C11C3/003

Methods for making free fatty acids from soaps using thermal hydrolysis followed by acidification

Provided are methods, processes and systems for treating a soapstock. In alternative embodiments, provided are systems and methods for treating a soapstock to generate free fatty acids and/or fatty acid derivatives, e.g. fatty acid alkyl esters. In alternative embodiments, provided are systems and methods for realizing the full fatty acid yield of a soapstock by first converting substantially all of the saponifiable material in a soapstock to salts of fatty acids (soaps) and acidulating the soaps to generate free fatty acids and/or fatty acid derivatives, e.g. fatty acid alkyl esters, wherein the soapstock comprises soaps and saponifiable lipids, e.g. glycerides and/or phospholipids, and the generating of free fatty acids and/or fatty acid is achieved.

Method for preparing functional edible oil rich in phytosterol esters and diglycerides

A method for preparing functional edible oil rich in phytosterol esters and diglycerides includes steps of: 1) adding a raw material: adding phytosterol, triglyceride and a molecular sieve into a reactor, wherein a ratio of the phytosterol and the triglyceride is 1:2-1:4, a molecular sieve amount is 50 g/L; heating to 50-60° C. and stirring for 30-60 min, for obtaining a pre-mixture; 2) providing non-aqueous enzymatic transesterification: adding 5-20 g/L lipase into the pre-mixture, adding 100-200 ppm antioxidant, stirring and reacting for 8-12 h with a temperature of 50-60° C. and an atmospheric pressure, stopping heating and naturally cooling to a room temperature; and 3) post-treating: after reaction, removing the lipase and the molecular sieve by centrifugation, for obtaining the functional edible oil. The functional edible oil rich in two nutritional active components is obtained by the one-step method. Products of the present invention do not need separation and purification, and operation is simple.

Malienated derivatives

This invention relates to malienated derivatives made from maleic anhydride, functionalized monomers, and one or more additional reagents, e.g., an oxygen-containing reagent (e.g., alcohol, polyol), a nitrogen-containing reagent (e.g., amine, polyamine, aminoalcohol), a metal and/or a metal compound. The invention relates to lubricants, functional fluids, fuels, dispersants, detergents and functional compositions (e.g., cleaning solutions, food compositions, etc.)

Process and apparatus for purifying a fatty mixture and related products including fuels
09738842 · 2017-08-22 · ·

There is described a process and an apparatus for purifying a mixture and related products. In particular, there is described a process and an apparatus for purifying a mixture comprising fats, oils and greases as are typically found in sewer waste. The process involves heating, acidifying and separating the mixture. The apparatus used includes a heating and separation device for separating into a solid fraction, an organic liquid fraction and an aqueous liquid fraction. Apparatus such as a three phase separation unit and a rotary vacuum filter may also be used.

SYSTEM AND METHOD FOR PROCESSING ALGAE-BASED PRODUCTS USING RECOVERED FLUE GAS HEAT
20170233678 · 2017-08-17 · ·

A method for processing algae-based products using flue gas heat includes mixing flue gas with water, receiving a heated gas in a first enclosure of a heat exchanger, receiving an algal paste in a second enclosure of the heat exchanger, introducing an organic solvent to the algal paste, extracting an algal oil and a plurality of algal shells from the algal paste by dissipating heat from the first enclosure to the second enclosure; and extracting the algal oil from the organic solvent and the algal shells.

Method for producing biofuel

The present invention provides a method for producing a biofuel that allows an animal/vegetable fat/oil raw material containing a free fatty acid to react with a lower alcohol in the presence of a solid acid catalyst, in which the consumption of the lower alcohol is reduced and the free fatty acid and the lower alcohol are selectively esterified to reform the animal/vegetable fat/oil. In this method, as a solid acid catalyst is used a catalyst selected from an SiO.sub.2/Al.sub.2O.sub.3 solid acid catalyst, an SiO.sub.2/Al.sub.2O.sub.3 solid acid catalyst with aluminum being partially introduced into mesoporous silica, an Al.sub.2O.sub.3/B.sub.2O.sub.3 solid acid catalyst, and a sulfated zirconia solid acid catalyst, with a molar ratio of the free fatty acid and the lower alcohol of 1 to 6.

Production of biodiesel and glycerin from high free fatty acid feedstocks

A system and method for the conversion of free fatty acids to glycerides and the subsequent conversion of glycerides to glycerin and biodiesel includes the transesterification of a glyceride stream with an alcohol. The fatty acid alkyl esters are separated from the glycerin to produce a first liquid phase containing a fatty acid alkyl ester rich (concentrated) stream and a second liquid phase containing a glycerin rich (concentrated) stream. The fatty acid alkyl ester rich stream is then subjected to distillation, preferably reactive distillation, wherein the stream undergoes both physical separation and chemical reaction. The fatty acid alkyl ester rich stream is then purified to produce a purified biodiesel product and a glyceride rich residue stream. The glycerin rich second liquid phase stream may further be purified to produce a purified glycerin product and a (second) wet alcohol stream. Neutralization of the alkaline stream, formed during the alkali-catalyzed transesterification process, may proceed by the addition of a mineral or an organic acid.

POWDER DISPERSANT, AND POWDER DISPERSION COMPOSITION AND COSMETIC PRODUCT CONTAINING THE SAME

A powder dispersant includes an ester compound of a polyglycerol having an average degree of polymerization of the polyglycerol, calculated from its hydroxyl value, in the range 2 to 20, a monovalent carboxylic acid or at least one derivative thereof, and a divalent carboxylic acid or at least one derivative thereof.

System and method for separating lipid based products from biomass
09718757 · 2017-08-01 · ·

Methods and systems for the production and isolation of fatty acid methyl esters (FAMEs) from a lipid source are described. The method includes extracting a lipid from a lipid source and transesterifying the lipid into a FAME. The method may also include fractionating the FAME from the system. A method of selectively transesterifying a lipid into a FAME is also described.

Processes and systems for catalytic manufacture of wax ester derivatives

Processes for transesterifying wax esters. Implementations may include: providing a feedstock including wax esters, contacting the feedstock with a lipase, and catalytically transesterifying the wax esters in the feedstock with the lipase to form a transesterified product. An oxidative stability index (OSI) of the transesterified product may be greater than an OSI of the feedstock.