Disclosed is lithium iron phosphate having an olivine crystal structure, wherein the lithium iron phosphate has a composition represented by the following Formula 1 and carbon (C) is coated on the particle surface of the lithium iron phosphate containing a predetermined amount of sulfur (S).
Li.sub.1+aFe.sub.1−xM.sub.x(PO.sub.4−b)X.sub.b  (1) (wherein M, X, a, x, and b are the same as defined in the specification).

This invention relates to processes for the removal of phosphorous from aqueous waste streams comprising phosphorus-containing compounds produced in the manufacture of glyphosate, in order to meet and typically exceed environmental regulations. More particularly, various embodiments of the present invention relate to the removal of phosphorous-containing compounds utilizing biological treatment system(s), oxidizing agent(s), and/or precipitant(s). The processes of the invention are also applicable to the removal of phosphorous compounds from phosphorous-containing waste streams other than those waste streams resulting from the manufacture of glyphosate.

This invention relates to processes for the removal of phosphorous from aqueous waste streams comprising phosphorus-containing compounds produced in the manufacture of glyphosate, in order to meet and typically exceed environmental regulations. More particularly, various embodiments of the present invention relate to the removal of phosphorous-containing compounds utilizing biological treatment system(s), oxidizing agent(s), and/or precipitant(s). The processes of the invention are also applicable to the removal of phosphorous compounds from phosphorous-containing waste streams other than those waste streams resulting from the manufacture of glyphosate.

This disclosure describes methods, processes and devices that remove or release organics from ores, such as phosphate ores or secondary sources such as mine tailings or waste. The method comprises: preparing an ore to a pre-set size; mixing the ore with an acidic reagent having an initial pH value in a slurry comprising the ore and the reagent; and while mixing the slurry, maintaining a pH level in the slurry to a pH range. While mixing the slurry, the slurry may produce a supernatant containing organic material removed from the ore and sediment containing refined ore. The method may also screen the slurry to create a first stream of materials that does not pass through the screen and a second stream of materials and refined ore that pass through the screen.

The invention provides a method for preparing lithium manganese iron phosphate, which includes the following steps: S1: mixing a manganese source and/or an iron source in solid phase to obtain a first mixture; S2: sintering the first mixture in solid phase at 300° C. to 1200° C. to obtain a manganese iron oxide (MnxFe1−x−y)mOn; S3: mixing the manganese iron oxide (MnxFe1−x−y)mOn with a lithium source, a phosphorus source, and optionally a manganese source and/or an iron source in solid phase to obtain a second mixture; and S4: sintering the second mixture in solid phase at 350° C. to 900° C. to obtain lithium manganese iron phosphate LiMnxFe1−x−yPO4, wherein 0≤x≤1, and 0≤y≤1. The method of the present invention can be used to prepare a lithium manganese iron phosphate material with high tap density, long cycle life, low costs, and high cost-effectiveness.

Methods of making a lithium mixed metal compound by reaction of starting materials are provided. The methods can include reacting and/or processed reacted starting materials to form the lithium mixed metal compound in the presence of a fluorine rich atmosphere or media.

Aerogel materials, aerogel composites, and the like may be improved by the addition of opacifiers to reduce the radiative component of heat transfer. Such aerogel materials, aerogel composites, and the like may also be treated to impart or improve hydrophobicity. Such aerogel materials and methods of manufacturing the same are described.

Aerogel materials, aerogel composites, and the like may be improved by the addition of opacifiers to reduce the radiative component of heat transfer. Such aerogel materials, aerogel composites, and the like may also be treated to impart or improve hydrophobicity. Such aerogel materials and methods of manufacturing the same are described.

A solid ionically conductive composition (e.g., nanoparticles of less than 1 micron or a continuous film) comprising at least one element selected from alkali metal, alkaline earth metal, aluminum, zinc, copper, and silver in combination with at least two elements selected from oxygen, sulfur, silicon, phosphorus, nitrogen, boron, gallium, indium, tin, germanium, arsenic, antimony, bismuth, transition metals, and lanthanides. Also described is a battery comprising an anode, a cathode, and a solid electrolyte (corresponding to the above ionically conductive composition) in contact with or as part of the anode and/or cathode. Further described is a thermal (e.g., plasma-based) method of producing the ionically conductive composition. Further described is a method for using an additive manufacturing (AM) process to produce an object constructed of the ionically conductive composition by use of particles of the ionically conductive composition as a feed material in the AM process.

Commercially beneficial carbon-containing fractions can be recovered from hydrothermal liquefaction reactions in various types of processors. Feedstock slurry from waste solids is placed into a pressurized processor where it is maintained at temperature and pressure for a predetermined period. On discharge from the processor the processed discharge is separated into liquid and solid fractions. Gaseous fractions including carbon dioxide can also be removed or off-taken from the processor. New molecular structures are created in this reaction, resulting in fractions including biogas, biofuels, biosolids and biocrude. Silica, phosphates, potash and low concentration nitrogen based fertilizer, along with carbonaceous material can also be recovered.