C01B39/26

Process for continuously synthesizing zeolite crystals

The present invention relates to a process for preparing zeolite crystals continuously, comprising the continuous introduction of a composition capable of generating zeolite crystals into at least one crystallization reaction zone subjected to stirring means, giving said composition a flow characterized by a relative Reynolds number Re.sub.r of between 40 and 50 000, and the continuous recovery of the crystals formed according to a flow characterized by a net Reynolds number Re.sub.n of between 1 and 1500.

Zeolite with tuned aluminum content and mesoporosity

Compositions and methods for preparing mesoporous and/or mesostructured materials from low SAR zeolites are provided herewith. In particular, methods are provided that involve: (a) providing a low SAR zeolite, (b) optionally subjecting the low SAR zeolite to an acid framework modification, and (c) subjecting the framework-modified zeolite to a mesopore formation treatment. The resulting mesoporous zeolites can have bi-modal mesoporosity and higher aluminum contents relative to existing mesoporous zeolites.

Zeolite with tuned aluminum content and mesoporosity

Compositions and methods for preparing mesoporous and/or mesostructured materials from low SAR zeolites are provided herewith. In particular, methods are provided that involve: (a) providing a low SAR zeolite, (b) optionally subjecting the low SAR zeolite to an acid framework modification, and (c) subjecting the framework-modified zeolite to a mesopore formation treatment. The resulting mesoporous zeolites can have bi-modal mesoporosity and higher aluminum contents relative to existing mesoporous zeolites.

Mordenite Zeolite Having Excellent Particle Uniformity and Method for Preparing Same
20210179437 · 2021-06-17 ·

The present invention pertains to a mordenite zeolite having excellent particle uniformity, and a method for preparing same, the method including a step for providing an aqueous solution in which a silica precursor is dissolved; a step for providing an aqueous solution in which a structure-inducing substance and an alumina precursor are dissolved; a step for providing an aqueous solution in which a surfactant is dissolved; a step for preparing a silica-alumina aqueous solution by mixing and stirring the basic silica suspension and the alumina aqueous solution; a step for preparing a zeolite synthesis composition by adding the surfactant aqueous solution to the silica-alumina aqueous solution; a step for gelling the zeolite synthesis composition; and a step for crystallizing the gelled zeolite synthesis composition.

PRODUCTION OF PULVERULENT, POROUS CRYSTALLINE METAL SILICATES BY MEANS OF FLAME SPRAY PYROLYSIS

The present invention relates to a process for preparing a pulverulent, porous crystalline metal silicate, comprising the following steps: a) hydrothermal synthesis in an aqueous mixture comprising (A) at least one silicon source, (B) at least one metal source and (C) at least one mineralizer to obtain an aqueous suspension comprising a porous crystalline metal silicate as reaction product; and b) calcination of the reaction product, characterized in that the calcination is conducted by means of flame spray pyrolysis at an adiabatic combustion temperature within a range of 450-2200° C., wherein the suspension having a solids content of 70% by weight which is obtained in step a) is sprayed into a flame generated by combustion of a fuel in the presence of oxygen to form a pulverulent, porous crystalline metal silicate.

PROCESS FOR THE SYNTHESIS, WITH MULTIPLE SEEDING, OF ZEOLITE CRYSTALS HAVING A CONTROLLED PARTICLE SIZE
20210139337 · 2021-05-13 · ·

The present invention relates to a process for preparing zeolite crystals having a multimodal particle size distribution, and the sizes of which are between 0.02 μm and 20 μm, said process comprising a first introduction of one or more seeding agents into the tubular reactor or upstream of the tubular reactor, and at least one second introduction of one or more, identical or different, seeding agents into the tubular reactor.

PROCESS FOR THE SYNTHESIS, WITH MULTIPLE SEEDING, OF ZEOLITE CRYSTALS HAVING A CONTROLLED PARTICLE SIZE
20210139337 · 2021-05-13 · ·

The present invention relates to a process for preparing zeolite crystals having a multimodal particle size distribution, and the sizes of which are between 0.02 μm and 20 μm, said process comprising a first introduction of one or more seeding agents into the tubular reactor or upstream of the tubular reactor, and at least one second introduction of one or more, identical or different, seeding agents into the tubular reactor.

SYNTHESIS OF MORDENITE USING MULTIPLE ORGANICS

The methods for synthesizing mordenite (MOR) zeolite crystals described herein utilize a combination of organics and produce MOR crystals with reduced size, higher Si/Al ratio, fewer stacking faults, less occluded organics in the final product, and a longer catalyst lifetime.

PROCESS FOR THE LARGE-SCALE MANUFACTURE OF ZEOLITE-TEMPLATED CARBON

A method for the large-scale synthesis of a zeolite-templated carbon (ZTC). The method includes the steps of: introducing a bed material comprising a zeolite to a fluidized bed reactor and heating the bed material to a temperature between 550 C. and 800 C.; fluidizing the bed material with a fluidizing gas and maintaining the temperature of the bed material between 550 C. and 800 C.; introducing an organic carbon precursor while fluidizing the zeolite for a period of time such that carbon is deposited on the zeolite by chemical vapor deposition to produce a zeolite-carbon composite; and treating the zeolite-carbon composite with an acid solution such that the zeolite template is dissolved and the ZTC is obtained.

Water-soluble electrolyzed/solvolyzed clinoptilolite fragments and nutraceutical, pharmaceutical, and environmental products based thereon
10894721 · 2021-01-19 · ·

Methods and processes are provided to make clinoptilolite into a water-soluble solvolyzed form with electrolytes suitable for various administration routes for use in the detoxification and rejuvenation in environment arena, nutraceutical arena, and pharmaceutical arena This process includes oral, topical, tablet, pill formulas, biotech delivery and intravenous. Absorption of water-soluble solvolyzed clinoptilolite fragments can aid in detoxification by binding to heavy metals, viruses and environmental toxins and can reduce reactive oxygen species and inflammation related to metals. The process and method described can provide an increase in energy, increase in growth factors that aid in hair, skin, and nail growth, and can provide an increase in focus, concentration, and memory. Water-soluble solvolyzed, electrolyzed clinoptilolite fragments can be combined with one or more dietary supplements, including various vitamins, minerals, and sleep aids to rejuvenate the cells and the environment during and after detoxification.