C22B7/006

OBTAINING VALUABLE SOLIDS AND COMBUSTIBLE GAS FROM ALUMINUM REMELTING WASTE

Methods for obtaining solid products and combustible gas using aluminum waste are disclosed. In some embodiments, a method for obtaining solid products and combustible gas using aluminum waste may comprise: obtaining a reactive mass, the reactive mass comprising aluminum remelting waste or a derivative thereof; applying a solvent to the reactive mass to generate a solution and a first solid product; separating the solution from the first solid product; applying a reactant to at least a portion of the first solid product to initiate a reaction, the reactant being different from the solvent, the reaction generating a combustible gas and a second solid product; and separating the reactant from the second solid product.

METHOD FOR RECYCLING LI-ION BATTERIES
20220411896 · 2022-12-29 ·

A method for recycling a battery including the following steps: a) dissolution of a battery waste, for example an electrode, including lithium and a metal selected from cobalt and manganese, such that a solution to be treated containing lithium ions and metal ions is formed, b) addition of a peroxymonosulfate salt to the solution to be treated, the solution to be treated being regulated at a pH ranging from 1 to 4 when the metal is cobalt or at a pH ranging from 0.1 to 2.5 when the metal is manganese, such that the metal ions are selectively precipitated in the form of metal oxyhydroxide, c) separation of the lithium ions from the solution to be treated. Advantageously, the solution further comprises nickel ions.

METHOD OF SEPARATING ONE OR MORE ELEMENTS FROM AN ALLOY
20220411894 · 2022-12-29 ·

A method of separating one or more elements from an alloy includes subjecting a metal alloy to a stimulus to form an enriched material including the one or more elements and to form a depleted material. The enriched material is enriched in the one or more elements compared to the alloy and the depleted material is depleted in the one or more elements compared to the alloy. The method also includes removing the enriched material and the depleted material from one another.

PROCESS FOR THE PURIFICATION OF LITHIUM SALTS

A process for the recovery of lithium from waste lithium ion batteries or parts thereof is disclosed. The process comprising the steps of A) providing a crude lithium hydroxide as a solid, which contains fluoride; and (B) dissolving the crude lithium hydroxide solid with a lower alcohol such as methanol or ethanol provides good separation of lithium in high purity.

METHOD FOR SEPARATING LITHIUM

Provided is a method for separating lithium from a lithium solution containing lithium by 200 mg/L or more and fluorine by 20 mg/L or more, the method including: a first removal step of adding a first component, which solidifies the fluorine contained in the lithium solution, to the lithium solution and removing the fluorine solidified to obtain a F-removed liquid; and a second removal step of adding a second component, which solidifies the first component remaining in the F-removed liquid, to the F-removed liquid and removing the first component solidified to obtain a first component-removed liquid.

ELECTROLYTE RECOVERY
20220399589 · 2022-12-15 ·

The invention provides a method of recovering a lithium electrolyte salt from a used electrolyte, the method comprising: contacting a used electrolyte comprising a lithium electrolyte salt and electrolyte solvent with a polar aprotic solvent to produce a solution comprising the lithium electrolyte salt, the electrolyte solvent and the polar aprotic solvent, wherein at least one of the electrolyte solvent and the polar aprotic solvent comprises carbonate solvent, combining the solution with a precipitation solvent in which the lithium electrolyte salt is poorly soluble; precipitating a precipitated composition comprising the lithium electrolyte salt solvated by the carbonate solvent from a solvent mixture comprising the polar aprotic solvent, the precipitation solvent and the electrolyte solvent, wherein the precipitated composition precipitates as a solid or as a liquid; and separating the precipitated composition from the solvent mixture.

METHOD FOR SEPARATION, SEGREGATION, AND RECOVERY OF CONSTITUENT MATERIALS FROM ELECTROCHEMICAL CELLS
20220384867 · 2022-12-01 ·

A method for separating and recovering materials from an electrochemical cell by dissolution in multiple solvents, separation of dissolved constituents, and recovery of materials.

Method for removing fluoride from a zinc-containing solution or suspension, defluoridated zinc sulfate solution and use thereof, and method for producing zinc and hydrogen fluoride or hydrofluoric acid

Embodiments of the invention relate to a process for removing fluoride from a solution or suspension containing zinc, in particular a solution of zinc sulfate, a defluoridated solution of zinc sulfate obtainable by such a process, its use as well as processes for producing zinc and hydrogen fluoride or hydrofluoric acid. The process for removing fluoride comprises (i) providing a solution or suspension A containing zinc, wherein the solution or suspension A containing zinc further contains fluoride ions; (ii) adding a solution B containing a dissolved salt of a rare earth element to the solution or suspension A containing zinc, wherein a solid comprising a rare earth element fluoride and a solution C containing zinc are formed; and (iii) separating the solid from the solution C containing zinc, wherein the solution C containing zinc has a lower concentration of fluoride ions than the solution or suspension A containing zinc.

METHOD FOR EXTRACTING LITHIUM BY MEANS OF EXTRACTION-BACK EXTRACTION SEPARATION AND PURIFICATION
20220372592 · 2022-11-24 ·

The present disclosure relates to a method for lithium recovery by extraction-stripping separation and purification, including: (1) performing an extraction on a lithium-containing solution using an extraction system including a composite extractant at a pH in a range of 10-13 and separating to obtain a lithium-loaded organic phase; (2) subjecting the lithium-loaded organic phase obtained in step (1) to a gas-liquid-liquid three-phase stripping to obtain a lithium-loaded stripping solution; and (3) subjecting the stripping solution obtained in step (2) to a thermal treatment and separating to obtain a lithium product and a separated mother liquor.

Method and apparatus for Ga-recovery

The present invention encompasses a method of selectively separating Ga from wastewaters with the aid of a dialysis method. This exploits the particular complexation behaviour of Ga, which forms an unstable tetrahalo complex. This forms only in the case of a sufficiently high halide concentration. Since the halide concentration becomes lower across the membrane, the Ga-tetrahalo complex breaks down in the membrane, as a result of which the Ga is retained. Other metals such as In and Fe do not show this behaviour, and therefore the tetrahalo complexes of these metals can pass through the membrane and hence can be selectively separated off.