Patent classifications
C23C2/26
METHOD FOR MANUFACTURING FLUORINATED STRUCUTURED ORGANIC PHOTORECEPTOR LAYERS
Disclosed herein is a method for manufacturing a fluorinated structured organic film (FSOF) composition for a photoreceptor. The method includes combining a fluorinated diol, an electroactive segment and a solvent in a round bottom reactor. The reacted is heated, without mixing dissolve the fluorinated diol composition. The dissolved fluorinated diol composition is mixed to dissolve the electroactive segment while maintaining the reactor at a temperature of between 80 and 85° C. A catalyst and a leveling agent are added to the solution to initiate a pre-cure reaction. The pre-cure reaction proceeds for at least 2 hours at a temperature of between 80 and 85° C. The solution is cooled to room temperature and filtered.
METHOD FOR MANUFACTURING FLUORINATED STRUCUTURED ORGANIC PHOTORECEPTOR LAYERS
Disclosed herein is a method for manufacturing a fluorinated structured organic film (FSOF) composition for a photoreceptor. The method includes combining a fluorinated diol, an electroactive segment and a solvent in a round bottom reactor. The reacted is heated, without mixing dissolve the fluorinated diol composition. The dissolved fluorinated diol composition is mixed to dissolve the electroactive segment while maintaining the reactor at a temperature of between 80 and 85° C. A catalyst and a leveling agent are added to the solution to initiate a pre-cure reaction. The pre-cure reaction proceeds for at least 2 hours at a temperature of between 80 and 85° C. The solution is cooled to room temperature and filtered.
METHOD FOR APPLYING A METAL PROTECTIVE COATING TO A SURFACE OF A STEEL PRODUCT
A method for applying a metallic protective coating to a surface of a steel product, where another surface is to remain free from the metallic protective coating, may involve applying the metallic protective coating by hot dip coating in a hot dip coating bath. A preliminary coating may be applied to the surface that is to remain free from the metallic protective coating prior to the hot dip coating. The preliminary coating may include SiO.sub.2 and may prevent the metallic protective coating from adhering to the intended surface during hot dip coating. Thus one surface of a steel product may be provided with a metallic protective coating, and another surface of the steel product may be kept free from the protective coating, all with a minimum of cost and complexity and with optimized resource economics. Further, the preliminary coating, deposited from a gas phase to that surface of the steel product that is to be kept free from the metallic protective coating, may be a layer that includes amorphous silicon dioxide and has a layer thickness of 0.5-500 nm.”
METHOD FOR APPLYING A METAL PROTECTIVE COATING TO A SURFACE OF A STEEL PRODUCT
A method for applying a metallic protective coating to a surface of a steel product, where another surface is to remain free from the metallic protective coating, may involve applying the metallic protective coating by hot dip coating in a hot dip coating bath. A preliminary coating may be applied to the surface that is to remain free from the metallic protective coating prior to the hot dip coating. The preliminary coating may include SiO.sub.2 and may prevent the metallic protective coating from adhering to the intended surface during hot dip coating. Thus one surface of a steel product may be provided with a metallic protective coating, and another surface of the steel product may be kept free from the protective coating, all with a minimum of cost and complexity and with optimized resource economics. Further, the preliminary coating, deposited from a gas phase to that surface of the steel product that is to be kept free from the metallic protective coating, may be a layer that includes amorphous silicon dioxide and has a layer thickness of 0.5-500 nm.”
HIGH-STRENGTH PLATED STEEL SHEET HAVING EXCELLENT PLATING PROPERTIES, WORKABILITY, AND DELAYED FRACTURE RESISTANCE, AND METHOD FOR PRODUCING SAME
Disclosed herein is a high-strength plated steel sheet having a plated layer on the surface of a base steel sheet and containing predetermined steel components. The steel sheet includes, in the order from the interface of the base steel sheet and the plated layer towards the base steel sheet: a soft layer having a Vickers hardness that is 90% or less of the Vickers hardness at a portion t/4 of the base steel sheet, where t is a sheet thickness of the base steel sheet; and a hard layer consisting of a structure which is mainly composed of martensite and bainite and in which the average grain size of prior austenite is 20 μm or less. The average depth D of the soft layer is 20 μm or greater, and the average depth d of an internal oxide layer is 4 μm or greater and smaller than D.
