C11B3/001

Compositions for reducing acidity
10815449 · 2020-10-27 · ·

The present invention provides a composition based on a starch powder (such as flour), wheat germ, SiO.sub.2, MgO, Al.sub.2O.sub.3, Fe.sub.2O.sub.3, and K.sub.2O. This composition is extremely useful in treating acid related disorders and reducing the acidity, removing water, deodorizing, from plant oil and extending the oils shelf life of 3-5 years instead of the average one-year available.

In line degumming and neutralization of oils and fats using hydrodynamic flow-through cavitation reactors

A process for the combined degumming and neutralization of an oil containing phosphatides and FFA, the process comprising: dosing an aqueous degumming reactant into the oil to form a mixture; introducing the mixture into a first set of flow-through hydrodynamic cavitation reactors to form at the exit of the first set of flow-through hydrodynamic cavitation reactors a mixture; dosing, at the exit of the first set of flow-through hydrodynamic cavitation reactors an aqueous caustic solution into the oil to form a mixture of aqueous caustic dispersed into the oil; introducing the mixture of an aqueous caustic dispersed into the oil into a second set of flow-through hydrodynamic cavitation reactors to form a mixture of oil containing hydrated phosphatides and neutralized FFA (soaps); and separating the mixture of oil containing hydrated phosphatides and soaps to obtain an oil phase and an aqueous phase.

COMPOSITIONS COMPRISING OMEGA-3 FATTY ACIDS, 17-HDHA AND 18-HEPE AND METHODS OF USING SAME

The present invention relates to a polyunsaturated fatty acid composition comprising Omega-3 fatty acids, 17-HDHA and 18-HEPE. The composition can furthermore comprise DPA and/or an acceptable carrier and can be present in a capsule or other suitable dosage unit. The invention also relates to the process of obtaining the composition and methods for using same.

ENZYMATIC DEGUMMING OF UNREFINED TRIGLYCERIDE OIL
20200299610 · 2020-09-24 ·

The invention relates to a process for enzymatic degumming of unrefined triglyceride oil, said process comprising the following successive steps: (a) providing an unrefined triglyceride oil having a phosphorus content of at least 100 mg per kg of unrefined triglyceride oil; (b) combining the unrefined triglyceride oil with water, an acid and a phospholipase to produce an oil-in-water emulsion having a pH in the range of 2.5 to 4.5; said phospholipase being selected phospholipase A1, phospholipase A2 and combinations thereof; (c) keeping the emulsion at a temperature of 20-90 C. for at least 10 minutes; (d) introducing a base into the emulsion; and (e) separating degummed triglyceride oil from the emulsion. This enzymatic degumming process is extremely effective in removing phospholipids, including non-hydratable phospholipids (NHP), from unrefined vegetable oils and produces degummed vegetable oil in high yield.

METHODS FOR MAKING FREE FATTY ACIDS FROM SOAPS USING THERMAL HYDROLYSIS FOLLOWED BY ACIDIFICATION

Provided are methods, processes and systems for treating a soapstock. In alternative embodiments, provided are systems and methods for treating a soapstock to generate free fatty acids and/or fatty acid derivatives, e.g. fatty acid alkyl esters. In alternative embodiments, provided are systems and methods for realizing the full fatty acid yield of a soapstock by first converting substantially all of the saponifiable material in a soapstock to salts of fatty acids (soaps) and acidulating the soaps to generate free fatty acids and/or fatty acid derivatives, e.g. fatty acid alkyl esters, wherein the soapstock comprises soaps and saponifiable lipids, e.g. glycerides and/or phospholipids, and the generating of free fatty acids and/or fatty acid is achieved.

