Patent classifications
C01B33/26
ALUMINOSILICATES, RELATED PROCESSES AND USES THEREOF AS SUPPLEMENTARY CEMENTING MATERIALS
The present disclosure concerns an aluminosilicate having a Blaine fineness of about 500 m.sup.2/kg to about 3000 m.sup.2/kg and/or a specific surface area of about 4 m.sup.2/g to about 20 m.sup.2/g, as well as the uses thereof. The present disclosure also comprises a dry cementing composition and a mortar or concrete composition, the compositions comprising said aluminosilicate. The present disclosure also comprises a process for the manufacture of aluminosilicate. The process comprises: roasting a spodumene concentrate in an acid medium; leaching the acidic roast spodumene concentrate so as to obtain a mixture comprising a solid comprising the aluminosilicate and a leachate; and separating the aluminosilicate from the leachate in an acid medium, wherein said aluminosilicate contains a calcium concentration of less than about 5%.
ALUMINOSILICATES, RELATED PROCESSES AND USES THEREOF AS SUPPLEMENTARY CEMENTING MATERIALS
The present disclosure concerns an aluminosilicate having a Blaine fineness of about 500 m.sup.2/kg to about 3000 m.sup.2/kg and/or a specific surface area of about 4 m.sup.2/g to about 20 m.sup.2/g, as well as the uses thereof. The present disclosure also comprises a dry cementing composition and a mortar or concrete composition, the compositions comprising said aluminosilicate. The present disclosure also comprises a process for the manufacture of aluminosilicate. The process comprises: roasting a spodumene concentrate in an acid medium; leaching the acidic roast spodumene concentrate so as to obtain a mixture comprising a solid comprising the aluminosilicate and a leachate; and separating the aluminosilicate from the leachate in an acid medium, wherein said aluminosilicate contains a calcium concentration of less than about 5%.
Crystal material and method of manufacturing the same
The present invention makes clear and defines a congruent composition of a langasite-based oxide, and establishes a method of manufacturing a crystal by any desired composition of AE.sub.3ME.sub.1+a(Ga.sub.1−xAl.sub.x).sub.3+bSi.sub.2+cO.sub.14 (AE is an alkaline-earth metal, ME is Nb or Ta, 0≤x≤1, −0.5<a≤0 or 0<a<0.5, −0.5<b≤0 or 0<b≤0.5, and −0.5<c≤0 or 0<c<0.5, excluding a=b=c=0). This makes it possible to suppress the formation of an impurity, and improve the yield and crystal manufacturing rate. The raw material is a raw material mixture prepared by mixing an alkaline-earth metal or its carbonate or oxide, Nb or Ta or its oxide, Ga or its oxide, Al or its oxide, and Si or its oxide.
Crystal material and method of manufacturing the same
The present invention makes clear and defines a congruent composition of a langasite-based oxide, and establishes a method of manufacturing a crystal by any desired composition of AE.sub.3ME.sub.1+a(Ga.sub.1−xAl.sub.x).sub.3+bSi.sub.2+cO.sub.14 (AE is an alkaline-earth metal, ME is Nb or Ta, 0≤x≤1, −0.5<a≤0 or 0<a<0.5, −0.5<b≤0 or 0<b≤0.5, and −0.5<c≤0 or 0<c<0.5, excluding a=b=c=0). This makes it possible to suppress the formation of an impurity, and improve the yield and crystal manufacturing rate. The raw material is a raw material mixture prepared by mixing an alkaline-earth metal or its carbonate or oxide, Nb or Ta or its oxide, Ga or its oxide, Al or its oxide, and Si or its oxide.
PROCESS FOR MAKING A CERAMIC PARTICULATE MIXTURE
A non-spray-drying, dry-granulation process for making a ceramic particulate mixture including from 4 wt % to 9 wt % water. At least 90 wt % of the particles have a particle size of from 80 μm to 600 μm. The process includes the steps of: (a) forming a precursor material; (b) subjecting the precursor material to a compaction step to form a compacted precursor material; (c) subjecting the compacted precursor material to a crushing step to form a crushed precursor material; and (d) subjecting the crushed precursor material to at least two air classification steps. One air classification step removes at least a portion of the particles having a particle size of greater than 600 μm from the crushed precursor material, and the other air classification step removes at least a portion of the particles having a particle size of less than 80 μm from the crushed precursor material.
AEROGEL COMPOSITIONS FOR HIGH TEMPERATURE APPLICATIONS
Aerogel materials, aerogel composites, and the like may be improved by the addition of opacifiers to reduce the radiative component of heat transfer. Such aerogel materials, aerogel composites, and the like may also be treated to impart or improve hydrophobicity. Such aerogel materials and methods of manufacturing the same are described.
AEROGEL COMPOSITIONS FOR HIGH TEMPERATURE APPLICATIONS
Aerogel materials, aerogel composites, and the like may be improved by the addition of opacifiers to reduce the radiative component of heat transfer. Such aerogel materials, aerogel composites, and the like may also be treated to impart or improve hydrophobicity. Such aerogel materials and methods of manufacturing the same are described.
Garnet powder, manufacturing method thereof, solid electrolyte sheet using hot press and manufacturing method thereof
The present disclosure relates to garnet powder, a manufacturing method thereof, a solid electrolyte sheet using a hot press, and a manufacturing method thereof. In particular, the present disclosure provides a method for manufacturing Li.sub.7La.sub.3Zr.sub.2O.sub.12 (LLZ) garnet powder including preparing a mixture by first dry mixing Li.sub.2CO.sub.3, La.sub.2O.sub.3, ZrO.sub.2, and Al.sub.2O.sub.3. The mixture is first calcinated for 5 to 7 hours in a temperature range of 800 to 1000° C. The calcinated mixture is ground to a powder with an average particle size of 1 to 4 μm through dry grinding. A cubic-phased LLZ garnet powder is prepared by second calcinating the ground mixture for 10 to 30 hours in a temperature range of 1100 to 1300° C.
Garnet powder, manufacturing method thereof, solid electrolyte sheet using hot press and manufacturing method thereof
The present disclosure relates to garnet powder, a manufacturing method thereof, a solid electrolyte sheet using a hot press, and a manufacturing method thereof. In particular, the present disclosure provides a method for manufacturing Li.sub.7La.sub.3Zr.sub.2O.sub.12 (LLZ) garnet powder including preparing a mixture by first dry mixing Li.sub.2CO.sub.3, La.sub.2O.sub.3, ZrO.sub.2, and Al.sub.2O.sub.3. The mixture is first calcinated for 5 to 7 hours in a temperature range of 800 to 1000° C. The calcinated mixture is ground to a powder with an average particle size of 1 to 4 μm through dry grinding. A cubic-phased LLZ garnet powder is prepared by second calcinating the ground mixture for 10 to 30 hours in a temperature range of 1100 to 1300° C.
Defoamer Active, Manufacturing Method Thereof, and Defoaming Formulation
This invention relates to a defoamer active. The defoamer active may include hydrophobized aluminum silicate particles. Aluminum silicate particles having a surface pH of at least about 9.6 and a BET surface area of less than about 150 m2/g are treated with a hydrophobilizing agent to provide the hydrophobized aluminum silicate particles. The defoamer actives are useful to prepare defoamer compositions which are useful for preventing or reducing foam in various aqueous systems.