C11B3/12

METHOD FOR PREPARING BIO-OIL FROM FATTY ACID WITH HIGH ACID VALUE
20230100175 · 2023-03-30 · ·

Disclosed is a method for preparing bio-oil, which can be used as bio heavy fuel oil and bio marine oil, from a fatty acid with high acid value. The method for preparing bio-oil comprises the steps of: inputting materials comprising glycerine and a fatty acid into respective material input ports positioned in the center of a column-type reactor and esterification reacting the material comprising glycerine and fatty acid in each tray of a reaction area, thereby producing glyceride and water, wherein the column-type reactor has the plurality of trays installed inside the reactor so as to form a plurality of compartments in the vertical direction inside the reactor, openings are formed in the plurality of trays to connect the compartments which are vertically adjacent, and the openings of the adjacent compartments are alternately formed in a crisscrossing manner; obtaining the produced glyceride through a lower part of the reactor; and vaporizing the water produced by the esterification reaction, moving the water in a vapor state to a distillation area in an upper part of the reactor to separate the water from active components (reaction material and bio-oil) comprised in the vapor, allowing the separated active components to flow into the reaction area, and removing the separated water through the upper part of the reactor in a vapor state. The acid value of the glyceride is 30 mgKOH/g or lower, and the esterification reaction is performed at a reaction temperature of 200 to 250° C. and at ordinary pressure without using a catalyst.

MICROBIAL LIPID PRODUCTION UTILIZING POST-FERMENTATION INDUSTRIAL WASTE STREAM FEEDSTOCKS

The disclosure relates to the production of lipids by microbes utilizing novel post-fermentation industrial feedstocks. The post-fermentation industrial feedstocks comprise one or more inhibitory compounds, which traditionally have made the post-fermentation media unsuitable for utilization as a feedstock for microbial lipid production. In aspects, the disclosure provides oleaginous yeast capable of utilizing these post-fermentation industrial waste streams as a novel feedstock, methods of producing lipids and microbial oils utilizing these microbes and feedstock, and novel compositions produced from the methods.

Highly unsaturated fatty acid or highly unsaturated fatty acid ethyl ester with reduced environmental pollutants, and method for producing same

A highly unsaturated fatty acid or a highly unsaturated fatty acid ethyl ester that has been produced using as a feedstock oil a fat or oil that contains highly unsaturated fatty acids as constituent fatty acids and which has been reduced in the contents of environmental pollutants, wherein among the dioxins contained, polychlorinated dibenzoparadioxins (PCDDs) and polychlorinated dibenzofurans (PCDFs) are contained in amounts of less than 0.05 pg-TEQ/g and coplanar PCBs (Co-PCBs) in amounts of less than 0.03 pg-TEQ/g. Also disclosed is a method for producing the highly unsaturated fatty acid or highly unsaturated fatty acid ethyl ester by the steps of removing free fatty acids and environmental pollutants by thin-film distillation from a feedstock oil, ethyl esterifying the resulting fat or oil, and refining the same by rectification and column chromatography.

Stability of short path evaporation treated oils
11634658 · 2023-04-25 · ·

The present invention relates to a process for increasing the oxidative stability of short path evaporated oils, by adding to short-path evaporated treated oil at least one other oil. It further relates to a composition comprising short-path evaporated treated palm oil and, at least one other oil. Furthermore, it relates to the food products comprising these oils with improved oxidative stability.

Stability of short path evaporation treated oils
11634658 · 2023-04-25 · ·

The present invention relates to a process for increasing the oxidative stability of short path evaporated oils, by adding to short-path evaporated treated oil at least one other oil. It further relates to a composition comprising short-path evaporated treated palm oil and, at least one other oil. Furthermore, it relates to the food products comprising these oils with improved oxidative stability.

Solvent free process for extraction of cholesterol from milk fat

The present invention discloses solvent free process for extracting cholesterol free of impurities from milk fat. The so isolated cholesterol is useful for the further preparation of vitamin D3. The present invention further provides pharmaceutical grade cholesterol from milk fat of high purity.