REMEDIATION OF PESTICIDES FROM AGRICULTURAL OILS

A method of remediating pesticides from an agricultural oil includes mixing a reaction solvent, a reducing agent, and an agricultural oil into a reaction mixture in a reaction vessel, controlling the temperature of the reaction mixture, producing a pre-neutralization mixture including a separation solvent, transferring the pre-neutralization mixture into a neutralization reactor that contains a neutralization agent, mixing the pre-neutralization mixture with the neutralization agent and allowing separation into an aqueous layer and a separation solvent layer, draining the aqueous layer, and distilling the separation solvent in the separation solvent layer from the remediated agricultural oils. A system has a reactor vessel, the reactor vessel having one or more inlets to allow a reducing agent, the agricultural oil, the separation solvent, and other additives as needed to produce a reaction mixture, a temperature control unit to control a temperature of the reaction mixture at a predetermined temperature for a predetermined time, a neutralization vessel fluidically connected to the reactor vessel to receive the reaction mixture from the reactor vessel, the neutralization vessel having an inlet to allow a neutralization agent to be introduced into the neutralization vessel to produce a neutralized reaction mixture, and a valve arranged at a bottom of the neutralization vessel to allow an aqueous phase of the reaction mixture to be drained from the neutralization vessel.

Non-dispersive process for oil recovery

A method of recovering one or more insoluble oils from a liquid source using one or more membrane or membrane contactors, comprising the steps of: pumping the liquid source comprising the one or more oils to the membranes or membrane contactors, contacting the liquid source with a first surface of the membrane or membrane contactors, coalescing the one or more oils within the liquid source onto the first surface of the membrane contactors, pumping one or more recovery fluids through the membrane or membrane contactors in contact with the second surface of the membrane or membrane contactors, and removing a first stream of oil coalesced from the second surface of the membranes or membrane contactors.

Method to recover free fatty acids from fats and oils

Methods for producing oil from distillers corn oil having high free fatty acid content are provided. In the method, distiller's corn oil is treated with a mixture including an alcohol to result in a low-free fatty acid oily phase and an alcohol phase. The mixture may also include an alkali. The alcohol may be a monohydric alcohol and an aqueous alcohol, such as an aqueous alcohol having a concentration of at least about 15% alcohol-by-weight. The low-free fatty acid phase may include oil and at least one impurity. The low-free fatty acid phase may be cooled, and the oil may be separated from the at least one impurity using membrane filtration.

IN LINE DEGUMMING AND NEUTRALIZATION OF OILS AND FATS USING HYDRODYNAMIC FLOW-THROUGH CAVITATION REACTORS
20200239809 · 2020-07-30 ·

A process for the combined degumming and neutralization of an oil containing phosphatides and FFA, the process comprising: dosing an aqueous degumming reactant into the oil to form a mixture; introducing the mixture into a first set of flow-through hydrodynamic cavitation reactors to form at the exit of the first set of flow-through hydrodynamic cavitation reactors a mixture; dosing, at the exit of the first set of flow-through hydrodynamic cavitation reactors an aqueous caustic solution into the oil to form a mixture of aqueous caustic dispersed into the oil; introducing the mixture of an aqueous caustic dispersed into the oil into a second set of flow-through hydrodynamic cavitation reactors to form a mixture of oil containing hydrated phosphatides and neutralized FFA (soaps); and separating the mixture of oil containing hydrated phosphatides and soaps to obtain an oil phase and an aqueous phase.

METHODS FOR MAKING FREE FATTY ACIDS AND FATTY ACID DERIVATIVES FROM MIXED LIPID FEEDSTOCKS OR SOAPSTOCKS

Provided are methods and systems for treating a soapstock. Provided are systems and methods for treating a soapstock to generate free fatty acids and/or fatty acid derivatives, and for realizing the full fatty acid yield of a soapstock by first converting substantially all of the saponifiable material in a soapstock to fatty acids and acidulating the soaps to generate free fatty acids and/or fatty acid derivatives, wherein the soapstock comprises soaps and saponifiable lipids, and the generating of free fatty acids is achieved. Provided are systems and methods for realizing the full fatty acid yield of a soapstock by first converting substantially all of the saponifiable material in a soapstock to salts of fatty acids and acidulating the soaps to generate free fatty acids and/or fatty acid derivatives, wherein the soapstock comprises soaps and saponifiable lipids, and the generating of free fatty acids is achieved.