Provided is a metal oxide production apparatus that implements a flux evaporation method. The production apparatus includes a firing furnace configured to subject a metal compound to firing in the presence of flux, a cooling pipe connected to the firing furnace and configured to convert vaporized flux resulting from the firing into powder, and a recovery means configured to recover powdered flux converted in the cooling pipe. Furthermore, provided is a metal oxide production method comprising a step (1) of subjecting a metal compound to firing in the presence of flux and obtaining a metal oxide and vaporized flux, a step (2) of converting the vaporized flux into powder by cooling the vaporized flux, and a step (3) of recovering powdered flux resulting from the converting.

A method for producing a metal oxide nanocrystals according to the embodiment of the present invention comprises continuously flowing a nanocrystal precursor solution comprising a nanocrystal precursor into a continuous flow path and heating the nanocrystal precursor solution in the continuous flow path to create nanocrystals, comprising: providing a nanocrystal precursor solution supply unit that is connected to the continuous flow path and comprises a first vessel and a second vessel; delivering a nanocrystal precursor solution in the second vessel to the continuous low path; and creating a nanocrystal precursor solution in the first vessel as a different batch from the nanocrystal precursor solution in the second vessel.

A method for producing a metal oxide nanocrystals according to the embodiment of the present invention comprises continuously flowing a nanocrystal precursor solution comprising a nanocrystal precursor into a continuous flow path and heating the nanocrystal precursor solution in the continuous flow path to create nanocrystals, comprising: providing a nanocrystal precursor solution supply unit that is connected to the continuous flow path and comprises a first vessel and a second vessel; delivering a nanocrystal precursor solution in the second vessel to the continuous low path; and creating a nanocrystal precursor solution in the first vessel as a different batch from the nanocrystal precursor solution in the second vessel.

Provided are a method of preparing a metal oxide-silica composite aerogel, which includes preparing metal oxide-silica composite precipitates by adding a metal salt solution to a silicate solution and performing a reaction, and drying the metal oxide-silica composite precipitates by irradiation with infrared rays in a wavelength range of 2 m to 8 m, and a metal oxide-silica composite aerogel having excellent physical properties, such as low tap density and high specific surface area, as well as excellent pore properties prepared by the method.

A method of preparing a metal/metal oxide material can make use of a nanostructure that includes a first metal to form the metal oxide, and a reaction surface with a reducing agent on the reaction surface. A second metal is deposited onto the reaction surface to form a bimetallic product. The bimetallic product is calcined to form the metal/metal oxide material.

A method of preparing a metal/metal oxide material can make use of a nanostructure that includes a first metal to form the metal oxide, and a reaction surface with a reducing agent on the reaction surface. A second metal is deposited onto the reaction surface to form a bimetallic product. The bimetallic product is calcined to form the metal/metal oxide material.

A method and system for producing nano-active powder materials. The method can be used with a reactor system comprising stages in which input particles flow under gravity progressively through stages of the reactor. A powder injector first stage in which ground input precursor powder is injected into the reactor. An externally heated preheater stage may be in the reactor, in which the precursor powder is heated to a temperature of calcination reaction. An externally heated calciner stage in the reactor, in which primary precursor volatile constituents can be rapidly removed calcination reactions as a high purity gas stream to produce the desired nano-active product. A post-processing reactor stage in which there is a change of the gas stream composition to produce the desired hot powder product by virtue of the nano-activity of the first powder material. A powder ejector stage in which the hot powder product is ejected from the reactor.

A method and system for producing nano-active powder materials. The method can be used with a reactor system comprising stages in which input particles flow under gravity progressively through stages of the reactor. A powder injector first stage in which ground input precursor powder is injected into the reactor. An externally heated preheater stage may be in the reactor, in which the precursor powder is heated to a temperature of calcination reaction. An externally heated calciner stage in the reactor, in which primary precursor volatile constituents can be rapidly removed calcination reactions as a high purity gas stream to produce the desired nano-active product. A post-processing reactor stage in which there is a change of the gas stream composition to produce the desired hot powder product by virtue of the nano-activity of the first powder material. A powder ejector stage in which the hot powder product is ejected from the reactor.

A system and method for synthesizing a nanoparticle material includes dissolving a metal nitrate in deionized water, adding a hydrogel precursor in the deionized water containing the dissolved metal nitrate to create an aqueous solution, heating the aqueous solution, cooling the aqueous solution to create a solid gel, and calcinating the solid gel to create a metal oxide nanoparticle material. The metal oxide nanoparticle material may include a zinc oxide-based nanoparticle material. The hydrogel precursor may include an agarose gel. The solid gel may be calcinated at approximately 600 C. The solid gel may be calcinated for approximately five hours in the presence of air. The aqueous solution may be heated to a boil. The aqueous solution may be heated at a temperature of 100 C.

A coating agent for forming a metal oxide film, which contains an organic solvent that is different from N,N-dimethyl acetamide (DMA) or N-methyl pyrrolidone (NMP), and which has excellent conformal coating properties; and a method for producing a substrate having a metal oxide film. A coating agent for forming a metal oxide film, which contains a solvent and a metal, and wherein the solvent contains a compound (A) represented by formula (1).

##STR00001##

In formula (1), each of R.sup.1 and R.sup.2 independently represents an alkyl group having 1-3 carbon atoms; and R.sup.3 represents a group represented by formula (1-1) or formula (1-2).

##STR00002##

In formula (1-1), R.sup.4 represents a hydrogen atom or a hydroxyl group; and each of R.sup.5 and R.sup.6 independently represents an alkyl group having 1-3 carbon atoms. In formula (1-2), each of R.sup.7 and R.sup.8 independently represents a hydrogen atom or an alkyl group having 1-3 carbon atoms.