Disclosed are methods for preparing a high-viscosity non-hazardous bitumen composition for transportation in a railcar, wherein the method may include: (a) providing to a fractionator system a low-viscosity bitumen composition previously residing in a pipeline having a first viscosity and comprising a miscible blend of hydrocarbons, which blend was prepared by mixing a first diluent composition with a first bitumen composition; (b) heating the low-viscosity bitumen composition in the fractionator system at an operating temperature of from 170 C to 232 C to provide a first light fraction and a first heavy fraction; (c) removing at least a portion of the first heavy fraction from the fractionator system, wherein the first heavy fraction has a second viscosity that is higher than the first viscosity; (d) forming a high-viscosity non-hazardous bitumen composition from at least a portion of the first heavy fraction; and (e) directing the high-viscosity non-hazardous bitumen composition to a railcar.

Mesophase pitch compositions may be obtained by subjecting isotropic pitch compositions to heat-treatment. Methods for producing mesophase pitch compositions may comprise heat treating an isotropic pitch composition comprising two or more aromatic classes linked with at least one methylene bridge between each aromatic classes, at a temperature of about 300? C. to about 500? C. to produce a mesophase pitch composition having a weight average molecular weight of about 300 g/mol to about 2,000 g/mol, a softening point of about 100? C. or greater, a mesophase content of about 0.01 vol % to 100 vol %, based on the total volume of the mesophase pitch composition, and a micro carbon residue of about 25 wt % or greater, based on the total weight of the mesophase pitch composition; wherein heat treating induces cyclization between at least two of the two or more aromatic classes to form one or more 5-membered rings and/or 6-membered rings.

Methods are provided to prepare a low sulfur fuel from hydrocarbon sources, such as light tight oil and high sulfur fuel oil, often less desired by conventional refiners, who split crude into a wide range of differing products and may prefer presence of wide ranges (C3 or C5 to C20 or higher) of hydrocarbons. These fuels can be produced by separating feeds into untreated and treated streams, and then recombining them. Such fuels can also be formulated by combinations of light, middle and heavy range constituents in a selected manner as claimed. Not only low in sulfur, the fuels of this invention are also low in nitrogen and essentially metals free. Fuel use applications include on-board large marine transport vessels but also on-shore for large land based combustion gas turbines, boilers, fired heaters and transport vehicles and trains.

A CIR train that is adapted to traverse a roadway of asphalt pavement in order to recycle and repair the asphalt pavement includes a milling machine for removing asphalt paving material from the roadway. The CIR train also includes an asphalt cement supply tank and a mechanism for dispensing asphalt cement onto asphalt paving material that has been removed from the roadway. A heater is in fluid communication with the asphalt cement supply tank and the mechanism for dispensing asphalt cement on the asphalt paving material that has been removed from the roadway. The heater is adapted to heat the asphalt cement from the asphalt cement supply tank prior to said asphalt cement being dispensed on the asphalt paving material that has been removed from the roadway.

Methods are provided to prepare a low sulfur fuel from hydrocarbon sources, such as light tight oil and high sulfur fuel oil, often less desired by conventional refiners, who split crude into a wide range of differing products and may prefer presence of wide ranges (C3 or C5 to C20 or higher) of hydrocarbons. These fuels can be produced by separating feeds into untreated and treated streams, and then recombining them. Such fuels can also be formulated by combinations of light, middle and heavy range constituents in a selected manner as claimed. Not only low in sulfur, the fuels of this invention are also low in nitrogen and essentially metals free. Fuel use applications include on-board large marine transport vessels but also on-shore for large land based combustion gas turbines, boilers, fired heaters and transport vehicles and trains.

An integrated method for mesophase pitch and petrochemicals production. The method including supplying crude oil to a reactor vessel; heating the crude oil in the reactor vessel to a predetermined temperature for a predetermined amount of time; reducing asphaltene content in the crude oil by allowing polymerization reactions to occur in the reactor vessel at an elevated pressure in the absence of oxygen; producing a three-phase upgraded hydrocarbon product comprising gas, liquid, and solid hydrocarbon components, where the liquid hydrocarbon component comprises deasphalted oil and the solid hydrocarbon component comprises mesophase pitch; separating the gas, liquid, and solid hydrocarbon components; directly utilizing the liquid hydrocarbon component for petrochemicals production; and directly utilizing the solid hydrocarbon component for carbon artifact production.

A method for preparing a paving material includes heating an aggregate comprising recycled asphalt pavement using an emitter generating electromagnetic radiation having a wavelength of from 2 microns to 1 millimeter. The method utilizes solid phase autoregenerative cohesion to prepare a material suitable for use as an aggregate in a hot mix asphalt pavement installation.

The use of recycled materials can have significant economic value. With the increasing quantity of recycled material used in viscoelastic materials, especially asphalt mixture, understanding how they interact with original materials to produce a mixture that performs successfully, becomes critical. Currently, the technology to determine the effect of additives on the performance of asphalt mixture is lacking. The present invention relates to a new unified methodology for mechanical testing of asphalt mixture and other viscoelastic materials that improves the current practice in speed, convenience, and accuracy. A new improved specimen mounting method on Dynamic Shear Rheometer (DSR), a new recovery method for fine portion of asphalt mixture, and three new tests for the performance of recovered material using DSR is disclosed. The new methods provide performance grading of asphalt mixtures that is new to the industry and provide necessary tools for determining the effect of recycled materials on performance.

A method for producing mesophase pitch includes the steps of flushing a vessel with an at least substantially inert gas to remove air and oxygen from the vessel; charging the vessel with a hydrocarbon feed; pressurizing the vessel to an initial increased pressure; heating the vessel to a pre-determined temperature; and maintaining the vessel at the pre-determined temperature for an amount of time operable to upgrade the hydrocarbon feed to a product comprising mesophase pitch.

Disclosed are methods for preparing a high-viscosity non-hazardous bitumen composition for transportation in a railcar, wherein the method may include: (a) providing to a fractionator system a low-viscosity bitumen composition previously residing in a pipeline having a first viscosity and comprising a miscible blend of hydrocarbons, which blend was prepared by mixing a first diluent composition with a first bitumen composition; (b) heating the low-viscosity bitumen composition in the fractionator system at an operating temperature of from 170 C to 232 C to provide a first light fraction and a first heavy fraction; (c) removing at least a portion of the first heavy fraction from the fractionator system, wherein the first heavy fraction has a second viscosity that is higher than the first viscosity; (d) forming a high-viscosity non-hazardous bitumen composition from at least a portion of the first heavy fraction; and (e) directing the high-viscosity non-hazardous bitumen composition to a railcar.