Patent classifications
C08G63/88
PPREPARING POLYESTER COMPRISING 2,5-FURANDICARBOXYLATE UNITS WITH GERMANIUM CATALYST
A process for preparing a polyester having 2,5-furandicarboxylate units includes subjecting a starting composition including 2,5-furandicarboxylic acid and an aliphatic diol to esterification conditions to produce an ester composition and contacting the ester composition with a germanium containing solution at polycondensation conditions to produce a polyester including 2,5-furandicarboxylate units, and polyester including 2,5-furandicarboxylate units including of from 5 to 100 ppm of germanium and having a number average molecular weight of at least 30 kg/mol.
Spherical polyester resin particles and method for producing same
Spherical polyester-based resin particles characterized in that the spherical polyester-based resin particles contain a polyester-based resin and have a crystallinity of 20% or less and an average circularity of 0.96 or more. The spherical polyester-based resin particles according to the present invention can provide suitable resin particles as compounding agents for cosmetics such as foundation, antiperspirants, and skin scrubs; various agents such as matte coating agents for paints, rheology modifying agents, antiblocking agents, slipperiness-imparting agents, light diffusion agents, electroconductive agents, and diagnostic testing agents for medical use; and additives to molded articles such as automobile materials and construction materials.
USE OF UTRASOUND AND ACOUSTICS TO CONTROL CRYSTALLISATION
The use of ultrasound or acoustics applied at a level below that which causes cavitation to control the energy balance between particles and the liquid phase in a metastable liquid.
Producing a bellows
Bellows, for example, a roll bellows and a folding bellows, can be produced that can be used at higher temperatures such as those prevailing in modern articulated constructions, using a mixture comprising at least one thermoplastic elastomer selected from the group of copolysters with a hard segment and a soft segment, wherein in a first step the at least one thermoplastic elastomer is mixed with approximately 0.8 wt. % to approximately 5 wt. % triallyl isocyanurate, based on the total amount of the mixture; in a second step the bellows is produced; and in a third step, the bellows is exposed to an ionizing irradiation in a range from approximately 140 kGy to approximately 350 kGy.
Producing a bellows
Bellows, for example, a roll bellows and a folding bellows, can be produced that can be used at higher temperatures such as those prevailing in modern articulated constructions, using a mixture comprising at least one thermoplastic elastomer selected from the group of copolysters with a hard segment and a soft segment, wherein in a first step the at least one thermoplastic elastomer is mixed with approximately 0.8 wt. % to approximately 5 wt. % triallyl isocyanurate, based on the total amount of the mixture; in a second step the bellows is produced; and in a third step, the bellows is exposed to an ionizing irradiation in a range from approximately 140 kGy to approximately 350 kGy.
Method for preparing biodegradable microspheres having improved stability and storage stability
The present invention relates to a method for producing biodegradable microspheres having improved safety and storage stability, and a method for producing the same. The present invention provides a method for preparing said biodegradable microspheres while minimizing the morphological changes of microspheres and significantly reducing residual solvents.
METHOD FOR CRYSTALLIZING A POLYESTER COMPRISING AT LEAST ONE 1,4:3,6-DIANHYDROHEXITOL UNIT
The invention relates to the field of polymers and relates to a process for crystallizing polyester. More particularly, this is a crystallization process comprising a step of provision of a polyester comprising at least one 1,4:3,6-dianhydrohexitol unit, a step of provision of a coalescence-preventing additive, and a step of crystallization of said semicrystalline polyester. The process according to the invention makes it possible to greatly limit, indeed even to eliminate, the phenomenon of agglomeration of the polyester granules during the crystallization.
METHOD FOR CRYSTALLIZING A POLYESTER COMPRISING AT LEAST ONE 1,4:3,6-DIANHYDROHEXITOL UNIT
The invention relates to the field of polymers and relates to a process for crystallizing polyester. More particularly, this is a crystallization process comprising a step of provision of a polyester comprising at least one 1,4:3,6-dianhydrohexitol unit, a step of provision of a coalescence-preventing additive, and a step of crystallization of said semicrystalline polyester. The process according to the invention makes it possible to greatly limit, indeed even to eliminate, the phenomenon of agglomeration of the polyester granules during the crystallization.
Preparation method for polylactic acid grafted chitosan nanowhiskers
Disclosed is a preparation method for polylactic acid grafted chitosan nanowhiskers, and belongs to the technical field of materials. The preparation method of the disclosure is that after lactide, a catalyst and chitosan are uniformly mixed, polymerization grafting is performed to prepare PLA-g-CS, and then the PLA-g-CS is dispersed into an alkali liquor to obtain nanowhiskers by a repeated freezing/unfreezing method, with no solvent used in a polymerization grafting process. The method has advantages that the nanowhiskers can be prepared from the PLA-g-CS without a good solvent, and the whole reaction is efficient, clean, and environmentally friendly.
RECYCLED PET BLEND PROCESSING METHOD
A recycled poly(ethylene terephthalate) (rPET) blend processing method includes steps: adding a compatibilizer having a porous carbon structure to an rPET blend, wherein the rPET blend includes at least one of PET/PE blend plastic materials and PET/PP blend plastic materials; the porous carbon structure has a diameter ranging from 300 nm to 10 μm and a specific surface area of 300-1500 square meters per gram; mixing the compatibilizer and the rPET blend homogeneously to form a mixture; granulating the mixture to obtain mixture granules; and performing a pre-crystallization process and a solid-state polymerization process of the mixture granules, whereby to recycle and reuse the rPET hard to separate originally and reused, increase the crystallinity of the rPET, and raise the IV value to 0.6 and above.