COATED STEEL SHEET WITH THIN ALUMINIUM ALLOY COATING AND COATING METHOD THEREOF
The present invention relates to a coated steel sheet having a thin aluminium alloy coating and a coating method thereof The coated steel sheet of the present invention is used for hot stamping. The coating thickness of the coated steel sheet is 5˜14 μm, wherein the aluminium alloy coating comprises a FeAlSi inhibitive layer adjacent to a substrate steel sheet and an Al alloy layer outside the FeAlSi inhibitive layer, wherein the thickness of the FeAlSi inhibitive layer is no more than 60% of the coating thickness and is 1.5˜6.0 μm. The diameters of Kirkendall voids within 2 μm from an interface between the FeAlSi inhibitive layer and the substrate steel to the interior of the substrate steel are no more than 2.5 μm, wherein the number of Kirkendall voids with a diameter of no less than 0.5 μm and no more than 2.5 μm does not exceed 15 per 35 μm. The present invention also discloses a coating method for coating a thin aluminium alloy coating on a substrate steel sheet for hot stamping. It can eliminate skip coating and enable a hot stamped component obtained by the coated steel sheet to have excellent resistance spot welding performance.
HOT-DIPPED Zn-Al-Mg-BASED PLATED STEEL
This hot-dip Zn—Al—Mg-based plated steel includes: a steel; and a plating layer formed on a surface of the steel, in which the plating layer contains, as an average composition, Mg: 1 to 10 mass %, Al: 4 to 22 mass %, and a remainder consisting of Zn and impurities, the plating layer includes an (Al—Zn mixed structure) in an area ratio of 10% to 70% in a cross section of the plating layer in a matrix of an (Al/Zn/MgZn.sub.2 ternary eutectic structure), the (Al—Zn mixed structure) includes a first region that has a Zn concentration in a range of 75 mass % or more and less than 85 mass % and a second region that is present inside the first region and has a Zn concentration in a range of 67 mass % or more and less than 75 mass %, and an area ratio of the second region in the (Al—Zn mixed structure) in the cross section of the plating layer is more than 0% and 40% or less.
METAL SHEET HAVING A DETERMINISTIC SURFACE STRUCTURE AND METHOD FOR PRODUCING A FORMED AND COATED SHEET-METAL COMPONENT
The invention relates to a sheet metal having a deterministic surface structure, the surface structure being impressed into the sheet metal, the surface structure having at least one peak region and at least one valley region, the peak region and the valley region being joined by a flank region. The invention further relates to a method for producing a formed and coated sheet-metal component.
Method for Producing a Flat Steel Product Having a Protective Zinc-Based Metal Layer and a Phosphating Layer Produced on a Surface of the Protective Metal Layer and Flat Steel Product of This Type
A method for production of a flat steel product including at least the following steps, completed in a continuous process: providing a flat steel product, wherein a protective metal layer of Zn, a Zn—Al alloy, a Zn—Mg alloy or a Zn—Mg—Al alloy is applied to at least one side by hot dip coating; at least partly removing a native oxide layer present on the surface of the protective metal layer by wetting this surface with an acidic solution of sulfuric acid, sulfurous acid, hydrochloric acid, phosphoric acid, phosphonic acid, nitric acid, formic acid, oxalic acid, acetic acid, citric acid, malic acid, tartaric acid, nitrous acid or hydrofluoric acid; activating the surface of the protective metal layer by applying an aqueous activation solution to the surface of the protective metal layer; and phosphating the activated surface of the protective metal layer by applying an aqueous phosphating solution to the activated surface.
Method for Producing a Flat Steel Product Having a Protective Zinc-Based Metal Layer and a Phosphating Layer Produced on a Surface of the Protective Metal Layer and Flat Steel Product of This Type
A method for production of a flat steel product including at least the following steps, completed in a continuous process: providing a flat steel product, wherein a protective metal layer of Zn, a Zn—Al alloy, a Zn—Mg alloy or a Zn—Mg—Al alloy is applied to at least one side by hot dip coating; at least partly removing a native oxide layer present on the surface of the protective metal layer by wetting this surface with an acidic solution of sulfuric acid, sulfurous acid, hydrochloric acid, phosphoric acid, phosphonic acid, nitric acid, formic acid, oxalic acid, acetic acid, citric acid, malic acid, tartaric acid, nitrous acid or hydrofluoric acid; activating the surface of the protective metal layer by applying an aqueous activation solution to the surface of the protective metal layer; and phosphating the activated surface of the protective metal layer by applying an aqueous phosphating solution to the activated surface.