The present invention relates to a grease composition which can impart excellent durability to a bearing used under a high-speed rotation condition with a DN value of 100,000 or more, wherein the grease composition contains a base oil (A) and a urea-based thickener (B), and particles containing the urea-based thickener (B) in the grease composition satisfy requirement (I) that the particles have an arithmetic mean particle diameter of 2.0 μm or less on an area basis when measured by a laser diffraction scattering method. The grease composition is used for a bearing used under a high-speed rotation condition with a DN value of 100,000 or more.

This disclosure relates to a lubricant powder composition that is made from a combination of wax, grease thickener, and additives. The lubricant powder composition exhibits low frictional, and improved mechanical stability in high temperature environments. This disclosure further relates to the use of a lubricant powder composition in a mechanical component.

This disclosure relates to a lubricant powder composition that is made from a combination of wax, grease thickener, and additives. The lubricant powder composition exhibits low frictional, and improved mechanical stability in high temperature environments. This disclosure further relates to the use of a lubricant powder composition in a mechanical component.

A lubricating oil composition for an internal combustion engine has a HTHS viscosity at 150° C. of 2.55-2.84 mPa.Math.s and includes: (A) a lubricating base oil including (a) mineral base oil(s) and/or (a) synthetic base oil(s), and having a kinematic viscosity at 100° C. of 3.8-4.6 mm.sup.2/s; (B) 1000-2000 mass ppm, in terms of metal content, of a metallic detergent including (a) metal salicylate detergent(s), and delivering 10 mmol/kg of total salicylate soap base per kilogram of the composition; (C) 1.0 to 4.0 mass % of a comb-shaped poly(meth)acrylate having a Mw of 350,000-1,000,000 and a PDI of ≤4.0; and (D) 100-1000 mass ppm, in terms of nitrogen, of a succinimide dispersant including (i) (a) non-modified succinimide dispersant(s) and/or (ii) (a) boric acid-modified succinimide dispersant(s), wherein the (i) and the (ii), in total, deliver 70 mass % of total nitrogen content of the component (D).

A lubricating oil composition for an internal combustion engine has a HTHS viscosity at 150° C. of 2.55-2.84 mPa.Math.s and includes: (A) a lubricating base oil including (a) mineral base oil(s) and/or (a) synthetic base oil(s), and having a kinematic viscosity at 100° C. of 3.8-4.6 mm.sup.2/s; (B) 1000-2000 mass ppm, in terms of metal content, of a metallic detergent including (a) metal salicylate detergent(s), and delivering 10 mmol/kg of total salicylate soap base per kilogram of the composition; (C) 1.0 to 4.0 mass % of a comb-shaped poly(meth)acrylate having a Mw of 350,000-1,000,000 and a PDI of ≤4.0; and (D) 100-1000 mass ppm, in terms of nitrogen, of a succinimide dispersant including (i) (a) non-modified succinimide dispersant(s) and/or (ii) (a) boric acid-modified succinimide dispersant(s), wherein the (i) and the (ii), in total, deliver 70 mass % of total nitrogen content of the component (D).

The present invention relates to a process for preparing a residual base oil from a hydrocarbon feed which is derived from a Fischer-Tropsch process, the process comprises the steps of: (a) providing a hydrocarbon feed which is derived from a Fischer-Tropsch process; (b) subjecting the hydrocarbon feed of step (a) to a hydrocracking/hydroisomerisation step to obtain an at least partially isomerised product; (c) separating at least part of the at least partially isomerised product as obtained in step (b) into one or more lower boiling fractions and a hydrowax residue fraction; (d) catalytic dewaxing of the hydrowax residue fraction of step (c) to obtain a highly isomerised product; (e) separating the highly isomerised product of step (d) into one or more light fractions and a isomerised residual fraction; (f) mixing of the isomerised residual fraction of step (e) with a diluent to obtain a diluted isomerised residual fraction; (g) cooling the diluted isomerised residual fraction of step (f) to a temperature between 0° C. and −60° C.; (i) subjecting the mixture of step (g) to a centrifuging step at a temperature between 0° C. and −60° C. to isolate the wax from the diluted isomerised residual fraction; (j) separating the diluent from the diluted isomerised residual fraction to obtain a residual base oil.

