic/diene-block copolymer A; the vinyl aromatic/diene-block copolymer A has improved orgnoleptic properties and is in particular suitable for producing food packaging materials.

Vinyl aromatic/diene-block copolymers having good organoleptic properties

The invention relates to a vinyl aromatic/diene-block copolymer A, obtained by an anionic polymerization of a monomer composition, comprising: Al: 60-95 wt.-% of at least one vinyl aromatic monomer, and A2:5-40 wt.-% of at least one diene monomer, wherein the vinyl aromatic/diene-block copolymer A in total comprises less than 10 parts per million (ppm) of acetaldehyde, methacrolein and styrene based on the total amount of vinyl aromatic/diene-block copolymer A; the vinyl aromatic/diene-block copolymer A has improved orgnoleptic properties and is in particular suitable for producing food packaging materials.