C01B13/36

Silicon oxide-coated iron oxide composition for coating comprising iron oxide particles coated with silicon oxide
10182975 · 2019-01-22 · ·

The present invention provides a composition for coating having high ultraviolet ray protection ability for a coating material, and properties required for a coating material such as texture, appearance, designability and weather resistance. The composition is a silicon oxide-coated iron oxide composition for coating comprising iron oxide particles, a primary particle diameter of which is 1 nm or more and 50 nm or less, wherein at least a part of the surface of said iron oxide particles is coated with silicon oxide, and wherein said composition comprises an iron oxide particle dispersion having the average molar absorption coefficient of 1500 L/(mol.Math.cm) or more for the light of the wavelengths from 190 nm to 380 nm in a state that said coated iron oxide particles are dispersed in a dispersion medium. It is preferable that the transmittance of said iron oxide particle containing dispersion for the light of the wavelengths from 200 nm to 420 nm is 2.0% or less, and the transmittance of said iron oxide particle containing dispersion for the light of the wavelengths from 620 nm to 780 nm is 80% or more.

Silicon oxide-coated iron oxide composition for coating comprising iron oxide particles coated with silicon oxide
10182975 · 2019-01-22 · ·

The present invention provides a composition for coating having high ultraviolet ray protection ability for a coating material, and properties required for a coating material such as texture, appearance, designability and weather resistance. The composition is a silicon oxide-coated iron oxide composition for coating comprising iron oxide particles, a primary particle diameter of which is 1 nm or more and 50 nm or less, wherein at least a part of the surface of said iron oxide particles is coated with silicon oxide, and wherein said composition comprises an iron oxide particle dispersion having the average molar absorption coefficient of 1500 L/(mol.Math.cm) or more for the light of the wavelengths from 190 nm to 380 nm in a state that said coated iron oxide particles are dispersed in a dispersion medium. It is preferable that the transmittance of said iron oxide particle containing dispersion for the light of the wavelengths from 200 nm to 420 nm is 2.0% or less, and the transmittance of said iron oxide particle containing dispersion for the light of the wavelengths from 620 nm to 780 nm is 80% or more.

Preparation of suspensions
10167203 · 2019-01-01 · ·

A method for preparing a suspension of LDH particles comprising the steps of: preparing LDH precipitates by coprecipitation to form a mixture of LDH precipitates and solution; separating the LDH precipitates from the solution; washing the LDH precipitates to remove residual ions; mixing the LDH precipitates with water; and subjecting the mixture of LDH particles and water to a hydrothermal treatment step by heating to a temperature of from greater than 80 C. to 150 C. for a period of about 1 hour to about 144 hours to form a well dispersed suspension of LDH particles in water, wherein said LDH particles in suspension comprise platelets having a maximum particle dimension of up to 400 nm.

Particles and manufacturing methods thereof

Particles and manufacturing methods thereof are provided. The manufacturing method of the particle includes providing a precursor solution containing a precursor dissolved in a solution, and irradiating the precursor solution with a high energy and high flux radiation beam to convert the precursor to nano-particles. Particles with desired dispersion, shape, and size are manufactured without adding a stabilizer or surfactant to the precursor solution.

Particles and manufacturing methods thereof

Particles and manufacturing methods thereof are provided. The manufacturing method of the particle includes providing a precursor solution containing a precursor dissolved in a solution, and irradiating the precursor solution with a high energy and high flux radiation beam to convert the precursor to nano-particles. Particles with desired dispersion, shape, and size are manufactured without adding a stabilizer or surfactant to the precursor solution.

Sol-gel process for synthesis of nanocrystalline oxides

A Continuous flow synthesis of nanocrystalline metal oxides by rapid sol-gel process is disclosed. The process disclosed uses an impinging microjet micromixer device to obtain the nano crystalline metal oxides. A method of fabricating and assembling the impinging microjet micromixer is also disclosed herewith.

Sol-gel process for synthesis of nanocrystalline oxides

A Continuous flow synthesis of nanocrystalline metal oxides by rapid sol-gel process is disclosed. The process disclosed uses an impinging microjet micromixer device to obtain the nano crystalline metal oxides. A method of fabricating and assembling the impinging microjet micromixer is also disclosed herewith.

Process for producing suspensions
10059602 · 2018-08-28 · ·

Process for producing a suspension by precipitation of a solid from a solution, wherein at least two solutions of salts are combined with one another in a stirred vessel so as to form a sparingly soluble solid, where portions of suspension are taken off continuously or discontinuously, the portions taken off in this way are processed in a combination of two separation apparatuses, where gas is separated off in a first separation apparatus which is selected from liquid-gaseous separation apparatuses, and mother liquor is separated off from precipitated sparingly soluble solid in a second separation apparatus selected from solid-liquid separation apparatuses, and the mother liquor is taken off, and the solid which has been separated off or enriched in this way is returned to the reaction mixture.

Method of producing silica-based particles

Hollow silica-based particles having cavities inside the outer shell having a low refractive index. The method of producing the silica-based particles comprises the following steps (a) and (b): (a) a step in which, when an aqueous silicate solution and/or an acidic silicic acid solution and an aqueous solution of an alkali-soluble inorganic compound are simultaneously added in an alkali aqueous solution to prepare a dispersion liquid of composite oxide particles, an electrolytic salt is added at the molar ratio of a mole number of the electrolytic salt (M.sub.E) versus that of SiO.sub.2 (M.sub.S) [(M.sub.E)/(M.sub.S)] in the range from 0.1 to 10, and (b) a step of furthermore adding an electrolytic salt, if necessary, to the dispersion liquid of composite oxide particles and then removing at least a portion of elements constituting the composite oxide other than silicon by adding an acid to prepare a dispersion liquid of silica-based particles.

SILICON OXIDE-COATED IRON OXIDE COMPOSITION FOR COATING COMPRISING IRON OXIDE PARTICLES COATED WITH SILICON OXIDE
20180200159 · 2018-07-19 · ·

The present invention provides a composition for coating having high ultraviolet ray protection ability for a coating material, and properties required for a coating material such as texture, appearance, designability and weather resistance. The composition is a silicon oxide-coated iron oxide composition for coating comprising iron oxide particles, a primary particle diameter of which is 1 nm or more and 50 nm or less, wherein at least a part of the surface of said iron oxide particles is coated with silicon oxide, and wherein said composition comprises an iron oxide particle dispersion having the average molar absorption coefficient of 1500 LI(mol.Math.cm) or more for the light of the wavelengths from 190 nm to 380 nm in a state that said coated iron oxide particles are dispersed in a dispersion medium. It is preferable that the transmittance of said iron oxide particle containing dispersion for the light of the wavelengths from 200 nm to 420 nm is 2.0% or less, and the transmittance of said iron oxide particle containing dispersion for the light of the wavelengths from 620 nm to 780 nm is 80% or more.