The treating method for a positive electrode for a non-aqueous electrolyte secondary battery is a treating method for a positive electrode for a non-aqueous electrolyte secondary battery which comprises a positive electrode having a foil containing Al and an active material which is a metal composite oxide, the method comprising: conducting a heating treatment for heating the positive electrode (heating step); melting the positive electrode using heat of reaction of the foil and the active material to obtain a molten material (melting step); and separating the molten material into a metal material containing a metal constituting the metal composite oxide and a slag (separating step). By subjecting the positive electrode to heating treatment, a reduction reaction of the positive electrode can be promoted at a low cost.

A treatment method of scrapped positive electrode slurry, includes the following steps: pretreating the scrapped positive electrode slurry to obtain a slurry solution; performing electrophoresis coagulation and filter pressing on the slurry solution to obtain a liquid phase and a solid phase; and performing gradient roasting on the solid phase to obtain a positive electrode material.

The invention relates to recovery of tin-lead solder from electronic printed circuit board scrap. The scrap is placed in a liquid-permeable and/or gas-permeable container, which is placed in a liquid or gaseous heat-transfer medium heated to or above the melting temperature of the tin-lead solder. After the tin-lead solder is melted, the heat-transfer medium is removed from the container, then, by means of rotation of the container, the melted tin-lead solder and the remains of the heat-transfer medium are removed from the container. The device comprises a hollow container, which is mounted so as to be capable of rotation and is designed in the form of a body of revolution, and is liquid-permeable and/or gas-permeable in a radial direction from the axis of rotation. The container can be designed in the form of a drum, which can be vertically displaced and has perforated side walls.

A method for recycling copper-indium-gallium-selenium (CIGS) waste is provided, comprising: vacuum distilling the CIGS waste to separate out selenium and obtain a distillation residue; electrolyzing the distillation residue to obtain copper and a remaining electrolyte containing indium and gallium; and separating indium and gallium from the remaining electrolyte containing indium and gallium. The method provides a novel route for recycling CIGS waste, the process is simple, and the environmental pollution caused by CIGS waste is decreased. Further, the residual raffinate can be reused in electrolyzing of the distillation residue as a copper sulfate electrolyte by adding appropriate amount of copper sulfate and sulfuric acid therein, such that the circulation of the copper sulfate electrolyte forms a closed cycle and the discharge of wastewater and pollution to the environment are reduced.

Provided is a method for recovering and reusing an active material from a positive electrode scrap. The method for reusing a positive electrode active material, including the steps of: heat treating a positive electrode scrap including a lithium transition metal composite oxide positive electrode active material layer including nickel, cobalt and manganese or aluminum on a current collector to perform thermal decomposition of the binder and conductive material in the active material layer, thereby separating the current collector from the active material layer and recovering the active material in the active material layer; performing a first washing of the recovered active material with an aqueous lithium compound solution showing alkalinity in an aqueous solution state; adding a lithium precursor to the washed active material and carrying out annealing; performing a second washing of the annealed active material; and surface coating the washed active material after the second washing step to obtain a reusable active material.

In general, according to one embodiment, a recycling method is provided. The method includes dispersing an electrode containing a niobium titanium oxide in water; separating the niobium titanium oxide from the electrode dispersed in the water; and applying a first heat treatment to the separated niobium titanium oxide.

A Li recovery method includes: an acid leaching step of adding an acid to a battery slag to produce a leachate; a first addition step of adding a Ca content to the leachate to produce a first processed product; a post-first-addition filtration step of filtering the first processed product to be separated into a first processing filtrate and a first processing residue; a second addition step of adding sodium carbonate to the first processing filtrate to produce a second processed product; a post-second-addition filtration step of filtering the second processed product to be separated into a second processing filtrate and a second processing residue; heating the second processing filtrate; blowing carbon dioxide into the heated second processing filtrate to produce a third processed product; and a post-carbonation filtration step of filtering the third processed product to be separated into a third processing filtrate and a third processing residue.

A method for recycling an aluminum alloy scrap includes performing selective oxidation roasting and washing treatment on the aluminum alloy scrap to obtain an uncoated aluminum alloy scrap; melting the uncoated aluminum alloy scrap in a refining furnace to obtain aluminum alloy melt liquid, online-detecting components of the aluminum alloy melt liquid and adding a metallic copper, a copper alloy, a magnesium alloy or a zinc alloy to the aluminum alloy melt liquid according to the requirements of target alloy components, performing pressure-controlled and oxygen-controlled melting through regulating pressure intensity and oxygen partial pressure in the refining furnace and coupling an external-field stirring mode to obtain refining aluminum alloy melt liquid; filtering the refining aluminum alloy melt liquid, to obtain an aluminum alloy melt with the target alloy components; and casting the aluminum alloy melt.

A method for obtaining a metal salt from a spent lithium-ion (Li-ion) battery may include contacting a leaching solvent to a portion of the spent lithium-ion battery to form a first dispersion. The first dispersion is heated to a temperature in a range from 50? C. to 90? C. by applying microwave radiation. The temperature of the first dispersion is maintained to be in the range from 50? C. to 90? C. for a period in a range from 10 seconds to 5 minutes by further applying microwave radiation to the heated first dispersion. The first dispersion is filtered to obtain a first filtrate. The first dispersion is then filtered to separate undissolved material from a first filtrate. The undissolved precipitate is dehydrated to obtain the black mass.

A method capable of inexpensively recovering valuable metals is provided. The method for recovering a valuable metal includes: a preparation step of preparing a charge containing at least lithium (Li) and a valuable metal; an oxidation and reductive melting step of subjecting the charge to an oxidation treatment and a reductive melting treatment to produce a reduced product containing a molten alloy and a slag, the molten alloy containing the valuable metal; and a slag separation step of separating the slag from the reduced product to recover the molten alloy, in which the mole ratio of lithium (Li) to aluminum (Al) (Li/Al ratio) in the slag is 0.15 or more and less than 0.40, and the mole ratio of calcium (Ca) to aluminum (Al) (Ca/Al) in the slag is 0.15 or more.