C22B1/02

METHOD AND SYSTEM FOR RECYCLING LITHIUM ION BATTERIES USING ELECTROCHEMICAL LITHIUM ION PURIFICATION
20240003019 · 2024-01-04 ·

A method of recycling lithium-ion batteries includes steps of: roasting black mass from lithium-ion batteries to produce a reduced black mass, conducting simultaneous aqueous leaching and wet magnetic separation of the reduced black mass for (a) extracting soluble lithium species and (b) enriching metallic NiCo and subjecting the extracted soluble lithium species to electrochemical lithium ion purification. A system for recycling lithium ion batteries includes a roaster, an aqueous leaching and wet magnetic separator and an electrochemical lithium ion separator.

METHOD AND SYSTEM FOR RECYCLING LITHIUM ION BATTERIES USING ELECTROCHEMICAL LITHIUM ION PURIFICATION
20240003019 · 2024-01-04 ·

A method of recycling lithium-ion batteries includes steps of: roasting black mass from lithium-ion batteries to produce a reduced black mass, conducting simultaneous aqueous leaching and wet magnetic separation of the reduced black mass for (a) extracting soluble lithium species and (b) enriching metallic NiCo and subjecting the extracted soluble lithium species to electrochemical lithium ion purification. A system for recycling lithium ion batteries includes a roaster, an aqueous leaching and wet magnetic separator and an electrochemical lithium ion separator.

METHOD FOR CLEAN METALLURGY OF MOLYBDENUM
20200399738 · 2020-12-24 · ·

Disclosed is a method for clean metallurgy of molybdenum, including steps: 1) roasting molybdenite with calcium to obtain calcified molybdenum calcine, and leaching the calcified molybdenum calcine with an inorganic acid to obtain a molybdenum-containing inorganic acid leachate; 2) extracting molybdenum in the leachate with a cationic extractant to obtain an organic phase loaded with molybdyl cations and a raffinate; 3) using a hydrogen peroxide solution as a stripping agent to obtain a molybdenum stripping liquor; and 4) heating the molybdenum stripping liquor to dissociate peroxymolybdic acid therein so as to form a molybdic acid precipitate, and then calcining to obtain a molybdenum trioxide product. The method solves the problem of ammonia nitrogen wastewater production and can also be used for the enrichment and recovery of rhenium.

METHOD FOR CLEAN METALLURGY OF MOLYBDENUM
20200399738 · 2020-12-24 · ·

Disclosed is a method for clean metallurgy of molybdenum, including steps: 1) roasting molybdenite with calcium to obtain calcified molybdenum calcine, and leaching the calcified molybdenum calcine with an inorganic acid to obtain a molybdenum-containing inorganic acid leachate; 2) extracting molybdenum in the leachate with a cationic extractant to obtain an organic phase loaded with molybdyl cations and a raffinate; 3) using a hydrogen peroxide solution as a stripping agent to obtain a molybdenum stripping liquor; and 4) heating the molybdenum stripping liquor to dissociate peroxymolybdic acid therein so as to form a molybdic acid precipitate, and then calcining to obtain a molybdenum trioxide product. The method solves the problem of ammonia nitrogen wastewater production and can also be used for the enrichment and recovery of rhenium.

System for processing Red Mud and method of processing Red Mud
10851007 · 2020-12-01 · ·

A system for processing red mud comprising: a first heating section controlled to heat red mud to a first temperature; a second heating section controlled to heat the red mud to a second temperature lower than the first temperature; a crusher configured to grind the red mud to a predetermined particle size; and one or more separators for physically extracting at least iron and aluminum from the red mud.

PROCESS FOR RECOVERING VANADIUM IN THE FORM OF IRON VANADATE FROM A GASIFIER SLAG

The present disclosure relates to a process for recovering vanadium in the form of iron vanadate from a gasifier slag. The process comprises pulverizing the slag to obtain pulverized slag (2). The pulverized slag (2) is soaked in water (6) and an alkali salt (4) to obtain a slurry (8), followed by roasting the slurry in the presence of air to obtain roasted slag (12) which is leached (14) to obtain a first solution (18). The first solution (18) is heated at a temperature in the range of 60 C. to 80 C. while adding an iron salt (17) in an amount in the range of 10 wt % to 60 wt % at a pH in the range of 4 to 10, to obtain a second solid residue (21) which is dried to obtain iron vanadate (24).

PROCESS FOR RECOVERING VANADIUM IN THE FORM OF IRON VANADATE FROM A GASIFIER SLAG

The present disclosure relates to a process for recovering vanadium in the form of iron vanadate from a gasifier slag. The process comprises pulverizing the slag to obtain pulverized slag (2). The pulverized slag (2) is soaked in water (6) and an alkali salt (4) to obtain a slurry (8), followed by roasting the slurry in the presence of air to obtain roasted slag (12) which is leached (14) to obtain a first solution (18). The first solution (18) is heated at a temperature in the range of 60 C. to 80 C. while adding an iron salt (17) in an amount in the range of 10 wt % to 60 wt % at a pH in the range of 4 to 10, to obtain a second solid residue (21) which is dried to obtain iron vanadate (24).

Treatment system and method for deep utilization of dolomite resources

The invention provides a complete set of treatment system and method for deep utilization of dolomite resources. The system includes a primary calcination device, a carbon dioxide capture device, a digestion device, a carbonization separation device, a pyrolysis device and a secondary calcination device; the primary calcination device includes a dolomite calciner, a plurality of hoardings and an exhaust pipe, and an exhaust chamber is formed between the hoardings, the top of the dolomite calciner and the outer wall of the blanking bin; the exhaust chamber is in communication with the carbon dioxide capture device through the exhaust pipe; the carbonization separation device includes a carbonization reaction tank whose gas inlet is in communication with the gas outlet of the carbon dioxide capture device; and the pyrolysis device includes a pyrolysis kettle and a vacuum pump which maintains a negative pressure state in the pyrolysis kettle.

Treatment system and method for deep utilization of dolomite resources

The invention provides a complete set of treatment system and method for deep utilization of dolomite resources. The system includes a primary calcination device, a carbon dioxide capture device, a digestion device, a carbonization separation device, a pyrolysis device and a secondary calcination device; the primary calcination device includes a dolomite calciner, a plurality of hoardings and an exhaust pipe, and an exhaust chamber is formed between the hoardings, the top of the dolomite calciner and the outer wall of the blanking bin; the exhaust chamber is in communication with the carbon dioxide capture device through the exhaust pipe; the carbonization separation device includes a carbonization reaction tank whose gas inlet is in communication with the gas outlet of the carbon dioxide capture device; and the pyrolysis device includes a pyrolysis kettle and a vacuum pump which maintains a negative pressure state in the pyrolysis kettle.

METHOD FOR GOLD RECOVERY AND EXTRACTION FROM ELECTRONIC WASTE OR GOLD CONTAINING MINERALS, ORES AND SANDS

A method for recovery of gold from gold-containing materials, such as electronic waste material, minerals and sands is described. The method includes crushing the gold containing material to obtain a particulate material. The particulate material is then preheated in an oxygen-containing gas environment in a preheating zone. The method also includes mixing the oxidized particulate material with a chlorine-containing material and treating the mixture in a reaction zone. The treatment is carried out by heating the mixture to provide thermal decomposition of the chlorine-containing material and produce a chlorine-containing gas mixture, and by applying an electromagnetic field to the chlorine-containing gas mixture to provide ionization of chlorine. A volatile gold-containing chloride product, produced in the reaction zone as a result of a chemical reaction between gold and chlorine ions, is then cooled to convert the volatile gold-containing chloride product into solid phase gold-containing materials.