METHOD FOR EXTRACTING HIGH-QUALITY KRILL OIL FROM KRILL

A method for extracting high-quality krill oil from krill includes the following steps: S1. performing extraction on krill with an organic solvent, and collecting an extracting solution; S2. adding alkaline water to the extracting solution to enable a free fatty acid to form a fatty acid salt to be separated from an oil phase, and performing oil-water phase separation and collecting the oil phase; and S3. purifying the oil phase to obtain the high-quality krill oil. In the present application, the preparation process for krill oil is optimized, organic solvent extraction and alkali refining are ingeniously combined, and process parameters are adjusted and optimized, thereby reducing the acid value of krill oil, and also ensuring the content of active ingredients such as phospholipid and astaxanthin in krill oil to the greatest extent, and improving the quality of krill oil.

AN OIL EXTRACT COMPRISING DIHOMOLINOLENIC ACID, AND A PROCESS FOR PRODUCING THE OIL EXTRACT

A solvent extraction process for extracting oil containing dihomolinolenic acid from marine macro-algae, since as ascophyllum. Harvested ascophyllum is desalted to a salt content of less than 3% by weight, and dried to a moisture content of less than 5% by weight, and is then chopped into pieces of maximum dimension not exceeding 5 mm. The desalted, dried and chopped ascophyllum is then packed into a cellulose soxhlet thimble (13) and covered with a silica glass wool. The soxhlet thimble (13) is then placed in a vessel (12) of a soxhlet apparatus (11). A solvent reservoir (15) is charged with the solvent, namely, a food grade hexane, and is evaporated from the solvent reservoir (15) and condensed in a condenser (22) above the vessel (12) and is drip-fed into the soxhlet thimble (13) for extracting the oil containing the dihomolinolenic acid from the ascophyllum. The solvent with the extracted oil entrained therein is returned to the solvent reservoir (15) and the process continues until substantially all the oil has been extracted from the ascophyllum. The oil containing the dihomolinolenic acid is then recovered from the solvent by low pressure distillation until the solvent content of the oil containing the dihomolinolenic acid has been reduced to less than 5% by weight. The oil containing the dihomolinolenic acid is then desolvated to remove the remaining solvent therefrom.

AN OIL EXTRACT COMPRISING DIHOMOLINOLENIC ACID, AND A PROCESS FOR PRODUCING THE OIL EXTRACT

A solvent extraction process for extracting oil containing dihomolinolenic acid from marine macro-algae, since as ascophyllum. Harvested ascophyllum is desalted to a salt content of less than 3% by weight, and dried to a moisture content of less than 5% by weight, and is then chopped into pieces of maximum dimension not exceeding 5 mm. The desalted, dried and chopped ascophyllum is then packed into a cellulose soxhlet thimble (13) and covered with a silica glass wool. The soxhlet thimble (13) is then placed in a vessel (12) of a soxhlet apparatus (11). A solvent reservoir (15) is charged with the solvent, namely, a food grade hexane, and is evaporated from the solvent reservoir (15) and condensed in a condenser (22) above the vessel (12) and is drip-fed into the soxhlet thimble (13) for extracting the oil containing the dihomolinolenic acid from the ascophyllum. The solvent with the extracted oil entrained therein is returned to the solvent reservoir (15) and the process continues until substantially all the oil has been extracted from the ascophyllum. The oil containing the dihomolinolenic acid is then recovered from the solvent by low pressure distillation until the solvent content of the oil containing the dihomolinolenic acid has been reduced to less than 5% by weight. The oil containing the dihomolinolenic acid is then desolvated to remove the remaining solvent therefrom.

METHODS OF REFINING A GRAIN OIL COMPOSITION

The present disclosure relates methods and systems for refining grain oil compositions using water, and related compositions produced therefrom. The present disclosure also relates to methods of using said compositions. The present disclosure also relates to methods of using grain oil derived from a fermentation product in an anti-foam composition.