The present invention relates to a process for preparing a residual base oil from a hydrocarbon feed which is derived from a Fischer-Tropsch process, the process comprises the steps of: (a) providing a hydrocarbon feed which is derived from a Fischer-Tropsch process; (b) subjecting the hydrocarbon feed of step (a) to a hydrocracking/hydroisomerisation step to obtain an at least partially isomerised product; (c) separating at least part of the at least partially isomerised product as obtained in step (b) into one or more lower boiling fractions and a hydrowax residue fraction; (d) catalytic dewaxing of the hydrowax residue fraction of step (c) to obtain a highly isomerised product; (e) separating the highly isomerised product of step (d) into one or more light fractions and a isomerised residual fraction; (f) mixing of the isomerised residual fraction of step (e) with a diluent to obtain a diluted isomerised residual fraction; (g) cooling the diluted isomerised residual fraction of step (f) to a temperature between 0° C. and −60° C.; (i) subjecting the mixture of step (g) to a centrifuging step at a temperature between 0° C. and −60° C. to isolate the wax from the diluted isomerised residual fraction; (j) separating the diluent from the diluted isomerised residual fraction to obtain a residual base oil.

A lubricant, including, by weight: 80-85 parts of a base oil; 1-2 parts of a methyl-silicone oil; 1-2 parts of polymethacrylate; 2-4 parts of pentaerythritol polyisobutylene succinate; 1-2 parts of di-n-butyl phosphite; 2-3 parts of butylhydroxytoluene; 2-4 parts of an ethylene-propylene copolymer; 1-2 parts of an alkenyl succinate; and 3-5 parts of copper nanoparticles. A method of preparing the lubricant includes: adding the base oil, the methyl-silicone oil, the polymethacrylate, the ethylene-propylene copolymer, the butylhydroxytoluene, the alkenyl succinate to a reactor, and stirring a resulting first mixture under normal temperature and pressure at 300-400 rpm for 3-4 hours, to yield a primary product; and adding the di-n-butyl phosphite, the pentaerythritol polyisobutylene succinate, and the copper nanoparticles to the primary product, and stirring a resulting second mixture at 150-250 rpm for 2-2.5 hours.

A lubricant, including, by weight: 80-85 parts of a base oil; 1-2 parts of a methyl-silicone oil; 1-2 parts of polymethacrylate; 2-4 parts of pentaerythritol polyisobutylene succinate; 1-2 parts of di-n-butyl phosphite; 2-3 parts of butylhydroxytoluene; 2-4 parts of an ethylene-propylene copolymer; 1-2 parts of an alkenyl succinate; and 3-5 parts of copper nanoparticles. A method of preparing the lubricant includes: adding the base oil, the methyl-silicone oil, the polymethacrylate, the ethylene-propylene copolymer, the butylhydroxytoluene, the alkenyl succinate to a reactor, and stirring a resulting first mixture under normal temperature and pressure at 300-400 rpm for 3-4 hours, to yield a primary product; and adding the di-n-butyl phosphite, the pentaerythritol polyisobutylene succinate, and the copper nanoparticles to the primary product, and stirring a resulting second mixture at 150-250 rpm for 2-2.5 hours.

The present invention provides a lubricating oil composition for automatic transmissions which comprises: 55 to 85 mass % of a Fischer-Tropsch synthetic oil with a kinematic viscosity at 100° C. of 2 to 4 mm2/s as a low-viscosity base oil; 1 to 10 mass % of an olefin copolymer 5 with a kinematic viscosity at 100° C. of 150 to 1,000 mm2/s as a high-viscosity base oil; and a polymethacrylate with a weight-average molecular weight of 10,000 to 50,000. This lubricating oil composition is such that the viscosity index of the composition is not 10 less than 190, the Brookfield viscosity is not more than 6,000 mPa.Math.s at low temperature (−40° C.), the kinematic viscosity at 100° C. is 6 to 7 mm2/s, and the rate of reduction of the kinematic viscosity after a KRL shear stability test (60° C., 20 hr) is kept to within not more 15 than 3%.