Patent classifications
C08J11/02
METHODS FOR PRODUCING SYNTHETIC OLIGONUCLEOTIDES AND REMOVAL AGENTS FOR REMOVING IMPURITIES FROM ORGANIC WASH SOLVENTS USED IN OLIGONUCLEOTIDE SYNTHESIS
The present invention provides methods for utilizing blended compositions of acetonitrile and toluene as organic wash solvents in the production of a synthetic oligonucleotide, the blended compositions producing higher synthetic oligonucleotide yields than a pure acetonitrile wash solvent. The method also provides a process for removing one or more impurities from the acetonitrile and toluene containing wash solvent received as a waste stream from the oligonucleotide synthesis process. The process includes adding at least one of an iodine reactive compound, a sulfur reactive compound and/or an acidic reactive compound to the waste stream, and fractionating the waste stream. The fractionation produces an overhead fraction and a bottom fraction where the overhead fraction includes the acetonitrile and the toluene, and the bottom fraction includes the one or more impurities.
Process for recovering valuables from vent gas in polyolefin production
A process for recovering valuables from vent gas in polyolefin production is disclosed. The process includes a compression cooling separation step, a heavy hydrocarbon separation step, a light hydrocarbon separation step, a N.sub.2 purification step, and a turbo expansion step in sequence. The N.sub.2 purification step comprises a membrane separation procedure. The light hydrocarbon separation step comprises at least one gas-liquid separation procedure. A first gas, which is obtained by the gas-liquid separation procedure and is heated through heat exchange with multiple streams in the light hydrocarbon separation step, enters the heavy hydrocarbon separation step and is further heated; the heated first gas then enters the N.sub.2 purification step; a first generated gas, which is obtained by the membrane separation procedure of the N.sub.2 purification step, enters the heavy hydrocarbon separation step and the light hydrocarbon separation step in sequence, and is cooled through heat exchange with multiple streams in the heavy hydrocarbon separation step and the light hydrocarbon separation step; and then the cooled first generated gas enters the turbo expansion step. The energy consumption of a compressor can be greatly reduced. An external cooling medium with a temperature lower than an ambient temperature is not needed. The purity and recovery of N.sub.2 and hydrocarbons can be improved, which can facilitate reduction of energy consumption of a whole system, an investment, and a material consumption.
Solvent Separation Apparatus and Solvent Separation Method
The present invention relates to a solvent separation apparatus and a solvent separation method, and the solvent separation apparatus and the solvent separation method according to the present application can reduce the used amount of cooling water and the used amount of steam, in a process of separating a polymer and a solvent.
Solvent Separation Apparatus and Solvent Separation Method
The present invention relates to a solvent separation apparatus and a solvent separation method, and the solvent separation apparatus and the solvent separation method according to the present application can reduce the used amount of cooling water and the used amount of steam, in a process of separating a polymer and a solvent.
Catalyst complex and method of degradation of a polymer material
A catalyst complex for catalysis of degradation of a polymer material is described. Said complex comprises a magnetic particulate body containing iron oxide at its surface with an average diameter of 150-450 nm, and a plurality of catalytic groups grafted onto the iron oxide surface of the magnetic particulate body, which catalytic groups comprise a bridging moiety and a catalyst entity, wherein the bridging moiety comprises a functional group for adhesion or bonding to the iron oxide surface and a linking group towards the catalyst entity, and wherein the catalyst entity comprises a positively charged aromatic heterocycle moiety, and a negatively charged moiety for balancing the positively charged aromatic moiety.
Catalyst complex and method of degradation of a polymer material
A catalyst complex for catalysis of degradation of a polymer material is described. Said complex comprises a magnetic particulate body containing iron oxide at its surface with an average diameter of 150-450 nm, and a plurality of catalytic groups grafted onto the iron oxide surface of the magnetic particulate body, which catalytic groups comprise a bridging moiety and a catalyst entity, wherein the bridging moiety comprises a functional group for adhesion or bonding to the iron oxide surface and a linking group towards the catalyst entity, and wherein the catalyst entity comprises a positively charged aromatic heterocycle moiety, and a negatively charged moiety for balancing the positively charged aromatic moiety.
METHOD FOR PURIFYING BIODEGRADABLE POLYMERS
The present disclosure relates to a process for obtaining an ultrapure polymer by simply and effectively removing unreacted residual monomer in polymer, which is generated during production of a biodegradable polymer such as polylactic acid or derivatives thereof.
Olefinic Monomer Recovery Apparatus
The present invention relates to an olefinic monomer recovery device capable of suppressing fouling and pressure drop in the recovery device in a process of separating and recovering unreacted monomers after production of a polyolefin resin. The olefinic monomer recovery device is used for separating and recovering unreacted olefinic monomers after production of a polyolefin resin, the apparatus comprising a vertical-type heat exchange unit, and a knock-out drum unit.
Olefinic Monomer Recovery Apparatus
The present invention relates to an olefinic monomer recovery device capable of suppressing fouling and pressure drop in the recovery device in a process of separating and recovering unreacted monomers after production of a polyolefin resin. The olefinic monomer recovery device is used for separating and recovering unreacted olefinic monomers after production of a polyolefin resin, the apparatus comprising a vertical-type heat exchange unit, and a knock-out drum unit.
Process to form oil containing ethylene-based polymers
The invention provides a process to form a composition comprising at least one ethylene-based polymer and at least one oil, said process comprising the following: polymerizing a mixture comprising ethylene, and optionally one or more comonomers, in a reactor system, comprising at least one reactor and at least one mixer, located downstream from the reactor, to form the ethylene-based polymer; and wherein the oil is added to the ethylene-based polymer upstream of the mixer. The invention also provides a reactor system for a process to form a composition comprising at least one ethylene-based polymer and at least one oil, said reactor system comprising at least one reactor, at least one mixer, and an oil feed into the ethylene-based polymer, and wherein the oil feed is located after the reactor and before the mixer.