C11B3/006

PREVENTION OF MCPDE FORMATION IN TRIACYLGLYCERIDE OILS

A method is provided for preventing or reducing the formation of monochloropropanediols (MCPDs) or monochloropropanediol esters (MCPDEs) in triacylglyceride oil, comprising the steps: (a) concentrating insoluble components in liquid triacylglyceride oil by (i) applying a 5 centrifugational force on the triacylglyceride oil whilst maintaining the triacylglyceride oil above its melting temperature; and/or (ii) allowing the insoluble components to settle by gravitational force whilst maintaining the triacylglyceride oil above its melting temperature; (b) separating the triacylglyceride oil from the insoluble components; (c) optionally applying additional refining steps and (d) applying heat treatment to the triacylglyceride oil. A purified 10 triacylglyceride oil obtainable by the method of the invention is also provided.

METHOD TO RECOVER FREE FATTY ACIDS FROM FATS AND OILS

Methods for producing oil from fats and oils having high free fatty acid content are provided. In the method, fats and oils are treated with a mixture including an alcohol to result in a low-free fatty acid oily phase and an alcohol phase. The mixture may also include an alkali. The alcohol may be a monohydric alcohol and an aqueous alcohol, such as an aqueous alcohol having a concentration of at least about 15% alcohol-by-weight. The low-free fatty acid phase may include oil and at least one impurity. The low-free fatty acid phase may be cooled, and the oil may be separated from the at least one impurity. Fats and oils amenable to such a method may include, but are not limited to, waste fats, waste oils, high acid grease, high acid tallow, sorghum heat oil, and corn oil, such as corn oil produced at an ethanol production plant.

Enzymatic method for preparation of lecithin polyunsaturated fatty acids (PUFAs)

The disclosure discloses an enzymatic method for preparation of lecithin polyunsaturated fatty acids (PUFAs), and belongs to the technical field of separation and application of enzyme. A heat treatment procedure is added after a reaction substrate is in contact with an enzyme to adjust the ratio of sn-1 lysophospholipid PUFAs to sn-2 lysophospholipid PUFAs in a reaction product and to promote the production of sn-2 lysophospholipid PUFAs, thereby promoting the production of lecithin PUFAs, which greatly increases the production efficiency of lecithin PUFAs and the lecithin PUFA content in the product. With simple operations and high reaction rate, the method can significantly increase the content of lecithin PUFAs in the product, can effectively avoid the oxidation of PUFA, and has high economic benefits and promising industrial application prospects.

Purification of triacylglyceride oils

A method for purification of a triacylglyceride oil comprising the steps: (a) admixing the triacylglyceride oil with an auxiliary trapping agent, wherein the melting temperatures of the triacylglyceride oil and the auxiliary trapping agent are substantially different, wherein the auxiliary trapping agent is soluble in the triacylglyceride oil, and wherein the auxiliary trapping agent is more polar than the triacylglyceride oil; (b) (i) crystallising the auxiliary trapping agent by cooling the mixture of step (a) below the melting temperature of the auxiliary trapping agent, wherein the auxiliary trapping agent has a higher melting temperature than the triacylglyceride oil; or (ii) crystallising the triacylglyceride oil by cooling the mixture of step (a) below the melting 10 temperature of the triacylglyceride oil, wherein the triacylglyceride oil has a higher melting temperature than the auxiliary trapping agent; and (c) separating solid and liquid phases of the product of step (b).

COMPOSITION

The present invention is related to extracts rich in polar lipids obtained or obtainable from macroalgae, microalgae, photosynthetic bacteria and/or photosynthetic organ(s) and/or tissue(s) of a plant and combinations thereof as well as their uses as emulsifiers.

COMPOSITIONS ISOLATED FROM DATE PALM TREE

Described herein are a method of preparing a vegetable oil, comprising pressing a non-fruit tissue of a date palm offshoot, as well as a vegetable oil and a polysaccharide-containing fraction obtained by such a method. Further described herein is an oil comprising esters of fatty acids, wherein at least 10 weight percent of the fatty acids are linolelaidic acid, as well as compositions comprising a variety of ingredients, such as saccharides and amino acids, as characterized herein, and a method of isolating dihydrouracil from an oil and/or composition described herein. Further described is a method of preparing a vegetable oil, comprising pressing date kernel tissue.

PURIFICATION OF RECYCLED AND RENEWABLE ORGANIC MATERIAL

A method is disclosed of purifying a recycled or renewable organic material, wherein the recycled or renewable organic material includes more than 1 ppm silicon as silicon compounds and/or more than 10 ppm phosphorous as phosphorous compounds. The method can include providing a feed of the lipid material; heat treating the organic material in presence of an adsorbent and the filtering organic material and hydrotreating the lipid material in a presence of a hydrotreating catalyst to obtain purified hydrotreated organic material having less than 20% organic material and/or less than 30% of the original phosphorous content of the organic material.

OLEAGINOUS MATERIAL EXTRACTION USING ALCOHOL SOLVENT

An oil extraction process may be performed on an oleaginous feedstock using an alcohol-based solvent, such as ethanol. In some examples, an extraction process involves conveying a material in countercurrent direction with an alcohol-based solvent to generate an extracted material and a miscella. The miscella stream is cooled (14) to form a first solvent-rich layer phase separated from a first oil-rich layer, which is then separated (18) to form a first separated oil-rich stream (100) and a first separated solvent-rich stream (102). In some examples, the first separated solvent-rich stream is recycled back to the extractor and introduced into the extractor at a location (38) different than a location (30) where fresh solvent is introduced into the extractor. Additionally or alternatively, water (103) may be introduced into the separated first oil-rich stream to form a second solvent-rich layer phase separated from a second oil-rich layer, which is then separated (20) to form a second separated oil-rich stream (104).

Apparatus and method for extracting oil from plant material

A process and apparatus for extracting plant oil from plant material by cooling an alcohol solvent to a temperature of −40° C. or lower, contacting the plant material with the cold solvent to extract plant oil to provide a solvent and plant oil mixture, heating the mixture to convert the solvent to a gaseous state to thereby separate the solvent from the plant oil, and cooling the separated gaseous solvent to a liquid to recover the solvent. The apparatus may include a heat exchanger to cool the alcohol solvent, a centrifuge configured to receive and contact a batch of plant material with the cold solvent to extract oil from the plant material to provide a solvent and oil mixture, and a programmable logic controller to monitor and control the temperature of the cold solvent, and control the centrifuge to agitate the solvent in contact with the plant material.

Prevention of MCPDE formation in triacylglyceride oils

A method is provided for preventing or reducing the formation of monochloropropanediols (MCPDs) or monochloropropanediol esters (MCPDEs) in triacylglyceride oil, comprising the steps: (a) concentrating insoluble components in liquid triacylglyceride oil by (i) applying a 5 centrifugational force on the triacylglyceride oil whilst maintaining the triacylglyceride oil above its melting temperature; and/or (ii) allowing the insoluble components to settle by gravitational force whilst maintaining the triacylglyceride oil above its melting temperature; (b) separating the triacylglyceride oil from the insoluble components; (c) optionally applying additional refining steps and (d) applying heat treatment to the triacylglyceride oil. A purified 10 triacylglyceride oil obtainable by the method of the invention is also provided.