A method of making a homogeneous mixture of polyolefin solids and a particulate solid additive without melting the polyolefin solids or the particulate solid additive during the making. The method comprises applying acoustic energy at a frequency of from 20 to 100 hertz to a heterogeneous mixture comprising the polyolefin solids and the particulate solid additive for a period of time sufficient to substantially intermix the polyolefin solids and the particulate solid additive together and while maintaining temperature of the heterogeneous mixture below the melting point of the at least one particulate solid additive and below the melting temperature of the polyolefin solids, thereby making the homogeneous mixture without melting the polyolefin solids or the at least one particulate solid additive.

A modified collagen fiber preparation method and application are provided. The modified collagen fiber is prepared by modifying a collagen fiber with a plant tannin; and a method of the preparation includes: mixing the plant tannin with the collagen fiber in a liquid environment with a pH of 5 to 8 to allow a reaction, and washing and drying a product. In the present disclosure, a plant tannin rich in phenolic hydroxyl can be combined with a collagen fiber in various ways such as multi-point hydrogen bonding and hydrophobic bonding, such that the plant tannin structure is introduced into a natural multi-layer micro/nano-structure of the collagen fiber; and due to a large number of phenolic hydroxyl structures in the plant tannin, the collagen fiber introduced with the plant tannin structure shows improved compatibility with a waterborne resin, and can produce strong hydrogen bonding with polar groups in the waterborne resin.

A heat-treated non-oriented principal film including a cast (co)polymeric component that is not capable of thermally-induced self-forming. The heat-treated principal film has first and second opposed major faces and at least one modification zone on the first major face, each modification zone including a central portion and a rim portion surrounding the central portion. Each rim portion is surrounded by a land portion. An average thickness of each rim portion is greater than an average thickness of the land portion surrounding each modification zone, and an average thickness of each central portion is less than the average thickness of the land portion, or zero. The first major face of the heat-treated principal film may be positioned in contact with an oriented carrier film including a molecularly-oriented (co)polymer that exhibits a relaxation temperature (T.sub.r). Methods of making such films and hand-tearable adhesive articles including such films are also disclosed.

The present invention is a composite stretchable film including: a surface film which is a cured product of a polyurethane 1 containing a copolymer of one or more of units “a1” to “a4” and silicone-pendant type urethane units “b1” and/or “b2” represented by the following general formula (1); and an inner film which is a cured product of a polyurethane 2 containing a unit “c” having polyether and urethane bonds represented by the following general formula (2), on which the surface film is laminated. The present invention provides a stretchable film that has excellent stretchability and strength, with the film surface having excellent water repellency, and a method for forming the same. ##STR00001##

A method for altering polymer properties for the molding of parts comprises exposing, to a scission-causing stressor, a region of a polymer form. The scission-causing stressor is controlled to achieve, in a relatively higher molecular-weight polymer at the region, an amount of scission that results in a reduction in the molecular weight of the relatively higher molecular-weight polymer, thereby forming a relatively lower molecular-weight polymer at the region.

The present invention provides: a highly transparent optical member which is formed from a silicone resin or a silicone rubber, and which has less mass change and excellent heat resistance without causing contact faults, or deterioration or contamination of the surface of other members due to adhesion to an electronic circuit or the surfaces of other members; and a production method for producing said optical member. According to the production method, the content of low-molecular-weight siloxanes D.sub.3-D.sub.20 in a optical member is reduced to an infinitesimal amount with use of a plurality of different low-molecular-weight siloxane removal steps.

A gas barrier polymer is formed by heat-curing a mixture including polycarboxylic acid and a polyamine compound, in which, in an infrared absorption spectrum, when a straight line connecting a measurement point at 1493 cm.sup.−1 and a measurement point at 1780 cm.sup.−1 is set as a baseline, an absorption intensity at 1660 cm.sup.−1 is set as I(1660), and an absorption intensity at 1625 cm.sup.−1 is set as I(1625), R represented by Equation (1) is greater than 1.

R=I(1660)/I(1625)−{−0.65×(total amine/COOH)+0.4225}  (1)

A resin-impregnated boron nitride body includes a polymer-derived boron nitride and a resin. A process for manufacturing such a resin-impregnated boron nitride body includes: polymerizing a boron nitride molecular precursor into a preceramic polymer shaping the preceramic polymer to form an infusible polymer body; submitting the polymer body to a thermal treatment to obtain a boron nitride body; impregnating the boron nitride body with a resin; and curing the resin.

The present invention is directed to dirt and anti-microbial resistant articles that include a substrate, a powder coating applied to the substrate, the powder coating may include a cross-linked polymeric binder. The powder coating may include a blend of metal borate and a sulfur-containing benzimidazole compound, wherein the metal borate and sulfur-containing benzimidazole compound are present in a weight ratio ranging from about 75:1 to about 10:1. The powder coating may include fluorosurfactant and a fluorosurfactant may be applied to the powder coating in an amount ranging from about 0.01 g/m.sup.2 to about 4 g/m.sup.2. The powder coating may be formed using a liquid-based fluorosurfactant.

A self-assembled film forming composition for forming a phase-separated structure of a block copolymer layer on a substrate, containing a block copolymer and a solvent, and is configured such that: the block copolymer is obtained by bonding a silicon-free polymer to a silicon-containing polymer that contains, as a constituent unit, styrene that is substituted by a silicon-containing group; the silicon-free polymer contains a structure derived from formula [1-1] or formula [1-2]; and the silicon-containing group contains one silicon atom. [In formula [1-1] or formula [1-2], each of R.sup.1 and R.sup.2 independently represents a hydrogen atom, a halogen atom or an alkyl group having 1-10 carbon atoms; and each of R.sup.3-R.sup.5 independently represents a hydrogen atom, a hydroxy group, a halogen atom, an alkyl group having 1-10 carbon atoms, an alkoxy group having 1-10 carbon atoms, a cyano group, an amino group, an amide group or a carbonyl group.]