Patent classifications
C22B7/001
METHOD FOR RECOVERING ACTIVE METAL OF LITHIUM SECONDARY BATTERY
In a method for recovering an active metal of a lithium secondary battery, a cathode active material mixture is prepared from a cathode of a lithium secondary battery. A first reductive process using a first reductive reaction gas and a second reductive process using a second reductive reaction gas that has a higher reaction source concentration than that of the first reductive reaction gas are performed sequentially and continuously to convert the cathode active material mixture into a preliminary precursor mixture. A lithium precursor is recovered from the preliminary precursor mixture. A lithium recovery ratio may be increased by a stepwise reduction while preventing an increase of heating value.
METHOD FOR RECOVERING VALUABLE METALS FROM WASTE BATTERY
Provided is a method for recovering valuable metals contained in waste batteries, wherein valuable metals can be efficiently recovered while suppressing a reduction in recovery rate. The method according to the present invention for recovering valuable metals from waste batteries comprises: a roasting step S1 for roasting a waste battery; a crushing step S2 for inserting an obtained roasted material into a crushing container, and crushing the roasted material using a chain mill; and a sieving step S3 for sieving an obtained crushed material and separating the crushed material into sieve upper material and sieve lower material. A chain mill equipment that is used in the crushing process is provided with: a rotating axial rod vertically erected with respect to a bottom surface of a crushing container; and a chain attached to a side surface of the rotating axial rod.
Method for Separating Transition Metal from Waste Positive Electrode Material
A method for separating a transition metal from a waste positive electrode material includes step 1 of preparing a waste positive electrode material represented by Formula 1, step 2 of heat treating the waste positive electrode material in an inert gas atmosphere or an oxygen atmosphere to phase separate the waste positive electrode material into a lithium oxide and a metal oxide, step 3 of cooling an obtained product of step 2 to room temperature in an inert atmosphere, and step 4 of mixing a cooled product cooled to room temperature in step 3 with distilled water, and then filtering the mixture to leach a transition metal.
METHOD FOR RECOVERING VALUABLE METAL
The purpose is to provide a method for recovering a valuable metal at low cost. The present invention is a method for recovering a valuable metal, the method comprising a step of preparing a burden material containing at least a valuable metal to obtain a raw material, a step of subjecting the raw material to an oxidation treatment and a reductive melting treatment to produce a reduced product containing an alloy and a slag, and a step of separating the slag from the reduced product to collect the alloy, in which the copper grade, which is a ratio of the mass of copper (Cu) to the total mass of nickel (Ni), cobalt (Co) and copper (Cu) contained in the alloy (i.e., a Cu/(Ni+Co+Cu) ratio), is adjusted to 0.250 or more.
INFECTIOUS WASTE DISPOSAL
A system for treating infectious waste is provided that employs a medical waste handling and shredding sub-system that feeds partially processed waste to an oxidizer to eliminate potential airborne infectious waste prior to transforming the medical waste into useful co-products. Medical waste is transformed into value added products including hydrocarbon based gases, hydrocarbon-based liquids, carbonized material, and recovered precious metals and rare earth materials in a system having as its transformative element an anerobic, negative pressure, or carbonization system. With medical waste as a feedstock for the production of valuable products, an economically viable and environmentally more responsible alternative to traditional methods of medical waste treatment is realized.
METHOD FOR RECYCLING HYDROGEN FUEL CELL OF NEW ENERGY VEHICLE
Disclosed is a method for recycling a hydrogen fuel cell of a new energy vehicle, including the following steps of: (1) discharging and disassembling a hydrogen fuel cell in turn to obtain a hydrogen supply system, an air supply system, a cooling system and a galvanic pile; (2) disassembling the galvanic pile into a catalyst and carbon cloth, and ashing to obtain ash; (3) adding an auxiliary agent into the ash, mixing, introducing inert gas, heating, introducing oxidizing gas, and absorbing tail gas by using an ammonium salt solution; and (4) adding a reducing agent into the ammonium salt solution absorbing the tail gas in step (3) to react, filtering, taking and cleaning a filter residue to obtain Pt.
METHOD FOR REUSING ACTIVE MATERIAL USING POSITIVE ELECTRODE SCRAP
There is provided a method of collecting and reusing an active material from a positive electrode scrap. The method of reusing a positive electrode active material according to the present disclosure includes (a-1) dry-milling a positive electrode scrap comprising an active material layer on a current collector to form the active material layer into a powdered state and separate the current collector, (a-2) thermally treating the active material layer in powder form in air for thermal decomposition of a binder and a conductive material in the active material layer, to collect an active material, (b) washing the active material collected from the step (a-2) with a lithium compound solution which is basic in an aqueous solution and drying, and (c) annealing the active material washed from the step (b) with an addition of a lithium precursor to obtain a reusable active material.
VOLATILLES CAPTURE EDUCTOR SYSTEM
A volatiles consuming eductor system for coated scrap metal furnaces with separate delacquering and melt chambers. Motive gas is forced through an inlet into a mixing chamber in a direction opposite a suction port, creating a Venturi that draws gases from the delaquering chamber through the mixing chamber. The motive gas and the drawn gases mix and are forced through a discharge port, ignited, and injected into the melt chamber to help heat the melt chamber. A computer monitors process conditions and controls a regulator that adjusts the motive gas flow in response to those conditions.
METHOD AND SYSTEM FOR SEPARATING CATHODE MATERIAL OF WASTE LITHIUM SECONDARY BATTERY USING OXIDATION REACTION OF ANODE MATERIAL AND REDUCTION REACTION OF CATHODE MATERIAL
Proposed are a method and a system for separating a cathode material of a waste lithium secondary battery using an oxidation reaction of an anode material and a reduction reaction of the cathode material. When lithium is heated to a level where lithium can undergo an explosive reaction using the low-temperature pyrolysis system, the binder, the electrolyte, and the separator contained in the waste lithium secondary battery are gasified into syngas by the explosive reaction of lithium and the resulting syngas is removed. The reduction reaction of the cathode material and the oxidation reaction of the anode material are promoted by the continuous explosive reaction of lithium and the stirring action of the spiral. As a result, the black powder and the current collector mixture are extracted. Therefore, it is possible to improve the recovery rate of valuable metals to more than 97%, thereby improving recycling efficiency.
ALLOY TREATMENT METHOD
An alloy treatment method is provided, in which a solution containing nickel and/or cobalt is obtained from an alloy containing nickel and/or cobalt and also containing copper and zinc, the method comprising: a leaching step for subjecting the alloy to a leaching treatment with an acid under the condition where a sulfating agent is present to produce a leachate; a reduction step for subjecting the leachate to a reduction treatment using a reducing agent to produce a reduced solution; an oxidation/neutralization step for adding an oxidizing agent and a neutralizing agent to the reduced solution to produce a neutralized solution containing nickel and/or cobalt and also containing zinc; and a solvent extraction step for subjecting the neutralized solution to a solvent extraction procedure using an acidic phosphorus compound-based extractant to produce a solution containing nickel and/or cobalt.