The invention concerns a continuous flow process for manufacturing surface modified metal oxide nanoparticles by supercritical solvothermal synthesis in an reaction medium flowing within a continuous flow chamber, said continuous flow chamber containing a hydrolysis area and a supercritical area, said process comprising the introduction of a flow of metal oxide precursor into the continuous flow chamber at a point P located in the hydrolysis area or in the supercritical area, and the introduction of a flow of is located downstream of P1 with respect to the flow direction, as well as the device for carrying out this process.

The invention concerns a continuous flow process for manufacturing surface modified metal oxide nanoparticles by supercritical solvothermal synthesis in an reaction medium flowing within a continuous flow chamber, said continuous flow chamber containing a hydrolysis area and a supercritical area, said process comprising the introduction of a flow of metal oxide precursor into the continuous flow chamber at a point P located in the hydrolysis area or in the supercritical area, and the introduction of a flow of is located downstream of P1 with respect to the flow direction, as well as the device for carrying out this process.

The purpose of the present invention is to provide a composite pigment which can be dispersed and made into paint in a manner that saves labor compared with conventional flat emulsion paints, and which can achieve concealing properties and low glossiness (a luster reduction effect) without separately adding a matting agent. This composite pigment contains an inorganic compound and/or an organic compound, and a fixed extender pigment.

The purpose of the present invention is to provide a composite pigment which can be dispersed and made into paint in a manner that saves labor compared with conventional flat emulsion paints, and which can achieve concealing properties and low glossiness (a luster reduction effect) without separately adding a matting agent. This composite pigment contains an inorganic compound and/or an organic compound, and a fixed extender pigment.

A process for producing hydrophobic and reactive, inorganic and/or organic fillers, including the steps of: (a) providing a filler having a defined surface area, (b) mixing the filler with the solution of at least one hydrophobizing and activating, biologically based reactive compound in a mixing assembly in an amount of 0.15×10-2 to 5.0×10-2 g per m2 filler surface area at a speed of 20 rpm to 200 rpm for 12 minutes to 120 minutes, (c) evacuating the hydrophobized and activated, inorganic and/or organic filler in a storage bag, a box or a drum, or directly in the casting compound.

There are provided a silyl-terminated resin composition and a method for producing the same, the silyl-terminated resin composition being superior in storage stability before curing and providing a cured product which has a low initial modulus and can maintain the low modulus even after a heat-accelerated test. The silyl-terminated resin composition comprises a surface-treated calcium carbonate and a silyl-terminated resin, wherein the surface-treated calcium carbonate is obtained by surface-treating calcium carbonate having a BET specific surface area in the range of 1 m.sup.2/g to 60 m.sup.2/g with a fatty acid, and has an alkali metal content in the range of 500 μg/g to 2000 μg/g and the free fatty acid as determined by ethanol extraction in the range of 1.8 to 2.5% by mass.

There are provided a silyl-terminated resin composition and a method for producing the same, the silyl-terminated resin composition being superior in storage stability before curing and providing a cured product which has a low initial modulus and can maintain the low modulus even after a heat-accelerated test. The silyl-terminated resin composition comprises a surface-treated calcium carbonate and a silyl-terminated resin, wherein the surface-treated calcium carbonate is obtained by surface-treating calcium carbonate having a BET specific surface area in the range of 1 m.sup.2/g to 60 m.sup.2/g with a fatty acid, and has an alkali metal content in the range of 500 μg/g to 2000 μg/g and the free fatty acid as determined by ethanol extraction in the range of 1.8 to 2.5% by mass.

Provided is an ink for use in electronic component production making use of screen printing, which is suitable for actually allowing fine lines with high precision to be drawn in screen printing, and for actually allowing successive screen printing operations to be performed. The ink for screen printing of the present invention includes surface-modified silver nanoparticles (A) and a solvent (B), and has a viscosity at a shear rate of 10 (1/s) and 25° C. of 60 Pa.Math.s or more. The surface-modified silver nanoparticles (A) each include a silver nanoparticle and an amine-containing protective agent coating the silver nanoparticle. The solvent (B) includes at least a terpene solvent. In solvent (B), a content of solvents having a boiling point of less than 130° C. is 20 wt % or less based on the total amount of solvents.

Provided is an ink for use in electronic component production making use of screen printing, which is suitable for actually allowing fine lines with high precision to be drawn in screen printing, and for actually allowing successive screen printing operations to be performed. The ink for screen printing of the present invention includes surface-modified silver nanoparticles (A) and a solvent (B), and has a viscosity at a shear rate of 10 (1/s) and 25° C. of 60 Pa.Math.s or more. The surface-modified silver nanoparticles (A) each include a silver nanoparticle and an amine-containing protective agent coating the silver nanoparticle. The solvent (B) includes at least a terpene solvent. In solvent (B), a content of solvents having a boiling point of less than 130° C. is 20 wt % or less based on the total amount of solvents.

To provide a powder coating material capable of forming a film excellent in metallic hue, concealing property and weather resistance. The powder coating material comprises the following fluororesin (A), the following resin (B) and the following pigment (C) as constituents thereof, wherein the content of the pigment (C) is from 0.7 to 23 mass %; Fluororesin (A): a fluororesin having a fluorine content of at least 10 mass %; Resin (B): a resin having a SP value larger than that of the fluororesin (A), and the difference between the SP value thereof and the SP value of the fluororesin (A) is at least 0.4 (J/cm.sup.3).sup.1/2; Pigment (C): a pigment which is a metallic pigment covered with a covering material, and the SP value of the covering material exceeds the SP value of the fluororesin (A) and less than the SP value of the resin (B).